Particle Size Reduction and Handling Techniques
Particle Size Reduction and Handling Techniques
Primary/Coarse size
reduction
Miscellaneous
methods
Solid-Gas separation
Dynamics of Fluidization
Storage, Handling Storage of solids particle in gas
and Transport of medium
Solids Transport of solids
Comminution/
Size Reduction
Resource
➢ Books
➢ Compression, impact or shearing loads are used for breaking brittle materials like coal and minerals whereas
fibrous materials like wood and asbestos are disintegrated by exerting tearing loads.
The Mechanism of Size Reduction
Grinding is achieved by mechanical stress followed by rupture and the energy required
depends upon:
1. the hardness of the material
2. the tendency of the material to crack (friability).
The force applied may be compression, impact, or shear, and both the magnitude of
the force and the time of application affect the extent of grinding achieved.
Comminution Laws
The original form of the law says that “energy required to produce analogues changes of configuration of
geometrically similar bodies varies as the volumes or masses of these bodies”
➢ The above statement is not valid when new surfaces are created
The modified Kick’s law that can be applied to crushing states that “the work required for crushing a
given mass of material is constant for the same reduction ratio irrespective of original size”
P DVS ,F
W = = K k ln ……(3)
m DVS , P
Comminution Laws
➢ The laws on comminution proposed by different authors help us determine the energy consumed in
comminution.
Rittinger’s Law (1867):
➢ The law says that “The work done in crushing is proportional to the surface exposed by the operation”
P 6K R 1 1 1 1
W = = K R ( s p − sF ) = − = KR
'
−
m s DVS , P DVS ,F DVS , P DVS ,F
1 ……(2)
KR is the Rittinger’s constant and is the Rittinger’s number.
KR
➢ Rittinger’s number is defined as the new surface created per unit mechanical energy absorbed by
the metrical being crushed.
X X
Cube 2
Cube 1
X'
X’
Force
Line of deformation
Line of deformation
Force
After Breakage
Cube 1 Cube 2
Plane of breakage X-X’ Plane of breakage X-X’
New area created 2A
New area created 2× A/4
X X
X X
A A A/4 A/4
X’ X’
X’ X’
Distance traveled by the to rapture the cube = D Distance traveled by the to rapture the cube = D
➢ It stats that “total work useful in breakage that has been applied to a given weight of homogeneous
broken material is inversely proportional to the square root of the average size of product particles,
directly proportional to the length of crack tips formed and directly proportional to the square root of
new surface created”
Or
➢ It stats that “work required to form particle of size Dp from very large feed is proportional to the
square root of the surface-to-volume ratio of the product”
P 1 1
W = = Kb − ……(4)
m DP DF
➢ Bond constant (Kb) is evaluated by defining Work index
➢ Work index (Wi) is defined as the gross energy requirement in kilowatt hours per ton
of feed needed to reduce a very large feed to such a size that 80 percent of the product
passes a 100 μm screen.
➢ If P in kilowatts, and ṁ in tons per hour,
a) K b = 100Wi = 10Wi When Dp is in microns
P 100 1
W = = Wi 1− ……(6)
m DP RR
DF
Where, Dp is in microns and RR = (Reduction ratio)
DP
Work Index (Wi)
➢ In 1957, Holmes (2) pointed out that, starting from Kick’s law, Bond’s third theory should be revised as
follows:
r
P 100 1
W = = Wi 1 − r ……(7)
m DP ( RR)
He demonstrated that r varies from 0.25 to 0.73 for several materials, and that such a concept leads to
a more consistent work index, Wi, than that calculated by Bond.
Energy for size reduction
➢ For efficient grinding, the energy applied to the material should exceed, by as small a margin as
possible, to the minimum energy needed to rupture the material.
➢ Excess energy is lost as heat and this loss should be kept as low as practicable.
➢ Grinding is a very inefficient process and it is important to use energy as efficiently as possible.
➢ Three theories/laws depend upon the basic assumption that the work done/Energy required to
produce a change dL in a particle of a typical size dimension L is a simple power function of L
dL
dW = −C n ……(1) Where, dW is the differential work done, dL is the
change in a typical dimension, L is the characteristic
L length
General Form
dL
dW = −C n
L
Sugar is ground from crystals of which it is acceptable that 80% pass a 500 μm sieve
(Standard Sieve No.35), down to a size in which it is acceptable that 80% passes a 88
μm (Standard Sieve No. 170) sieve, and a motor working at 5 HP ( working at 90% of its
full power) is used for the required throughput. If the requirements are changed such
that the grinding is only down to 80% through a 125 μm (No.120) sieve but the
throughput is to be increased by 50% would the existing motor have sufficient power
to operate the grinder? Assume Bond's law to be valid.
