Scribd
Upload
15 views1 page

Powder Analysis Results - August 2023

The document presents an analysis of a sample identified as '1', processed by Mukesh on December 8, 2023, using the FP method. The results indicate the composition of the sample, with key components including CaO (57.1 mass%), SiO2 (21.2 mass%), and MgO (11.6 mass%). Additionally, the document includes measurement conditions and a spectrum analysis of various elements.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
15 views1 page

Powder Analysis Results - August 2023

The document presents an analysis of a sample identified as '1', processed by Mukesh on December 8, 2023, using the FP method. The results indicate the composition of the sample, with key components including CaO (57.1 mass%), SiO2 (21.2 mass%), and MgO (11.6 mass%). Additionally, the document includes measurement conditions and a spectrum analysis of various elements.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result

Sample Information
Sample name 1
File name 1
Application Powder_A
Date 08-12-2023 18:37
Analyzed by MUKESH
Counts 1
Comment FP

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 50 6.3
Mid-Z C 35.0 342 1.6 50 27.5
Low-Z Open 6.5 126 1.6 50 37.3

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 CaO 57.1 mass% 0.103 0.0150 0.0449
2 SiO2 21.2 mass% 0.0552 0.0106 0.0317
3 MgO 11.6 mass% 0.219 0.365 1.10
4 Al2O3 5.22 mass% 0.0511 0.0419 0.126
5 K2O 2.35 mass% 0.0250 0.0210 0.0631
6 Fe2O3 1.59 mass% 0.0066 0.0020 0.0061
7 SO3 0.574 mass% 0.0047 0.0065 0.0194
8 TiO2 0.191 mass% 0.0081 0.0156 0.0469
9 SrO 0.168 mass% 0.0004 <0.0001 0.0003
10 MnO 0.0300 mass% 0.0015 0.0031 0.0093
11 ZrO2 0.0240 mass% 0.0005 0.0004 0.0012
12 NiO 0.0090 mass% 0.0004 0.0009 0.0027
13 Cr2O3 0.0085 mass% 0.0019 0.0051 0.0153
14 ZnO 0.0068 mass% 0.0002 0.0004 0.0012
15 Rb2O 0.0056 mass% <0.0001 0.0001 0.0003
16 CuO 0.0044 mass% 0.0003 0.0006 0.0017
17 Y2O3 0.0020 mass% <0.0001 0.0001 0.0004

Spectrum
cps/μA
Ｘ 10 Ｘ 5.0 Ｘ 0.070
1.0
Mg-Kα

Mn-Kα
Ca-Kα

Cu-Kα

Rb-Kα
Fe-Kα

Zn-Kα
Cr-Kα

Ca-Kα-Ca-Kα-SUM

Sr-Kα
Ni-Kα

Zr-Kα
Zr-Kα
Al-Kα
Si-Kα

Fe-Kα-ESC Ti-Kα
S-Kα

K-Kα

Y-Kα

Y-Kα

0.8

0.6
Intensity

Ca-Kβ1

Rb-Kβ1
Fe-Kβ1

Zn-Kβ1

Sr-Kβ1
Ni-Kβ1

Zr-Kβ1
Si-Kβ1

Ti-Kβ1
S-Kβ1

0.4

0.2

0.0
1.0 1.5 2.0 2.5 4 6 8 10 12 14 20 30 40
Low-Z Mid-Z High-Z keV

You might also like