analusu 1

Name of Experiment.. OOlt -......... Date.. 24 /03 / 20l?

Experiment No.. ***....

5
Experiment Result.
Page No. 2'
MODEL PROCEDURE FOR THE SYSfEMA1sc
ANALYSTS OF SLMPLE LNOnGANÍG SALT
Salt -1
|AM: Analyze the given inosganic salt systematically and
idenhfy one acid and one basic sadical.
PRELLgNARY 1eI
a. Phy sical state - cxystalline solid
6. Colour- Colousle ss
c. Smell / Odous
ExPERMEN o6sERVATLON LNPERENCE
Take Small am ount of Smell of ammonia. May be NH¡t caHon
Salt on-a watch gas
glass and [Link]
dyops of watey, mix
it with a help or
glass od, Note
down the odouy
d. Dry heaing test
EPERLMENT OBSER VA15ON GNFERENCE
Make salt in a dry Colourtess gas wlih May be NH¡t
hard alass test tubepung ent smell / odour
and heat it at Arst of ammonia
gently, then shsongly
eScli, tesr Ererrert . E e n g t Fest

Hor in a dtu test tube rangerd opors

Flone coloUY imported. Ine above vopaurs YelowSoiunon 1s

chorocetshc
f. Flome test - tn are -ent) re passed ino a Oyrained
(2Syi2, Co
test bute containing

vodiGals (Co,) 1o he aboe yeouw Ergh yeo

* Detechon of first group odd SNFERENCE soluhon add aceHc precipiae is oraind con fie) (
ErERSMErK 08SEPVA1orN
acid and lead
Solt di1. HCI
b8raia colouriess, absent (co) acetate soluhons
cdoutess g0s MCI(a4) + AgNO (aa) ’ MNOg (a4) > FacI(s)
Curdy he ppt
Deiecion cf oroup 1 ocd vodicab (Cr,B, NOS, CgC00)
ErEPMEN CesERVA10 SNFERENCE 2KHSD + 4Na HSOa + 2Cc, o
o. Solt in odry testi) A colour less pungentoup ocid Yodicals
tube * Cone, nsoa Srnell g0s which gi ore presernt Co0,d,t .+ 2NaOH Na, Croa + 2HCI
J
dense ushite Fumes May be Chioride ion Yellow solukon
with o gioss rod NaCr04 + (CA,coo),P% ’ 2CeCOONa + Pb Cx De
d'pped in Nh; on, vellow pp
when exposed o he
nout of the test ANALYSS OF BASJC RADICAL -
ube
* Pepasation of orig inal soluHon
o Confirngry test For GI hepazah On+ About holF test bube of solvent is huken
EREREMENY OGSERVKLoN fNFeRENCE the salt is added itHe by little coits con Stahr shaking w,
i) Silve rdteae test Acuedy uwhite precip Chlorde ion is a satusated clear, homnogenous soluhon s obtained.
irate ushich is sdluble .
conHemed. NO1E: Always use 2 oy 3 dsops of oNginal soluhion rr
Lhion detechon of basic adical.
jCheornyl chloride trs
 Ammonium ion ((NHy) Experiment...Solt
analw
Date. 24/03/2013
DErechon of zexO 9r0up basic radical, Name of
S Page No. z?
* INFERENCE Experiment No. Experiment Result...
OBSERVAsoN
ExPERSMEN
Pungent smeling gas Zero gOup acid
Salt+ dil. NaOH soluhon (arnmonia) is evoved Yadical is presernt
+ 6oil May be ammonium
which gives dense
whlte Fumes wih ion. (NMyt)

glass rod dipped in

Conc. HCI.

oConfirmaBoxy test ( Nesslexs Yeagent test) Aromonium ion (NHgt)

Salt soluhon + excess- Brown precipitaBe is
is confismed.
dil. NaoH + Nesselex s obtoined
veagent
NMaX t NaoH +NM, + H,O + Noax

NessHers Amido iodomedvty

Yeagenh (Brouon preipibot)
RESULT
Radical Name Foxmula Ghtoup
Acid radical Chloide

Basic vadical Ammonium Nhat Zexo

Sa1t Ammonium
chloíde
Name of Experiment.. Salt anaysu
.... ....
-2 Date. OS4/ 12/2013
Experiment No. Experiment Result. Pago No 2
MODEL PROCERURE FOR THE SYSTEMATIC
ANALVSSS OE SfPLE NORGANI c SALT
Salt - 2