Ans: The motor has to run 98 % of its full power to meet the requirement
22
Problem 2
A grinder is to be used ( which is 8% efficient) to handle 10 tonnes (1 tonne= 1000 kg) per
hour of an ore ( specific gravity = 2.65). The feed and product analysis are given below
Mass Fraction
Screen Size, mm
Feed Product
-3.327 +2.362 0.143 0.0
-2.362 +1.651 0.211 0.0
-1.651 +1.168 0.230 0.0
-1.168 +0.833 0.186 0.098
-0.833 +0.589 0.120 0.234
-0.589 +0.417 0.076 0.277
-0.417 +0.295 0.034 0.149
-0.295 +0.208 0.0 0.101
-0.208 +0.147 0.0 0.068
-0.147 +0.104 0.0 0.044
-0.104 0.0 0.029 23
The grinder costs Rs. 40,000. It operates on a 24 hour basis for 300 days per year and
the miscellaneous cost amount to 50% of the power cost. Electricity costs 70 p. per
kWh. If the machine depreciates on a straight line basis for 10 years, estimate the
annual processing cost of the ore if the work index of the ore is 13.57 kWh/ tonne.
24
Ans:
Open Circuit: 68.76 kW
Closed Circuit: 19.4 kW
Effectiveness: 78.09%
Problem 4:
Mass Fraction
Mesh size (mm)
Make-up feed Discharge Oversize
to crusher from crusher from screen
Sphalerite having density of 4000 kg/m3 is
-6.680+4.699 0.07 0 0
-4.699+3.327 0.22 0 0 fed to crusher at 10000 kg/h in a closed
-3.327+2.362 0.035 0 0 circuit. Crushed material passes through
-2.362+1.651 0.24 0 0 screen of 0.417 mm size. Rittinger’s number
-1.651+1.168 0.08 0.02 0.03 for the material being crushed is 0.573 m2/J.
-1.168+0.833 0.04 0.04 0.06
The crusher consumes 3.5 KW when running
-0.833+0.592 0 0.06 0.09
empty and 6.5 kW when crushing the
-0.592+0.417 0 0.08 0.12
material. Compute the overall and theoretical
-0.417+0.296 0 0.32 0.34
efficiency of the crusher.
-0.296+0.208 0 0.29 0.22
-0.208+0.147 0 0.12 0.09
-0.147+0.104 0 0.05 0.05
-0.104+0.074 0 0.02 0
Make-up feed to crusher = F, Discharge from crusher =Pc
oversize from screen =R
Ans:
Overall efficiency: 8.785%
Theoretical efficiency: 19.03%
Crushing Efficiency
➢ The ratio of surface energy created by crushing to the energy absorbed by the solid
is the crushing efficiency and is denoted by c
➢ If es is the surface energy per unit area, sp and sF are the specific surface areas of
product and feed, respectively, then the the energy absorbed by a unit mass of the
material (Wn)
es (s p − sF )
Wn = ………..(11)
c
➢ The surface energy created by the fracture is small in comparison with the total
mechanical energy stored in the material at the time of rupture.
Ref. McCabe, Smith
➢ Rest are converted into heat during the time of rapture.
➢ The energy absorbed by the solid Wn is less than that fed to the machine.
Wn es (s p − sF )
W= = ………..(12)
m mc
➢ So the power required by the machine is
mes (s p − sF )
P = Wm =
mc
Where, 𝑚ሶ is the mass flow rate of the feed.
➢ If the sauter diameter of the feed and product is DVS,F and DVS,P respectively then
6mes 1 1 6
P= − ………..(13) sp =
mc s DVS , P DVS ,F s DVS
Several probabilities involved
1. whether or not the particle hits an objective.
2. whether collision is strong enough to produce a stress larger than the breaking
stress of the material.
3. whether crack tips within a solid will propagate and eventually break the solid.
The general equation should include these three different probabilities, along
1
with n
L
Since specific surface is inversely proportional to particle size, equation 1 can
be rewritten as follows:
dL
dW = −C n
……(1)
L
ds
= C 1LN
……(8) Where, N = n-2
dE
ds
= K ( Pc )( P )( Pa ) LN ……(9)
dE
Where,
Pc is the probability of collision,
Pσ the probability that the material’s breaking stress will be exceeded,
Pa the probability of crack tip propagation,
and K is a constant.
