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Paper Surface Roughness With 3D Profilometry
Technical Report · January 2014
DOI: 10.13140/RG.2.1.4344.7203
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Paper Surface Roughness
With 3D Profilometry
Prepared by
Craig Leising
6 Morgan, Ste156, Irvine CA 92618 · P: 949.461.9292 · F: 949.461.9232 · [Link]
Today's standard for tomorrow's materials. © 2010 NANOVEA
INTRO:
Paper is still a primary source for communication around the world and is now more portable,
from size reductions and has triggered new research developments with cleaning products,
printing, foods and many others. An important key to growth in the paper and pulp industry is
sustainable use which will require continued research to improve renewable product quality.
IMPORTANCE OF SURFACE METROLOGY INSPECTION FOR R&D AND QUALITY CONTROL
Paper surface topography is vital to the intended use and quality of the product. To control
paper product quality it will heavily rely upon quantifiable, reproducible and reliable surface
measurement. Precise surface measurement and evaluation of a paper product can lead to the
best selection of processing and control measures. The Nanovea 3D Non-Contact
Profilometers utilize chromatic confocal technology with unmatched capability to measure
paper surfaces. Where other techniques fail to provide reliable data, due to probe contact,
surface variation, angle and reflectivity, Nanovea Profilometers succeed.
MEASUREMENT OBJECTIVE
In this application, the Nanovea ST400 is used to measure the surface of three paper samples
for comparative review. The samples range from very rough to premium surface. Additionally,
each sample has received a printed letter from a laser printer to study the effect surface
roughness on ink settling. Several surface parameters can automatically be calculated
including the most common, Sa (average surface roughness), step height, area and many
others.
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MEASUREMENT SET-UP & TIPS:
All samples were subject to the same process and measurement. The optical pen used
provides 12 nanometers of Z resolution.
MEASUREMENT PRINCIPLE:
The axial chromatism technique uses a white light source, where light passes through an
objective lens with a high degree of chromatic aberration. The refractive index of the objective
lens will vary in relation to the wavelength of the light. In effect, each separate wavelength of
the incident white light will re-focus at a different distance from the lens (different height).
When the measured sample is within the range of possible heights, a single monochromatic
point will be focalized to form the image. Due to the confocal configuration of the system,
only the focused wavelength will pass through the spatial filter with high efficiency, thus
causing all other wavelengths to be out of focus. The spectral analysis is done using a
diffraction grating. This technique deviates each wavelength at a different position,
intercepting a line of CCD, which in turn indicates the position of the maximum intensity and
allows direct correspondence to the Z height position.
Nanovea optical pens have zero influence from sample reflectivity. Variations require no
sample preparation and have advanced ability to measure high surface angles. Capable of
large Z measurement ranges. Measure any material: transparent/opaque, specular/diffusive,
polished/rough.
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RESULTS:
Linen Paper
2D Top Surface of Linen Paper
3D Image of Linen Paper Surface
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Profile Extracted From Linen Paper
Profile Extracted 2D Surface Contrast Image
Here we had to use a contrast image of the surface in order to see the
absorbed ink.
ISO 25178
Height Parameters
Roughness values calculated
outside of ink area:
Sq 6.806 μm
Ssk -0.2662
Sku 3.056
Sp 40.64 μm
Sv 28.85 μm
Sz 69.49 μm
Sa 5.435 μm
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RESULTS:
Standard Paper
2D Top Surface of Standard Paper
3D Image of Standard Paper Surface
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Profile Extracted From Standard Paper
Profile Extracted 2D Surface Contrast Image
Here we had to use a contrast image of the surface in order
to see the absorbed ink.
ISO 25178
Height Parameters
Roughness values calculated
outside of ink area:
Sq 5.722 μm
Ssk -0.3142
Sku 3.080
Sp 42.26 μm
Sv 34.19 μm
Sz 76.45 μm
Sa 4.586 μm
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RESULTS:
Premium Paper
2D Top Surface of Premium Paper
3D Image of Premium Paper Surface
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Profile Extracted From Premium Paper
Profile Extracted 2D Surface Measurement
Here we did not have to use a contrast image because the ink was
still measureable resting on the surface.
ISO 25178
Height Parameters
Roughness values calculated outside
of ink area:
Sq 3.176 μm
Ssk -0.08975
Sku 3.302
Sp 14.07 μm
Sv 18.62 μm
Sz 32.69 μm
Sa 2.498 μm
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Height Parameter Definition
Mean surface roughness.
Arithmetical Mean
Sa
Height
Sa =
Standard deviation of the height distribution, or RMS surface
roughness.
Root Mean Square
Sq
Height Sq =
Computes the standard deviation for the amplitudes of the
surface (RMS).
Maximum Peak
Sp Height between the highest peak and the mean plane.
Height
Maximum Pit
Sv Depth between the mean plane and the deepest valley.
Height
Sz Maximum Height Height between the highest peak and the deepest valley.
Skewness of the height distribution.
Ssk =
Skewness qualifies the symmetry of the height distribution. A
Ssk Skewness negative Ssk indicates that the surface is composed of mainly
one plateau and deep and fine valleys. In this case, the
distribution is sloping to the top. A positive Ssk indicates a
surface with a lot of peaks on a plane. Therefore, the
distribution is sloping to the bottom.
Due to the large exponent used, this parameter is very
sensitive to the sampling and noise of the measurement.
Kurtosis of the height distribution.
Sku =
Sku Kurtosis
Kurtosis qualifies the flatness of the height distribution.
Due to the large exponent used, this parameter is very
sensitive to the sampling and noise of the measurement.
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CONCLUSION:
In this application, we have shown how the Nanovea ST400 3D Profilometer can precisely
characterize both the topography and the nanometer details of paper surface. From our
results we can see how the difference in surface roughness clearly changed the settling and
possibly the absorption of ink from the laser printer. With this information the surface
topography of paper can be investigated and to what effect it has on the settling and
distribution of ink on the surface; a crucial understanding for paper product use. To further
view in detail a 2D cross section can quickly be chosen to analyze, at nanometer range, step
height and planarity among others. Special areas of interest could have been further analyzed
with integrated AFM module. Nanovea 3D Profilometers speeds range from 20mm/s to 1m/s
for laboratory or research to the needs of hi-speed inspection; can be built with custom size,
speeds, scanning capabilities, Class 1 Clean Room compliance, with Indexing Conveyor and for
Inline or online Integration.
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