ASM: Analyze the given inoxganic solt systermiatically and idenrify

aAOne acid and one baslc radicals.

s PRELSNÍ NARY ÍES1

he pseliminary test which is pevfosmed with doy salt is callea
dru test
a. Physical state - Crystalline solid
6. ColouY - Colour less
C. Solubility tes+
1Watex DilHC)
Cold Hot Cold Hot
X

d. Flanme tes - NO chayachexiShc Flame. (Bat SY, catare

absent)

1 ANALYSÍS OF ACN RARLCALS

*DetecHon of First goup acid xadical (co,)
ExPERSMENT O8SERvATION SNFERENCE

Salt + dil. HcI No GziSk effervestence I g30up acid yadicab

liberating colouY less, absent
odour less gas.
 * Detecion of qroup 2
acid Yadicals (CI,B . NOg,cHcoo) Name of Experiment.. Salt anals .....
2 Date. OS12/2023
OBSERVA1LON LNFERN CR Experiment No. Experiment Result.
Page No.2
ExPERÍMEN
**.....

No wbite fumes Chloside (c) is cbsen

a. Salt in a dy test No Yeddish bxoon Boomide (BY )is ahsen ANALY5fS OF BASIC RARSCALS
tube + Conc. H,S0a Detechon of basic rad'cal (excepr zero qroup) oF salt is bosed on
fumes
precipitaiorn reachon in soluHon. hence its necessary to prepare
6. 1F no Yeachon in |original sOluhon.
cold condiHon
Salt+ dry test tube+ No xeddish- byown Nitrate ion (NO) is
fumes absent k Nelechon of zeo group basic vadical (NH- Ammonium ion)
Conc. Ha 50a + Cu
ExPERSMENT O6SERVATLON SNFERENeE
turnings + heat No Smelh of vinegas Acetate CCH, COO") is Salt t dil. NaOH NO Pungent smellingZero group basic
absent
3oluhon + boil gas (am monía) is Yadicals are a6sen
group acid xadical evolved
are ab sent

* DetecHon of qxoup M acid adicals (Sulphate r S04) *Detechon of group basic radicals (P6*2- Lead ion)
ExPERLMENM 0BSERVA1SON SNFERENCE
ExPERSMENT OBSERVA1sON TNFERENCE Originai soluhon t No whie precipitate 1 g0up basic xadi cab
1. Bariam chloide test
! gxoup acid xadica dil. HCL is o6tained. absent P6*)
Salt solution + Bal A Ehick white preci-
Soluhon present
pitate is obtained May be so,-t ion
o Confismalovy test fos Sol íon Detechon of group I basic Yadicals (Cutt, Cd2)
2. Above precipitate + ExPERSMENT O8SERVAT1ON -NFERENCE
ex cess of Conc. ue
Precipitate is insoluble So is confismed Original soluhon + NO whle poecipiate Goup basic Yadicals
2. Lead Acetare test dil, nCi+ H, S are absent (cd* Cut)
Salt solui on + Feu
White
preipitatc dbraincd
drops of acehic acid soluble in excess Of ho SO2 is confismeo *Detechon of qxoup basic xadicals. (A1, Fet3)
ard lead acetate ExPERSMENÍ NFERENCE.
ammonium aceate
Na, So4 (a4) + Gac, Caa,) Original soluHon + Nhc No precipiate Dgoup baic vadicols
’ Basoa (s) + s)+ Excess of Nn4 OM
white 2NaCi (aq) axe absent (Fet3, Art3)
Na, 504 + precipitote (aq)
Pb so4 ts) +
Ohite precipitate 201,cOO H(aq)
 basic xackcals (2n, 1n t2)
* Detecion of v qroup Name of Experiment.. Salt araysis 2 Date. OS /12/203
Page No Zs
0BSERVAfON INFERENCF Experiment No Experiment Result.
ExPERINENT

