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Powder A Analysis Results Summary

The document presents the analyzed results of a sample identified as '1' using the FP method, conducted by Mukesh on December 8, 2023. Key components identified include CaO (57.1 mass%), SiO2 (21.2 mass%), and MgO (11.6 mass%), along with detailed measurements and statistical data. The analysis was performed under specific conditions with a focus on various elements and their intensities.

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Shalini Dolai
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14 views1 page

Powder A Analysis Results Summary

The document presents the analyzed results of a sample identified as '1' using the FP method, conducted by Mukesh on December 8, 2023. Key components identified include CaO (57.1 mass%), SiO2 (21.2 mass%), and MgO (11.6 mass%), along with detailed measurements and statistical data. The analysis was performed under specific conditions with a focus on various elements and their intensities.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result

Sample Information
Sample name 1
File name 1
Application Powder_A
Date 08-12-2023 18:37
Analyzed by MUKESH
Counts 1
Comment FP

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 50 6.3
Mid-Z C 35.0 342 1.6 50 27.5
Low-Z Open 6.5 126 1.6 50 37.3

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 CaO 57.1 mass% 0.103 0.0150 0.0449
2 SiO2 21.2 mass% 0.0552 0.0106 0.0317
3 MgO 11.6 mass% 0.219 0.365 1.10
4 Al2O3 5.22 mass% 0.0511 0.0419 0.126
5 K2O 2.35 mass% 0.0250 0.0210 0.0631
6 Fe2O3 1.59 mass% 0.0066 0.0020 0.0061
7 SO3 0.574 mass% 0.0047 0.0065 0.0194
8 TiO2 0.191 mass% 0.0081 0.0156 0.0469
9 SrO 0.168 mass% 0.0004 <0.0001 0.0003
10 MnO 0.0300 mass% 0.0015 0.0031 0.0093
11 ZrO2 0.0240 mass% 0.0005 0.0004 0.0012
12 NiO 0.0090 mass% 0.0004 0.0009 0.0027
13 Cr2O3 0.0085 mass% 0.0019 0.0051 0.0153
14 ZnO 0.0068 mass% 0.0002 0.0004 0.0012
15 Rb2O 0.0056 mass% <0.0001 0.0001 0.0003
16 CuO 0.0044 mass% 0.0003 0.0006 0.0017
17 Y2O3 0.0020 mass% <0.0001 0.0001 0.0004

Spectrum
cps/μA
Ｘ 10 Ｘ 5.0 Ｘ 0.070
1.0
Mg-Kα

Mn-Kα
Ca-Kα

Cu-Kα

Rb-Kα
Fe-Kα

Zn-Kα
Cr-Kα

Ca-Kα-Ca-Kα-SUM

Sr-Kα
Ni-Kα

Zr-Kα
Zr-Kα
Al-Kα
Si-Kα

Fe-Kα-ESC Ti-Kα
S-Kα

K-Kα

Y-Kα

Y-Kα

0.8

0.6
Intensity

Ca-Kβ1

Rb-Kβ1
Fe-Kβ1

Zn-Kβ1

Sr-Kβ1
Ni-Kβ1

Zr-Kβ1
Si-Kβ1

Ti-Kβ1
S-Kβ1

0.4

0.2

0.0
1.0 1.5 2.0 2.5 4 6 8 10 12 14 20 30 40
Low-Z Mid-Z High-Z keV

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