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Powder Analysis Results Summary

The document presents the analyzed results of a sample identified as 'Powder_A' conducted by Mukesh on December 8, 2023. It details the composition of the sample, listing various components and their respective mass percentages, with Calcium Oxide (CaO) being the most abundant at 47.3%. Additionally, measurement conditions and statistical data are provided, including limits of detection and quantification for each component.

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Shalini Dolai
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0% found this document useful (0 votes)
21 views2 pages

Powder Analysis Results Summary

The document presents the analyzed results of a sample identified as 'Powder_A' conducted by Mukesh on December 8, 2023. It details the composition of the sample, listing various components and their respective mass percentages, with Calcium Oxide (CaO) being the most abundant at 47.3%. Additionally, measurement conditions and statistical data are provided, including limits of detection and quantification for each component.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result Page 1/2

Sample Information
Sample name 2
File name 2
Application Powder_A
Date 08-12-2023 18:43
Analyzed by MUKESH
Counts 1
Comment FP

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 50 6.6
Mid-Z C 35.0 342 1.6 50 28.5
Low-Z Open 6.5 123 1.6 50 37.2

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 CaO 47.3 mass% 0.0827 0.0130 0.0390
2 SiO2 19.5 mass% 0.0479 0.0084 0.0253
3 MgO 13.9 mass% 0.196 0.272 0.815
4 Na2O 9.65 mass% 0.577 1.12 3.35
5 Al2O3 4.73 mass% 0.0440 0.0369 0.111
6 K2O 2.53 mass% 0.0241 0.0204 0.0613
7 Fe2O3 1.49 mass% 0.0059 0.0017 0.0052
8 SO3 0.491 mass% 0.0040 0.0053 0.0160
9 TiO2 0.190 mass% 0.0073 0.0137 0.0411
10 SrO 0.127 mass% 0.0003 <0.0001 0.0003
11 MnO 0.0317 mass% 0.0014 0.0027 0.0080
12 ZnO 0.0215 mass% 0.0003 0.0003 0.0010
13 ZrO2 0.0192 mass% 0.0004 0.0004 0.0011
14 BaO 0.0116 mass% 0.0004 0.0010 0.0030
15 NiO 0.0091 mass% 0.0004 0.0008 0.0023
16 V2O5 0.0068 mass% 0.0034 0.0099 0.0296
17 Rb2O 0.0067 mass% <0.0001 <0.0001 0.0003
18 Cr2O3 0.0050 mass% 0.0016 0.0044 0.0131
19 CuO 0.0040 mass% 0.0002 0.0005 0.0015
20 Y2O3 0.0015 mass% <0.0001 0.0001 0.0004
21 Nb2O5 0.0007 mass% 0.0001 0.0003 0.0010
22 PbO 0.0005 mass% 0.0001 0.0003 0.0009
23 As2O3 <0.0001 mass% <0.0001 0.0002 0.0005
Intensity

Date

Counts

cps/μA

0.0
0.2
0.4
0.6
0.8
1.0
Comment
File name

Spectrum
Application

Analyzed by
Sample name
Zn-Lα
Na-Kα
Mg-Kα
Al-Kα
Si-Kβ1 Si-Kα

1
2
2

X 20
Analyzed result
Sample Information

Low-Z
P-Kα

FP
S-Kα
S-Kβ1

1.0 1.5 2.0 2.5


Cl-Kα MUKESH
Powder_A

Sb-Ll
U-Mβ U-Mα
K-Kα
Sb-Lα
Ca-Kα
Sb-Lβ1

4
Sb-Lβ3
Ca-Kβ1
Sb-Lβ2
08-12-2023 18:43

Sb-Lγ1 Ba-Lα
Ti-Kα
Sb-Lγ2
Fe-Kα-ESC
Ba-Lβ1
Ti-Kβ1
Ba-Lβ2 V-Kα
Cr-Kα

6
Mn-Kα
Fe-Kα
Fe-Kβ1
Ca-Kα-Ca-Kα-SUM
Ni-Kα

8
Ni-Kβ1 Cu-Kα
Zn-Kα
Zn-Kβ1
X 5.0

Mid-Z
10
As-Kα
Pb-Lα

12
Pb-Lβ1
Pb-Lβ2
Rb-Kα
U-Lα

14
Sr-Kα
Rb-Kβ1 Y-Kα
Sr-Kβ1 Zr-Kα
Y-Kα
Zr-Kα
Nb-Kα
20

Ag-Kα2 Ag-Kα
Sn-Kα2
Sb-Kα2 Sn-Kα
Page 2/2

Sb-Kα
Sn-Kβ1
30

Ba-Kα2 Ba-Kα
High-Z
X 0.070

40
keV

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