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Chemical Process Technology Tutorial 2

The document outlines a tutorial for a Chemical Process Technology course, focusing on process flow diagrams (PFDs) and piping and instrumentation diagrams (P&IDs). It includes tasks such as analyzing a PFD, developing diagrams for a stirred tank heater and a surge tank, and exploring multiphase reactors. Additionally, it provides practice problems related to multiphase reactors and their characteristics.
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0% found this document useful (0 votes)
23 views3 pages

Chemical Process Technology Tutorial 2

The document outlines a tutorial for a Chemical Process Technology course, focusing on process flow diagrams (PFDs) and piping and instrumentation diagrams (P&IDs). It includes tasks such as analyzing a PFD, developing diagrams for a stirred tank heater and a surge tank, and exploring multiphase reactors. Additionally, it provides practice problems related to multiphase reactors and their characteristics.
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd

DEPARTMENT OF CHEMICAL ENGINEERING, IITD

CHEMICAL PROCESS TECHNOLOGY & ECONOMICS (CLL371)


TUTORIAL 2
1. Study the PFD called “Industrial Design” and answer the following questions:
a) What is the story of the process shown?
b) How many phases exist in the process?
c) Why are there no reactors or distillation column or heat exchangers in this PFD?
d) Identify each of the symbols used.

2. A stirred tank heater is being used to heat up a process stream to a given


temperature. The temperature of the process stream is to be controlled by the flow
rate of steam, which is passing through a coil that enters the tank but doesn’t
contact the process stream. Because the process stream comes from an earlier part
of the process, its initial temperature is known to vary. Develop the PFD and then
the P&ID of the process.

3. Surge tanks are used as intermediate storage for fluid streams being transferred
between process units. Consider the process flow diagram shown below, where a
fluid stream from process 1 is fed to the surge tank; the effluent from the surge
tank is sent to process 2.
There are constraints on the fluid height in this tank. If the tank overflows it may
create safety and environmental hazards, and if it is too low, there may be problems
with the flow to process 2. Develop a P&ID to control the fluid height in the tank
(the desired height is known as the setpoint).

4. Using the block diagram below, write the summary of the process taking place
and draw a detailed PFD.

Answer:

Problems for practice:

2. Listed below are examples of multiphase reactors used in industry. For each reactor:
1. Draw a sketch and identify the phases
2. Identify and list the dispersed phase and continuous phases for each.
1. Slurry reactor
2. Spray tower
3. Emulsion reactor
4. Bubble column
5. Packed bed
6. Gas-solid fluidized bed
7. Fluidized catalytic cracker
8. Trickle bed

Sample answers

3. For the following multiphase chemical reactors construct a table indicating the phases,
whether they are mixed or unmixed, the major reactions, and in what phases the reaction
is occurring. A sketch may be shown.
1. Oil drop burner
2. Coal burner
3. Cement kiln
4. Iron ore refiner
5. Wood chip burner
6. Concrete pavement laying
7. Spin coater
8. Fiber spinner
9. Catalytic hydrogenation of vegetable oil
10. Oxidation of organic sewage
11. Homogenization and pasteurization of milk
12. Fluidized catalytic cracking of gas oil
13. Trickle bed hydrotreating of residual oil

Common questions

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Phase characteristics, such as the physical state, density, and phase distribution, heavily influence reactor choice and design as these factors direct mass and heat transfer rates, reaction kinetics, and overall process efficiency. In applications like catalytic cracking, a gas-solid fluidized bed is chosen where the solid catalysts provide a large surface area for gas-phase reactions. In hydrotreating, trickle bed reactors utilize a liquid-gas-solid configuration to ensure intimate contact with catalysts for hydrogenation processes. By matching reactor type to process needs, industries optimize reaction conditions for yield and safety .

A PFD might exclude reactors, distillation columns, and heat exchangers to simplify the depiction of processes where these are not central elements, such as preliminary designs focusing on fluid flow, mixing, or phase separation. This exclusion forces the observer to concentrate on other process elements like pumps, compressors, or material flows, providing an understanding of process connectivity and overall material balance without delving into the specifics of reaction kinetics or separation efficiencies .

Block diagrams simplify complex chemical processes by abstracting detailed operations into higher-level units, thus clarifying the primary functions and material flows. Typically, these diagrams include blocks representing major equipment, lines showing material or energy flows, and annotations describing the input and output relationships of each block. They facilitate understanding by highlighting process structure and sequences, making it easier to communicate process concepts and identify bottlenecks or inefficiencies .

The design of the heating coil in a stirred tank ensures efficient heat transfer through indirect contact by maximizing the surface area exposed to the process stream while ensuring that steam, as an external heating medium, circulates through the coil. This method allows precise temperature control by adjusting steam flow rates, maintaining the process integrity and avoiding any contamination that might occur if the process stream and heating medium mixed directly .

When developing a P&ID for a surge tank, considerations include identifying critical control elements like level sensors, overflow and drainage lines, input/output flow regulation, and integrating these into a wider control system. The setpoint is crucial as it defines the desired fluid height, against which real-time measurements are evaluated. This ensures that the system maintains optimal fluid levels by automatically adjusting flows to prevent overfilling or underfilling, thus safeguarding both the equipment and operational continuity .

Sketches and diagrams facilitate conceptualization by visually distinguishing phases, reaction zones, and flow patterns, aiding in the comprehension of complex interactions within reactor systems. In educational and professional settings, these visuals help convey intricate information succinctly, support collaborative design or analysis efforts, and provide a common reference to align understanding and strategies among diverse stakeholders .

Fluid dynamics affect surge tank operation by influencing fluid flow rates and pressure within the tank, impacting the stability and continuity of downstream processes. Tank constraints, such as maximum volume and pressure limits, dictate operational parameters to avoid overflow or collapse risks. Safety is ensured by maintaining operating conditions within these limits using control systems that adjust input or output flows based on real-time data, thereby preventing accidents and maintaining process integrity .

In multiphase chemical reactors, the dispersed phase is typically a minority phase such as solid particles or gas bubbles within a continuous phase, which could be a liquid or another gas. Identifying these phases is critical to understand mass transfer mechanisms, interfacial area interactions, and how each phase's dynamics influence reaction rates. For instance, in slurry reactors, solid catalysts act as a dispersed phase in a liquid continuous phase, impacting how the reactants interact with catalytic surfaces .

The primary challenges in controlling a process stream's temperature with variable initials include maintaining consistent output quality and preventing thermal shock to equipment. The steam flow rate is critical because it provides a versatile way to adjust the heating energy imparted to the process stream, accommodating fluctuations in initial temperature. Effective control involves real-time monitoring and rapid adjustments to the steam flow, ensuring that desired temperature setpoints are quickly achieved and maintained .

Surge tanks serve as buffers between interconnected process units, accommodating fluctuations in flow rates and helping to stabilize upstream and downstream processes. Maintaining the correct fluid height is crucial because an overflow poses safety and environmental hazards, while an insufficient level can disrupt material transfer to subsequent processes. Effective control of fluid height involves monitoring and adjusting inputs and outputs, typically through automated valves and level sensors tied to setpoints within process control systems .

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