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Powder Sample Analysis Results

The document presents the analyzed results of a powder sample, including detailed measurements of various components and their respective mass percentages. Key components identified include CaO (51.1%), SiO2 (22.8%), and MgO (15.6%). The analysis was conducted by Mukesh on December 8, 2023, under specific measurement conditions using a helium atmosphere.

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Shalini Dolai
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0% found this document useful (0 votes)
21 views1 page

Powder Sample Analysis Results

The document presents the analyzed results of a powder sample, including detailed measurements of various components and their respective mass percentages. Key components identified include CaO (51.1%), SiO2 (22.8%), and MgO (15.6%). The analysis was conducted by Mukesh on December 8, 2023, under specific measurement conditions using a helium atmosphere.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result

Sample Information
Sample name 3
File name 3
Application Powder
Date 08-12-2023 18:49
Analyzed by MUKESH
Counts 1
Comment Powder

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 30 6.4
Mid-Z C 35.0 342 1.6 30 27.2
Low-Z Open 6.5 134 1.6 30 37.4

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 CaO 51.1 mass% 0.125 0.0191 0.0573
2 SiO2 22.8 mass% 0.0709 0.0129 0.0386
3 MgO 15.6 mass% 0.288 0.407 1.22
4 Al2O3 5.57 mass% 0.0650 0.0504 0.151
5 K2O 1.96 mass% 0.0298 0.0269 0.0806
6 Fe2O3 1.55 mass% 0.0082 0.0026 0.0078
7 SO3 1.01 mass% 0.0075 0.0077 0.0230
8 TiO2 0.182 mass% 0.0104 0.0211 0.0634
9 SrO 0.128 mass% 0.0004 0.0001 0.0003
10 MnO 0.0332 mass% 0.0019 0.0036 0.0109
11 ZrO2 0.0195 mass% 0.0006 0.0005 0.0014
12 NiO 0.0095 mass% 0.0005 0.0011 0.0032
13 Cr2O3 0.0070 mass% 0.0022 0.0060 0.0181
14 ZnO 0.0058 mass% 0.0003 0.0005 0.0014
15 Rb2O 0.0053 mass% <0.0001 0.0001 0.0004
16 CuO 0.0039 mass% 0.0003 0.0007 0.0020
17 Y2O3 0.0017 mass% <0.0001 0.0002 0.0005
18 As2O3 0.0002 mass% <0.0001 0.0002 0.0007

Spectrum
cps/μA
X 20 X 5.0 X 0.070
1.0
Tm-Mα
Dy-Mα
Mg-Kα
Yb-Mα

Mn-Kα
Tb-Mα
Ta-Mα

Tm-Lα

Ga-Kα
Ca-Kα

Co-Kα

Cu-Kα

Rb-Kα

Ag-Kα
Sn-Kα
Sb-Kα
Ba-Kα
Rb-Lα

Sc-Kα

Fe-Kα

Zn-Kα

As-Kα

Te-Kα
Dy-Lα
Sb-Lα
Ba-Lα

Yb-Lα
Te-Lα

Cr-Kα
Tb-Lα

Ta-Lα
Ca-Kα-Ca-Kα-SUM

Sr-Kα
Cl-Kα

Ni-Kα

Zr-Kα
Zr-Kα
Al-Kα
Si-Kα

Er-Lα

Hf-Lα
Ti-Kα
Ir-Mα
P-Kα
S-Kα

K-Kα

V-Kα

Y-Kα

Y-Kα
Y-Lα

Ir-Lα

I-Kα
I-Lα

0.8
Fe-Kα-ESC

0.6
Intensity

Tm-Lβ1
Tm-Lβ2
Tm-Lγ1
Tm-Lγ2
Ca-Kβ1

Co-Kβ1

Cu-Kβ1

Rb-Kβ1

Ag-Kα2
Sn-Kα2
Sb-Kα2
Ba-Kα2
Sn-Kβ1
Te-Kα2
Rb-Lβ1
Rb-Lβ3

Sc-Kβ1

Fe-Kβ1

Zn-Kβ1
Rb-Lγ2

Dy-Lβ4
Dy-Lβ1
Dy-Lβ3
Dy-Lβ2
Sb-Lβ1
Sb-Lβ3
Sb-Lβ2
Ba-Lβ1

Yb-Lβ1
Yb-Lβ2
Dy-Lγ1
Dy-Lγ2
Dy-Lγ4
Sb-Lγ1
Sb-Lγ2

Yb-Lγ1
Te-Lβ1
Te-Lβ3
Te-Lβ2

Tb-Lβ1
Tb-Lβ2

Ta-Lβ1
Ta-Lβ2
Tm-Mβ

Te-Lγ1
Te-Lγ2

Tb-Lγ1

Sr-Kβ1
Zr-Kβ1
Si-Kβ1

Er-Lβ1
Er-Lβ2
Hf-Lβ1
Er-Lγ1
Er-Lγ2
Ti-Kβ1
Dy-Mβ
Yb-Mβ
Tb-Mβ

Ta-Mβ
Tb-Mγ

Ta-Mγ

S-Kβ1
Rb-Lη
Y-Lβ1

Ir-Lβ1

I-Kα2
Rb-Ll

Ir-Mβ

Dy-Ll
Sb-Ll

I-Lβ1
I-Lβ2
Te-Ll

Tb-Ll
I-Lγ1
I-Lγ2

Er-Ll
I-Ll

0.4

0.2

0.0
1.0 1.5 2.0 2.5 4 6 8 10 12 14 20 30 40
Low-Z Mid-Z High-Z keV

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