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Powder Sample Analysis Results

The document presents an analysis of a powder sample conducted by Mukesh on December 8, 2023. It includes detailed measurements of various components, with SiO2 being the most prevalent at 57.5 mass%, followed by CaO and Al2O3. Additionally, the document outlines the measurement conditions and provides a spectrum of intensity versus energy levels.

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Shalini Dolai
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0% found this document useful (0 votes)
3 views1 page

Powder Sample Analysis Results

The document presents an analysis of a powder sample conducted by Mukesh on December 8, 2023. It includes detailed measurements of various components, with SiO2 being the most prevalent at 57.5 mass%, followed by CaO and Al2O3. Additionally, the document outlines the measurement conditions and provides a spectrum of intensity versus energy levels.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result

Sample Information
Sample name 7
File name 7
Application Powder
Date 08-12-2023 19:07
Analyzed by MUKESH
Counts 1
Comment Powder

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 30 6.8
Mid-Z C 35.0 342 1.6 30 27.8
Low-Z Open 6.5 150 1.6 30 37.5

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 SiO2 57.5 mass% 0.0845 0.0074 0.0223
2 CaO 22.8 mass% 0.0774 0.0180 0.0540
3 Al2O3 8.90 mass% 0.0591 0.0373 0.112
4 Na2O 5.08 mass% 0.518 1.14 3.43
5 Fe2O3 2.30 mass% 0.0080 0.0018 0.0053
6 MgO 1.25 mass% 0.0981 0.243 0.729
7 SO3 1.22 mass% 0.0073 0.0059 0.0177
8 TiO2 0.666 mass% 0.0128 0.0153 0.0459
9 K2O 0.255 mass% 0.0138 0.0283 0.0850
10 MnO 0.0253 mass% 0.0013 0.0027 0.0080
11 Cr2O3 0.0147 mass% 0.0018 0.0045 0.0134
12 SrO 0.0147 mass% 0.0001 <0.0001 0.0002
13 ZrO2 0.0130 mass% 0.0004 0.0003 0.0009
14 ZnO 0.0076 mass% 0.0002 0.0003 0.0010
15 NiO 0.0060 mass% 0.0003 0.0007 0.0020
16 CuO 0.0039 mass% 0.0002 0.0005 0.0015
17 Y2O3 0.0016 mass% <0.0001 0.0001 0.0003
18 Rb2O 0.0009 mass% <0.0001 <0.0001 0.0002
19 PbO 0.0007 mass% 0.0001 0.0003 0.0009
20 As2O3 0.0003 mass% <0.0001 0.0002 0.0005

Spectrum
cps/μA
X 50 X 3.0 X 0.20
1.0
Tm-Mα
Dy-Mα
Mg-Kα
Yb-Mα

Pb-Mα

Pm-Lα
Mn-Kα
Tb-Mα
Ta-Mα

Tm-Lα

Ga-Kα
Na-Kα

Ca-Kα

Co-Kα

Cu-Kα

Rb-Kα

Cd-Kα
Ag-Kα
Sn-Kα
Sb-Kα
Ba-Kα
Rb-Lα

Sc-Kα

Fe-Kα

Zn-Kα

As-Kα

Te-Kα
Dy-Lα
Sb-Lα
Ba-Lα

Yb-Lα

Pb-Lα
Zn-Lα

Te-Lα

Cr-Kα
Tb-Lα

Ta-Lα

Br-Kα

Sr-Kα
Cl-Kα

Ni-Kα

Zr-Kα
Zr-Kα
Br-Lα
Al-Kα
Si-Kα

Er-Lα
Ti-Kα
Ir-Mα
P-Kα
S-Kα

K-Kα

V-Kα

Y-Kα

Y-Kα
Y-Lα

Ir-Lα

I-Kα
I-Lα

0.8
Fe-Kα-ESC

0.6
Intensity

Pm-Lβ1

Tm-Lβ1
Tm-Lβ3
Tm-Lβ2
Tm-Lγ1
Tm-Lγ2

Cd-Kα2
Ca-Kβ1

Co-Kβ1

Ag-Kα2
Sn-Kα2
Sb-Kα2
Ba-Kα2
Sn-Kβ1

Ba-Kβ1
Ba-Kβ2
Te-Kα2
Rb-Lβ1
Rb-Lβ3

Sc-Kβ1

Fe-Kβ1

Zn-Kβ1
Rb-Lγ2

Dy-Lβ4
Dy-Lβ1
Dy-Lβ3
Dy-Lβ2
Sb-Lβ1
Sb-Lβ2
Ba-Lβ1
Ba-Lβ3
Ba-Lβ2

Yb-Lβ1

Pb-Lβ1
Pb-Lβ2
Dy-Lγ5
Dy-Lγ1
Dy-Lγ2
Dy-Lγ4
Sb-Lγ1
Sb-Lγ2
Ba-Lγ1
Ba-Lγ2
Te-Lβ1
Te-Lβ3
Te-Lβ2

Tb-Lβ1
Tb-Lβ2

Ta-Lβ1
Tm-Mβ

Te-Lγ1
Te-Lγ2

Tb-Lγ1
Tb-Lγ2

Sr-Kβ1
Zr-Kβ1
Br-Lβ1
Br-Lβ3
Si-Kβ1

Er-Lβ1
Er-Lβ2
Er-Lγ1
Er-Lγ2
Ti-Kβ1
Dy-Mβ
Yb-Mβ

Pb-Mβ
Tb-Mβ

Ta-Mβ
Ta-Mγ

S-Kβ1

V-Kβ1
Rb-Lη
Y-Lβ1

Ir-Lβ1
Br-Lη

I-Kα2
Rb-Ll

Ir-Mβ

Dy-Ll
Sb-Ll

I-Lβ1
I-Lβ2
Te-Ll

Tb-Ll
I-Lγ1
Br-Ll

Er-Ll
I-Ll

0.4

0.2

0.0
1.0 1.5 2.0 2.5 4 6 8 10 12 14 20 30 40
Low-Z Mid-Z High-Z keV

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