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Powder Sample Analysis Results

The document presents an analysis of a powder sample conducted by Mukesh on December 8, 2023, detailing the sample's composition and measurement conditions. The results indicate the mass percentages of various components, with SiO2 and CaO being the most abundant. Additionally, the document includes a spectrum analysis showcasing the intensity of various elements across different energy levels.

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Shalini Dolai
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0% found this document useful (0 votes)
3 views1 page

Powder Sample Analysis Results

The document presents an analysis of a powder sample conducted by Mukesh on December 8, 2023, detailing the sample's composition and measurement conditions. The results indicate the mass percentages of various components, with SiO2 and CaO being the most abundant. Additionally, the document includes a spectrum analysis showcasing the intensity of various elements across different energy levels.

Uploaded by

Shalini Dolai
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Analyzed result

Sample Information
Sample name 5
File name 5
Application Powder
Date 08-12-2023 18:58
Analyzed by MUKESH
Counts 1
Comment Powder

Meas. cond.
Diaphragm DE-10mm Atmosphere Helium Sample spin None Meas. order optimization Yes
Condition name Primary filter Tube voltage(kV) Tube current(μA) ST(μsec) Meas. time(sec) Dead time(%)
High-Z F 60.0 200 1.6 30 5.5
Mid-Z C 35.0 342 1.6 30 25.7
Low-Z Open 6.5 175 1.6 30 37.5

Analyzed result(FP method)


No. Component Result Unit Stat. Err. LLD LLQ Element line Intensity(cps/μA)
1 SiO2 55.3 mass% 0.0955 0.0103 0.0309
2 CaO 27.1 mass% 0.0967 0.0212 0.0635
3 Al2O3 10.3 mass% 0.0734 0.0469 0.141
4 Fe2O3 2.54 mass% 0.0091 0.0019 0.0058
5 MgO 1.78 mass% 0.140 0.350 1.05
6 SO3 1.74 mass% 0.0091 0.0068 0.0205
7 TiO2 0.603 mass% 0.0136 0.0183 0.0549
8 K2O 0.524 mass% 0.0195 0.0335 0.100
9 MnO 0.0285 mass% 0.0015 0.0029 0.0088
10 SrO 0.0196 mass% 0.0001 <0.0001 0.0003
11 ZrO2 0.0176 mass% 0.0005 0.0003 0.0010
12 Cr2O3 0.0149 mass% 0.0020 0.0051 0.0152
13 NiO 0.0079 mass% 0.0004 0.0008 0.0023
14 ZnO 0.0050 mass% 0.0002 0.0004 0.0011
15 CuO 0.0046 mass% 0.0003 0.0005 0.0016
16 Y2O3 0.0023 mass% <0.0001 0.0001 0.0004
17 Rb2O 0.0018 mass% <0.0001 <0.0001 0.0003
18 PbO 0.0011 mass% 0.0001 0.0003 0.0010
19 As2O3 0.0004 mass% <0.0001 0.0002 0.0007

Spectrum
cps/μA
X 30 X 3.0 X 0.20
1.0
Tm-Mα
Dy-Mα
Mg-Kα
Yb-Mα

Pm-Lα
Mn-Kα
Tb-Mα
Ta-Mα

Tm-Lα

Ga-Kα
Ca-Kα

Co-Kα

Cu-Kα

Rb-Kα

Nb-Kα

Nd-Kα
Ag-Kα
Sn-Kα
Sb-Kα
Ba-Kα
Rb-Lα

Sc-Kα

Fe-Kα

Zn-Kα

As-Kα

Te-Kα
Dy-Lα
Sb-Lα
Ba-Lα

Yb-Lα

Pb-Lα
Te-Lα

Cr-Kα
Tb-Lα

Ta-Lα

Br-Kα

Sr-Kα
Cl-Kα

Ni-Kα

Zr-Kα
Zr-Kα
Br-Lα
Al-Kα
Si-Kα

Er-Lα
Ti-Kα
Ir-Mα
P-Kα
S-Kα

K-Kα

V-Kα

Y-Kα

Y-Kα
Y-Lα

Ir-Lα

I-Kα
I-Lα

0.8
Fe-Kα-ESC

0.6
Intensity

Pm-Lβ1

Tm-Lβ1
Tm-Lβ3
Tm-Lβ2
Tm-Lγ1
Tm-Lγ2
Ca-Kβ1

Co-Kβ1

Ag-Kα2
Sn-Kα2
Sb-Kα2
Ba-Kα2
Sn-Kβ1

Ba-Kβ1
Ba-Kβ2
Te-Kα2
Rb-Lβ1
Rb-Lβ3

Sc-Kβ1

Fe-Kβ1

Zn-Kβ1

As-Kβ1
Rb-Lγ2

Dy-Lβ4
Dy-Lβ1
Dy-Lβ3
Dy-Lβ2
Sb-Lβ1
Sb-Lβ2
Ba-Lβ1
Ba-Lβ3
Ba-Lβ2

Yb-Lβ1

Pb-Lβ1
Pb-Lβ2
Dy-Lγ5
Dy-Lγ1
Dy-Lγ2
Dy-Lγ4
Sb-Lγ1

Ba-Lγ1

Yb-Lγ1
Te-Lβ1
Te-Lβ3
Te-Lβ2

Tb-Lβ1
Tb-Lβ2

Ta-Lβ1
Tm-Mβ

Te-Lγ1
Te-Lγ2

Tb-Lγ1
Tb-Lγ2

Sr-Kβ1
Ni-Kβ1

Zr-Kβ1
Br-Lβ1
Si-Kβ1

Er-Lβ1
Er-Lβ2
Er-Lγ1
Er-Lγ2
Ti-Kβ1
Dy-Mβ
Yb-Mβ
Tb-Mβ

Ta-Mβ
Ta-Mγ

S-Kβ1

V-Kβ1
Rb-Lη
Y-Lβ1

Ir-Lβ1
Br-Lη

I-Kα2
Rb-Ll

Ir-Mβ

Dy-Ll
Sb-Ll

Pb-Ll
I-Lβ1
I-Lβ2
Te-Ll

Tb-Ll
I-Lγ1
Br-Ll

Er-Ll
I-Ll

0.4

0.2

0.0
1.0 1.5 2.0 2.5 4 6 8 10 12 14 20 30 40
Low-Z Mid-Z High-Z keV

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