Original soluton + No precipitate s group baaic RESUILT

formed Yadicals ae abent
NHaCI (S) + Excess ot Radícal Name Fosmula
(2nt,Mn12)
NMp OM 80luion + H,S Acid xadical Sulphate So4-2
Basic aadical Magnesium Mgt V
Detecion of Vqroup baic todicals (Bat, Srt?, Ca) Salt Magnesium Mgsoq
ExPERTMENT OGSERVALoN INEERENCE
Sulphale
Oricinal solaton+ NYaCi No ahite precipiBakey gsoup bawic Yadicod
(s) + Excess of NH0M is Poxmed absent
Soluhon + Ammonium
CarbonaBe sotuhon

t Detechon of oroup basic tadical Chg*t ) + Confiamabon

Expeximent ObservaHon Snfeverne
Orig inal soluhon +NraCAcohite crphalline Pp goup baic
(s) + Excess of NHOH fosmed.
soluton + isodiom
sadicals poesent
Mgt2 is confiomed
ydrogen phaphot or
dihydrogen ammonituan
phaphore Jroch the
innex odlls ot Hhe test
tube with a qaw 0d
Smootly
Mg*(oq) +(Un),PO¢ (aq) + NH4 OM (aqa)
Mg (NHg)Po¢ (3) +
white cryst alline
2hm aci (aq) + H,o()
Name of Experiment. Date
Page No.6
Experirnent No.... Experiment Result.

MODEL PROCEpURE FOR THE

SYSTEMA1LC ANALYSLS Oe spE
INORGANDG SALÍ-3

Pgn: Analyze the gien inorganic salt systematicaly ond

identify one acid and one ba sic Yadical

1PRELsMENARY fESt
The preliminary test which is pexfomed with dy salt is called
dry test.
[Link] state Cystalline solid
[Link] - Coloutless
c. Solubiiity test
Water Dil. HcI
Cold Hot Cold Mot
X

d. Flame test - NO characterishc flame (8af2, Srt, Cat2

are absent)

1ANALYS[S OF ACLO RADLCALS

Detechon of Fisst gzoup acid radical (cos)
ExPEAIMENT OGSERVASON INFERENCE
Salt + dil. HC No Gsis keffervescene I group acid
ibexating colou less, Yodicals absent
odouxlesS gas
 rodicals (Cr, Br NOS, ChgCoo)
* Detechon of axoup 2 acid
Name of Experiment. Date.
OBSERVAfION
LNFERENCE Page No G2
ExPERÍMENT
Experiment No. Experiment Result....

NO white fumes are CI ion is absent

Salt + Concentyated
evolved

Brownfumes are Br ion may be +Acid radical present in given Salt is Bromde ion (Gr)
evolved Present
+Basic Yadical present in given salt is Amm Onium ion (NH¡t)
o Confimatory test for Br ion + Hence, the given salt is Armmoniurn Bromide CNt¡br)
EXPERLMENT oGSERVATLON LNFERENCE

PgNog test V EQUA11ONS

Salt + AgNOg soluHor Pale yellow ppt obtainet Br ion is con firmed. Zdentification of Bx
Partialty soluble in ’ 2NaBo.+ MyS04 24Bx + Na, SO4
NM4OM Reddish byown
alobule test Fumes
salt solutiont kMng Orange red globule Br- ion is con fimed
Coystals +Conc. HcI is formed * Confimation of By
OY Cl, water. Shahe
wetl Na By + AgNOg ’ AgBr + NaNO, (AgNQ test)
Ye llow ppt
HO ANALYSIS OF BASTCRA0SCALS (Globule test)
* Detection of qxOup 0 basic radicals Sp aringly soluble complex
ExPERÍMENT O8SERVArçoN LNFERENCE
Salt + di). NaO + white dense fumes NHgt ion may be *Tdentificakion of Nrnt
Glass rod dipped axe obsesved. present ’ NM4t + Na0M NHg + Mg0 t Nat
in concentrated HCI ’ Nh4CI fwhite fumes)
bxought neay mouh
of best tube * Confismation of NHgt
o Confisnatory test for Nnat ion + Nn4 t + 2K,Ha I4 t 3 Naon
ExPEREMENT OBSERVTION LNFERENCE
Salt solution + Naon Brown ppt is formed NHt ion is confiymed (Millon's base )Brown ppt
+ Nestlers eagernt
Name of Experiment .......
Date.

Expeniment Result.
Page No63
Experiment No.