Pc Pσ Pa
Probability of collision
L v p
2
Where, D is the diameter of the objective and v is the
=
18 D particle impact velocity and L is the characteristic length
of the particle and μ is the viscosity of the surrounding
fluid (mostly air)
ηT = Pc
ψ
Probability of Exceeding Breaking Stress
According to Hertz , the maximum stress produced in a material at impact is expressed by:
1 3 4
−
m1m2 2
1 1 1 − 1 1 − 2
5 5 5
max = a v +
5
+
m1 + m2 r1 r2 1 2
where m1 and m2 are the masses of the two bodies
ε1 and ε2 are the moduli of elasticity; β1 and β2 are Poisson’s ratio of the bodies.
v is the relative velocity of the particle
Rumpf, H., Chem. Ing. Tech. 31, 323 (1959).
Probability of Exceeding Breaking Stress
The probability of exceeding the breaking stress of material is proposed as
− kP
Pa e
P is the pressure within the crusher and k is a constant which depends on the crushing mechanism
Final Correlation
m
a − kP
s = E K Pc 1 − e L
N
……(10)
max
Problem 3
A material is crushed in a Blake jaw crusher such that the average size of particle is
reduced from 50 mm to 10 mm with the consumption of energy of 13.0 kW/(kg/s).
What would be the consumption of energy needed to crush the same material of
average size 75 mm to an average size of 25 mm :
Which of these results would be regarded as being more reliable and why ?
Ans: Consumption of energy using Bond’s law / Kick’s law will give more accurate estimate for the given
problem
41
Different stages of size reduction
Fx = ( F1 L tan ) / 2 x
Fx
3. Spindle: it carries the maximum load and is therefore built of great strength and capable of withstand continuous shock or load.
4. Suspension bearing: it is a split steel nut with a downward taper and fits the sleeve of the spindle. It rests on the wearing rings of the
spider.
5. Gear: it is made mostly of cast steel.
6. Counter shaft bearing: it is made as a integral part of the bottom plate and is made extra long and capable of adjustment to take up
wear on the gear and
Operation of Gyratory Crusher
The crusher can be of short spindle, long spindle or fixed spider type. The
capacity varies with different types of materials and operations. The
capacity is expressed in terms of reduction tons.
Adjustments of gyratory crusher are a) width of discharge opening, b)throw
and c) speed.
Smooth-roll crusher
N sinθ
θ L − d cos
R=
θ
2θ
2(cos − 1)
Tcosθ
To estimate the radius R of the roll, the nip angle, 2θ is required
L
(1 + 1.12 )
K =
(1 + 6 )
Roll Crusher Circuit
Capacity of Roll Crushers
Problem 7 : In a roll crusher, rolls of diameter 1 m each are set in such a manner that
minimum clearance between the crushing surfaces is 15 mm. If the angle of nip is 31 deg
the maximum diameter of the particle (in mm) which can be crushed is…?
Hammer Mill
➢ The hammer mill or swing hammer crusher or impactor is
used as a primary crusher for reducing runoff quarry
material to a size of less than 1” or as a secondary crusher
to crush to ¾” size feed or less.
➢ It is almost confined to softer, easily crushable such as
phosphates, gypsum, barite, asbestos rock, and cement
rock and hard limestone (being the hardest rock commonly
ground).
➢ The mill is particularly useful for clayey material that would
clog reciprocating type primary crusher.
➢ It is also used for crushing bituminous coal for coke ovens,
power plant.
➢ The hammers are suspended by pins between heavy steel
dishes which are spaced by suitable spacers. The shaft is
carried on heavy bearings.
➢ A heavy flywheel is mounted on one side of the shaft; the
other end is fitted to the drive pulley or directly to the
motor.
Force in hammer mill breaking
Let H be the hammer hitting a falling particle. If M is the change in momentum of the particle b in the
direction of the velocity of hammer, the average force of blow = F av = M/t, where t is the time taken by the
particle to reach a maximum velocity i.e.
Where W is weight of the hammer, u= velocity of the hammer, 1.5 is experimentally determined constant, t
for highly elastic substance is 0.001 sec and for inelastic substance 0.002 sec. So,
a) characteristics of rock
b) size of feed
c) type of mill
d) grid spacing
e) hammer weight
➢ Another type is rod mill which delivers a more uniform and granular product. The pebble is a fluid with ceramic pebbles as the
grinding media and may be lined with ceramic or any other non-metallic liner.
