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Powder Sample Analysis Results

The document presents an analysis of a powder sample conducted by Mukesh on December 8, 2023, detailing the measured conditions and results. It lists the composition of the sample, including percentages of various components such as SiO2 and CaO, along with their statistical errors. Additionally, it includes a spectrum analysis showing intensity values across different energy levels.

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Shalini Dolai
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0% found this document useful (0 votes)
3 views1 page

Powder Sample Analysis Results

The document presents an analysis of a powder sample conducted by Mukesh on December 8, 2023, detailing the measured conditions and results. It lists the composition of the sample, including percentages of various components such as SiO2 and CaO, along with their statistical errors. Additionally, it includes a spectrum analysis showing intensity values across different energy levels.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result

Sample Information
Sample name 4
File name 4
Application Powder
Date 08-12-2023 18:53
Analyzed by MUKESH
Counts 1
Comment Powder

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 30 5.8
Mid-Z C 35.0 342 1.6 30 27.6
Low-Z Open 6.5 146 1.6 30 37.6

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 SiO2 49.7 mass% 0.0862 0.0094 0.0282
2 CaO 26.2 mass% 0.0861 0.0189 0.0568
3 Al2O3 14.2 mass% 0.0794 0.0400 0.120
4 SO3 3.26 mass% 0.0123 0.0050 0.0150
5 Fe2O3 2.84 mass% 0.0093 0.0019 0.0057
6 MgO 2.25 mass% 0.124 0.284 0.851
7 TiO2 0.792 mass% 0.0144 0.0168 0.0504
8 K2O 0.637 mass% 0.0190 0.0294 0.0881
9 V2O5 0.0468 mass% 0.0054 0.0142 0.0426
10 MnO 0.0358 mass% 0.0016 0.0029 0.0087
11 SrO 0.0242 mass% 0.0002 <0.0001 0.0003
12 ZrO2 0.0233 mass% 0.0005 0.0004 0.0011
13 ZnO 0.0133 mass% 0.0003 0.0004 0.0011
14 NiO 0.0084 mass% 0.0004 0.0007 0.0022
15 CuO 0.0058 mass% 0.0003 0.0005 0.0016
16 Rb2O 0.0028 mass% <0.0001 <0.0001 0.0003
17 Y2O3 0.0026 mass% <0.0001 0.0001 0.0004
18 PbO 0.0020 mass% 0.0001 0.0003 0.0010
19 As2O3 0.0003 mass% <0.0001 0.0002 0.0007

Spectrum
cps/μA
X 40 X 3.0 X 0.20
1.0
Tm-Mα
Dy-Mα
Mg-Kα
Yb-Mα

Pm-Lα
Mn-Kα
Tb-Mα
Ta-Mα

Tm-Lα

Ga-Kα
Ca-Kα

Co-Kα

Cu-Kα

Rb-Kα

Nb-Kα
Ag-Kα
Sn-Kα
Sb-Kα
Ba-Kα
Rb-Lα

Sc-Kα

Fe-Kα

Zn-Kα

As-Kα

Te-Kα
Dy-Lα
Sb-Lα
Ba-Lα

Yb-Lα

Pb-Lα
Te-Lα

Cr-Kα
Tb-Lα

Ta-Lα

Br-Kα

Sr-Kα
Cl-Kα

Ni-Kα

Zr-Kα
Zr-Kα
Br-Lα
Al-Kα
Si-Kα

Er-Lα
Ti-Kα
Ir-Mα
P-Kα
S-Kα

K-Kα

V-Kα

Y-Kα

Y-Kα
Y-Lα

Ir-Lα

0.8
Fe-Kα-ESC

0.6
Intensity

Pm-Lβ1

Tm-Lβ1
Tm-Lβ3
Tm-Lβ2
Tm-Lγ1
Tm-Lγ2
Ca-Kβ1

Co-Kβ1

Rb-Kβ1

Ag-Kα2
Sn-Kα2
Sb-Kα2
Ba-Kα2
Sn-Kβ1

Ba-Kβ1
Te-Kα2
Rb-Lβ1
Rb-Lβ3

Sc-Kβ1

Fe-Kβ1

Zn-Kβ1

As-Kβ1
Rb-Lγ2

Dy-Lβ4
Dy-Lβ1
Dy-Lβ3
Dy-Lβ2
Sb-Lβ1
Sb-Lβ2
Ba-Lβ1
Ba-Lβ3
Ba-Lβ2

Yb-Lβ1

Pb-Lβ1
Pb-Lβ2
Dy-Lγ5
Dy-Lγ1
Dy-Lγ2
Dy-Lγ4
Sb-Lγ1

Ba-Lγ1
Ba-Lγ2
Te-Lβ1
Te-Lβ3
Te-Lβ2

Tb-Lβ1
Tb-Lβ2

Ta-Lβ1
Tm-Mβ

Te-Lγ1
Te-Lγ2

Tb-Lγ1
Tb-Lγ2

Sr-Kβ1
Ni-Kβ1

Zr-Kβ1
Br-Lβ1
Br-Lβ3
Si-Kβ1

Er-Lβ1
Er-Lβ3
Er-Lβ2
Er-Lγ1
Er-Lγ2
Ti-Kβ1
Dy-Mβ
Yb-Mβ
Tb-Mβ

Ta-Mβ
Ta-Mγ

S-Kβ1

V-Kβ1
Rb-Lη
Y-Lβ1

Ir-Lβ1
Br-Lη
Rb-Ll

Ir-Mβ

Dy-Ll
Sb-Ll

Pb-Ll
Te-Ll

Tb-Ll

Ta-Ll
Br-Ll

Er-Ll

0.4

0.2

0.0
1.0 1.5 2.0 2.5 4 6 8 10 12 14 20 30 40
Low-Z Mid-Z High-Z keV

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