SALT ANALYSTS 4

TPRELÍMINARy fES:
+ State : Coystalline solid
Colour : white
Solubility: Soluble in Ho

TTOEN1IELCA1LON OE Acgo RADICALS

*Detection- of group 1 acid adicals ( C ,)
ExPEREMENT OBSERVATLON LNFERENCE
Salt + dilute HCI No Brisky effervescend Co,-2 jon is absen t

* Detection of group 2 acid radicals (CI,Br7 Ng7

ExPERIMENT OBSERVATTON LNFERENCE
Salt + Concentrated No white fumes CI ion is absent
HzS04 NO byown fumes Bo ion is absent
Salt+ Cu tunnings No bxown fumes NO, ion is absent
+ Concentrared h, SO4 evolved
+ Heat

t Detechon of group 3 acid xadicals (S0,)

EXDERMENT O8SE RVATpON LNFERENCE
Salt solubon + Bacl, White Ppt which is S042 ion is present
Solution insoluble in excess of and con,fiymed.
NH;OM
 RADLCALS
0 LDE NFLCATLON OR BA5Sc
Name of Experiment. Date..

Yadicals. (NH, )
0basic
Page No
* dentificabion of group Experiment No. Experiment Result.

LNFERENCE
ExpERLMENT
O8SERVefLON
Add 3 ox 4 dyops Blue precipibate At3 ion is
white Nngt Bon is absent of itmus solution
Salt solution + dil. Na4 NO dense Aoats in colourless con fismed.
in fumes evolved and then add NMg0n solution.
t glass vod dipped
Concentrated Hci brought solution till 6lue colour
heay mouth of test Fades.
bube
VReSULT: -
radicals (P6 )
* Ldentification of group 1 basic
ExPERIMENT OGSERVMcON INEERENCE ’ Acid vadical present in given salt is Sulphate ion (S042)
Sat solut ion + diluBe MCI NO cwhite ppt P6 t2 ion is obsent +Basic xadical present in given salt is Aluminium ion (At3)
Hernce, the givern salt is Aluminium Sulphate (Al, $04))
Cdentification of qroup 2basíc Yodicals (Cut2)
ExPERLMeNT OBSERVAtoN INFEREN CE.
yEQUAT[ONS
5alt soluhon +dilute HcI NO 6lack ppt Cut2 jon is absent
+ 1,S Solubion
*Jdentiicahon & con fiymation of sog?
’ Na,SO4 + Bacl, + BasO4 + 2NaCI
white ppt.
Tdentification o Giroup 3 basc vadical (AIt3)
ExPER[MENT OGSERVATLON INFERENeE *Ldentification of Ait3
Salt solution + Nn4 CI (S) Cühite gelatinous ppt Art3 ion may be + AI(0H)h t 3NM4 CI
+Nng0H (og) for med present helatinous white ppt
o Confrmotoxy test for A1t3 ion
Ex?EREMENT OBSERVATTON LNE ERENCE *Confimation of At3
Bigsove the white ’ Al(oH), t 3MC) ’ AlCl t3H,0
gelatinuous ppt in + Ar(Onh +3 Nn¡CI
dilute Hel and divide
Gelatinous ppt reappears
the solution inbo 2 part
For 1s part of soluHon tshite gelohnaes ppt
add Nna On solution.
At3 ion ig confirmed
appears
Fox 2rd paxt of soluhon
Name of Experiment. Date.

Experiment No.
Page No s
Experiment Result.

Salt anolssis -5

’Physical-state : Amorphous solid

+ColuY : white
+ Solubility : Lnsoluble in wate, soluble in HCI

1 LoENFCATLON De ACIp RADSCALS

Sdenification of grOyp 1 acid xadicals (co,-)
we EXPERLMENT OBSE RVAtON TNFERENCE
Salt + dilute HCi/M,So4 Gxisky effervescence Co,2 ion may be psesert
oCon fiYm atory test for Co,-2 ion
EXPERIMENT 08SERVATION INEERENCE
3alt + dilute HcI Brisky efervescence
be vating colourles
0dour iess gas
ass colouxless gas Lime water turns |Co,2 ion is con fimed
though lime oater milky