➢ Autogenous mills are one of the latest developments and are gradually coming into use in different industries where the specific
gravity of the material is high and contamination with the grinding media is not desired. In principle the balls are replaced by large
lumps of the ore itself which act as media.
Mechanism of Crushing in Tubular Mills
Tubular Mill Types based on discharge
Basic design parameters of the tubular mills
B
M 2 Mg cos = v = linear velocity (m/s) of the ball
R (R − r) R, r = radii of the mill and ball,
respectively
Mg
A
At the critical speed (vc) of the ball mill = 0 cos = 1
θ Mg cos
c2 4 2 ( R − r ) 2 c2
g= =
( R − r ) ( R − r ) 3600
Where v = 2(R − r)ω/60 rpm
……(8)
At the rotational speed , v = 2(R − r)ω/60 rpm
Substituting
[2 ( R − r ) ]2
cos =
9.81( R − r )602
At u = 0, cos =1, the force of gravity tending to pull the ball
off the wall will be at a maximum and the speed required to
overcome this force is known as the critical speed.
Denoting the critical speed as vC,
In a ball mill of 2000 mm diameter, 100 mm diameter steel balls are being used for
grinding at a speed of 15 rpm. At what speed will the mill have to run if the 100 mm
balls are replaced with 50 mm balls, all the other conditions remaining same?
Final Product
Open Circuit
overflow
underflow
Problem 5
Crushed product of a primary crusher having 57% of +1 is sent to 1 screen. The
overflow of the screen is again crushed in a secondary crusher to –1 size and sent
along with underflow of the screen as final product.
(a) Draw the crushing circuit with all details.
(b) Calculate the rate of the material crushed in secondary crusher if the effectiveness
of the screen is 80% based on oversize
(c) Calculate the same when effectiveness of the screen is 80% based on undersize
The feed rate to the primary crusher is 100 tons/hr.
Solution:
As the product from the overflow from the screens are not fed back to the same
crusher the entire crushing cycle is an open circuit operation
Solution (contd):
The crushing circuit for the problem is shown in the Figure
100 tph
Primary
Crusher
Product
43% of -1” (U1) 57% of +1” (O1 )
Secondary
1 Screen
(O2 ) Crusher
57
∴ Weight of overflow obtained from the screen = = 71.25 tons/hr (O 2 )
0.80
Circulating load
Oversize
Feed Crusher Screen
Undersize
Product
Problem 6
0.46(C+100)
∴ = 0.85 ⇒ C=117.95 tons/hr
C
Circulating load if the screen efficiency is based on oversize = 117.95 tons/hr (Ans (a))
b)
(C +100)
0.54(C +100)
100
∴ = 0.85 ⇒ C=117.86 tons/hr
0.54(C+100)
Circulating load if the screen efficiency is based on undersize = 117.86 tons/hr (Ans (b))
Problem 7
In the crushing circuit shown in Figure , calculate the circulation load (C in tph) and total load on ½ "
screen. Assume steady state operation.
Screen efficiencies (η) are based on oversize material.
Solution:
+1" material in the feed to 1" screen=0.60×200=120 tons/hr
Colloid mill
Working principle
➢ Colloid mill works on the principle of sharing
➢ The main function of the colloid mill is to ensure a breakdown of agglomerate or in the case of emulsions
to produce droplets of fine size around 1 micron.
➢ Rotational speed of the rotor varies from 3000-20,000 rpm with the spacing between the rotor and stator
capable of fine adjustment varying from 0.001 inch to 0.005 inch depending on the size of the
equipment.
➢ The feed being forced through the narrow clearance by centrifugal action taking a spiral path.
➢ Most of the colloid mills are fitted with water jackets and it is also necessary to cool the materials before
and after passing through the mill.
Fluid energy mill
Fluid energy mill
➢ Product 0.5 to 10 m
There are two types of grinding practices i.e. “wet” and “dry” grinding. The selection of the process is
mainly governed by type of material and use of material. If water changes physical or chemical properties
of the material, dry grinding is a must. Conversely, if the finished material is to be used as a suspension in
water and classified by hydraulic method, then we prefer wet grinding.
Wet grinding has got the following advantages:
1. lower wear rate of mill liners and grinding media compared to wet grinding
2. Higher percentage of fines in mill product. In many cases, this is desirable e.g. cement,
talcum powder, pulverized coal etc.