1OENTEFLCATON OF BASIC RADsCALS

* Tdentification Of qoup 0 basic yYadicals
ExPER[MENT OBSERVATION TNFERENCE

Salt *oluhon + dilule No dense white NH¡t ion is asent

NaoH+ glass rod dipped fumes evo lved
in concentrared HCI
bYought near mouth
Of test bube
 basic radicals
+Ldentificalion of group 1 OBSERVA1LON
Name of Experiment. Date....
Page NoG6
LNFERENCE Experiment No. Experiment Result
ExPERINENT
ppb P% +2 ion is absent oConfirmatoxy test for Cat2 jon
Salt solubiont dilute HCi NO cohite
ExPERSMENT OGSERVATLONS INFERENCE
* 1dentiflcation of group 2 6asic Yadlcals Salt solution+ white ppt is preer Cat2 jon is
ExPEREMENT O8SERVA1LON CNFERENCE fnmonium oxalate Confiomed
Cutz jon is absent solution (NMa), Con
Salt solution + dilute HcI NO black ppt is
+ MzS solution formed
o Flame test fo Cat fon
*Ldentification of group 3 basic radicals ExPEREMENT OGSERVATLONS ZNFERENCA
TNEERENCE Cat2 ion is
ExPBRTMENT OGSERVATTON
Salt + Concentrated mci Gaick red flame is
Salt solution + NM4CI6) No white gelatinous Ait3 ion is absent make paste and observed Confismed.
+ Nh40M (aq) ppt heat n the burner
with glass rod
*Identification of group 4 basic Yadicais
ExPERINENT OBSERVATION LNEERENCE VRESUL:
Salt soluHon + NnaCI (s) No white ppt Znt2 ion is absent
M¡ oH (aq,)+ H,S sol. No brown ppt Mnt2 on is absent Acid radical in 9iven Salt is Garbon ate ion (co,2)
Basic vadical in given sait is Calcium ion (Cat2)
TdentificaHon af group S basc vadicals Hence, the given salt is Cacium Carbonare (Cacog)
EXPERIMEN OBSERVAT[ON LNFERENCE
Salt soluon t NMaCI (S) white ppt formed Cot, [Link] Sr VEQUATJONS
+NroH caa,) t (NMa),cog may be presert * Bdentificahon Of Co2 ion
oConfrmatoxy tes for Cat2 ion
ExPEREMENT O8SE RVATLON INFERENCE
Salt solution +Potossiur No yellow ppt Batt ion is absent +| Confixmaion Of COg2 ion
Chxomate soluion(K,Gro4)
oConfirmaboxy test for Srt2 ion
Salt solution + Argmoun NO whike ppt Tdenti fication of cat' ion
Srt ion is absent
Sulphate solution
Name of Experiment. Date.

Experirnent No... Experiment Result.

SALT- ANALYSTS -6

TPRELIMINARY TEST
|Physical state : Cystalline solid
Coour : White

|Solobility : Soloble in H0

ALOENTEF1CATsON OF AcIO RADL CAL

* Lde ntficotion Of gOup 1 acid Yadicals

hEXPERLMENT OGsERVATSON INFERENCE
Salt + dilute HCI. No Bxisk efferYescence Co ion is absent

Ldentification of group 1 acid radicals

BrPERLMENT OBSERVATIONS [NFERENCS

Salt + Concentyated No White fumes CI ion is absent

No Bxown fumes BY ion is ab Sen t
Salt + concentsated Brown fumes NO, ion m-y be
|M,SO4 + Cu tunnings + evolved present
Meat
o Confsmatory test foy NOg iOn
EXPERLMENT O8sERVATLON LNFERENCE
Salt soluion t equal Bxouwn ing fos ms NO, - ion is
quantity of Fesog between junction confirmed
sclution +Concentrated of 2 liquids
|M,S04 ttoough walls
of test tube
 Name of Experiment.. Date
LOENIELCA1TON OF BAsIC RAOLCALS Experirnent Result.
Page No 69
of group o basic vadicals
Experiment No.

* Tdentificati on
OBSERVALON LNFERENCE olConfiomation of Znt ion
ExPERIMENT
NM4 ion is absent ExPERIMENT OGSERVATSON INFERENCE
Salt solution + Na0H + No white dense
Fumes Salt soluHon + NaOn white ppt 2nt jon is
glass rod dipped in solution con fismed
Concentsated HCI dipped
Salt soluhon +Potassium No yellow ppt Znt ion is obsent
neay m outh of test
bube
fenocyonide («eeN)

* Tdentification 0f group 1 basic Yadlcals * Zdentification of group 5 bosiG Yodicals

OBSERVATION INFERENCE ExPERTMENT OBSERVpON INFERENE
BxER{MENT
P6+2 ion is absen Salb solution + NNgds) white ppt Batt, Syt os Cat
Salt solution + dilube No white ppt
HCI +NAgCOH) Caq) +(NMa),( ion mGy be preSent
Con gismatory test for Bat ion
OBSE RVALON LNFERE NCG
* dentifi cation of group 2 basíc radicals ExPERIMENT
OBSERVATI ON LNFEREN CE Salt soluion + Yellow ppt Bat jon is
ExpERIMENT
No blach ppt Cut2 jon is absent K,Cro4 soluhon Con firmed
Salt soluhon+ dilute
HCI+ M, Ssolution
oFlame test for Bat2 ion
Salt + Concentrated Apple gveen flame Bat2 ion is confirmed
+ Tdentification of group 3 basic radicals
ExPER[MENT OBSERVATLONS [NFERENCE |HCI+ make pase and is observed
Art3 ion is absent heat on the burnes
Salt solution+ Nn,cI(s) No gelatinous ppt
+ NMa OM (ag) Of glass Yod.

k Identi ficakion of gxoup 4 basic tadicals IY RESULT: -

ExPERLMENT 0GSERVA TLON LNFERENCS
Salt soluion +Nna CI(S) white ppt Znt2 ion may be preen +Acid Yodical present in given Salt ig Nitsate ion (No,)
No bxOuwn ppt Mnt jon is absent + Basic Yadlcal present in given Salt is Barum ion (Bat)
Soluhon Hence, Ehe given salt is Banum Nitsate (Ca(No,), )
 Narne of Experiment. Date
Page No.
Experiment No. Experiment Result.

of NO, ion
1fdentification 3Cu
3cusog+ Nags04 t 2No+ 4 Ha0
’ 2NaNO, + 4H,SO4 +
P2NO2
(byown fumes)

NO, 10n
*Confirmation of
’ NO, + MzS04
3Fet1 4 3n+
’NO + 3Fe f3+ 2M,0
’ HNO3 4 O
Fe (n,0)s(NO)J** + H,
’ [Fe(H,0),J*2 + NO
Bat2 jon
* Tdentifcation of +BacO + 2Nhqt
(Nna),CO3 (white)

ion
* Con firmation of Bat
’ Bat+ KCrO4 + BaCr04 + 2Kt
(Yellotw ppt)
Name of Experiment Date
Page No
Experiment No Experiment Result.

SALT ANALYSIS-7

4PRELSHINARY TEsr
|Phy sical sbate : Crystalline solia
Colout : Pale pink
Solubiliby : Soluble in H,0

1LDENSFLCA1LON OF Aczo RADL CALS

Tdentifcaion of group 1 acd yadicas
EXPERLMENT OBSERVATION LNFERENCE
Salt t dilute HCI No Bxisky efFervescence Co, "2 ion ís absent

* dentification of group 2 acid radicals

ExPER[MENM OBsERVATJON INEERENCE

Salt + Concentsared No white funes CI ion is absent

NO brown fumes By ion is abS ent
Salt + Ceu tunnings + NO brown fumes NOG lon is absent
Concentsated M,So t
heat

* Tdentification of group 3 acid rodicals

ExPERJHENT OBSERVATLON LNFERENCE
Salt soluion + Bacl, white ppt in soluble SO4 2 ion is Present
|solution+ dilute HCI in excess of HC and con fismed
in excess
 Narne of Experiment.. Date.
Page No 72
ANALYSIS OF BASTC RAOTCALS0 bastc radical Experiment No. Experiment Result.
T0
gTOup
* sdentificotion of OBSE RVATLON
LNEERENCE
ExPERLMENT
No Whlte dense NHat is absent
NaOH +
Salt soluhon +
fumes
Acid Yadical present in given salt is Sulphate ion (s0g)
Galass xod dipped in Basic radicol present in given salt is Manganese ion (Mn*)
concentrated HcA brought
tute
Hence, given salt is Manganese Sulphate (MnSO¢)
neas mouth of test

VEQUATIONS
group 1 basic xadicals
* dentification of O8SERVATION [NPERENCE t Equabions involving detechon of s042 ion
EYPERIMENT
NO white ppt P612 ion is absent +BaCl, + Na,So4 +Baso4 t+ 2NoClI
Salt solbont dilute HCI
(white ppt)
basic vadicals
* dentification of qroup 2 O0SERVA TTONS INFERENCE *Equahons involving detechion of Mnt2 ion
ExPERIMENT

No Black ppt Cut2 jon is absent ’ Mnt2 + S -2 + MnS

Salt soluHont diluhe HCI
’ Mn S + 21CI
+ M,s soluhon
Mn Clh t 2 NaOn. +In(o4),o 2NaCI

*Tdentificahon of aroup 3 basic adi cals

EXPERSMEN O8SERVATION LNFEKENCE

Salt sotuHon-+ NnaCI(s) No gelahinous ppt Art3 ion is dbsent

* Tdentificahon of group 4 basic vadicals

oBSERVATLON INFERENCF

Salt soluhon t NMal(s) No whhe ppt Znt ion is dbsent

+Nn¢on(a4) + MyS sol uhon Gxouwn fleshy ppt Nn+2 ion togy be prese
oConfrmahon of Mot2 jon
ExPERIMENT O0SE RVATION INEERENCE

Salt soluhon + Na 0
Broun or buf ppt Mnt2 jon is con Pymed
Soluhon
 Name of Experiment... Date.
Page No.3
Experiment No...
Experiment Result.

SALÍ-ANA LYSÇS 0?

TPRELLMINARY feST

Physical state : Amorphous solic

Colous : White
Solubiliby 1 Solu6le in HCI

LDENTIFLCA15ON OF AcD RA0GCALS

*dentificati on of group.1 acid radicas
oBSERVASLON LNFeRENCE
ExPERIMEN
Bxisky effevescence
Salt+ dilute HCI cog ion may be preset
oConfimatoy test fo Co2 ion
EXPERL MENT OBSERVATLON INFERENCE

Salt + dilute MCI Brisk effervescente wit

colouriess, odourless gas
Gras passed thxough Line water tusns co, on is confrmed
Lime wates milky

DLOENTIFICATI ON OF BASLC RADICAcS (g04p 0)

OBSERVATTON INEERENCE
ExPERI MENT
Solt soluti on + NaoHt No Dense whi te NHat in s absent
glass xod dipped in fumes
concentated HcA
brought neay mouth
of test tube.
 radicals Name of Experiment.. Date.

of group 1 basic
Page No. 74|
* Jdenti fication O8SERVA1ON
LNFERENCE Experiment No. Experiment Result..

EXPER[MENT
P6 ion is absent IV RESULT: -
HCI No whlte ppt
Salt soluhon +dilue

gxoup 2 6a Sic
xadicals Acid Yadical present in qiven solt is Corbon ate jon Co,)
*fdenbification of OGSERVAfLON LNEERENCE Basic xadical present in given salt is Magnesium íon (Mg+)
EXPERSMENT
Cut' jon is absSent Mg Co )
Salt soluhont dilute No black ppt + Nence,given Salt is Magnesium Carbonate
HCI+ H,S solahon
VEqUATLONS

dentificohion of group 3 basic

adicals Ldentificahon of co? ion
NaCI + Co,Tt h,o
ExPERMENT
OBSERVAT[ON LNPE RENCE +Na, CO, +2 HCI
Salt soltuhont Nhaa[S) No gelatinoas ppt A3 (on is ab sent ’ Ca(on),+ CO

* |LdenhH i cahon of Mgt2 ion

+Ma (N PO4 t 2Nat t M,o
Ldenb fcahon of group 4 basic vodicals
ExPEREMENT OBSERVA1LON TNFERENCE

Salt soluhon+ NneCi(S) No white ppt ZntB ion is absent

4NH40Htoq)+ MaS solakon No lesh ppt Mntl jon is ab Sent

*Tdentificahon of group S basic radic als

EXPgRIHENT OBSERVATÍON SNFERENOE
Salt soluhon + NM¡s) NO white ppt Bat,Ss2 and Ct?
ions ae absent

* Tdentifcohon and Con fismokon of aroup 6 basic radicals

ExPERIMENT
06SERVATONS INFERPNCE
Salt soluhon + Nnat (s) white ppt Mgt2 ion is poesent
+Nh¡onfoq)+ NanOa (oa) and confirmed.