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General Unit 03

The document discusses various aspects of mass spectrometry, including sample preparation, peak identification, and data interpretation. It emphasizes the importance of relative abundance and stability of peaks in analyzing compounds. Additionally, it covers methodologies for analyzing alkanes and other organic compounds through spectrometric techniques.

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pittalaaravind08
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0% found this document useful (0 votes)
5 views36 pages

General Unit 03

The document discusses various aspects of mass spectrometry, including sample preparation, peak identification, and data interpretation. It emphasizes the importance of relative abundance and stability of peaks in analyzing compounds. Additionally, it covers methodologies for analyzing alkanes and other organic compounds through spectrometric techniques.

Uploaded by

pittalaaravind08
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF or read online on Scribd
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Hea lool oar prom fou XB wi rns Rule Sn 08 PUG) fle oven Tr ow oy an elumurd » els ob! vel celet no veliog 3 wager oe nitregin = nn amass Wy en elt 4d) norbewsle Gntacn odd meee yy Al “aed ynwyl bre utlh add pro. of hovod nibe unas = af Bee morleale. cortatn eno) 4 auc po-od tibungers be art TaN Snr eal P| Limidediians = ells, ¢ AP) at cull pot seta oe sel CH. , 22 : gf & a4 ié/ = @) a ; Omi = 16 * nr read” =>. Beno rove ome Bn ame amt hoof mad opie ae- 1) | (EP ent’ ead my = 3 m/e=3lo >. dd “no-od nibiogen ce Sample” ‘maagh due) edd odd Aor vot amans wy aq. fly W- Cy“ AMy Hav 49 ly wile | whee » ME=6 m= lor Me abuve adel trilafn eon too! pichergers > He arabes rest oe even foro} MaHs +f. td a sl aed | | | 1 Oye tere i mh 150, \ mk 8 [> Pe chove Samp ‘rls = Ahowe L) Sangh § indials _grewnee of geo 6) evn real! Be tl eal be tla, i od roof iv! ’ angi zal sully = > tahith Aner 20 a abst shoul) be boob. sah Gin ata suerte ns 9 iy chonndishs fragt Jin grow spedbondy 4 Hye-cHar Hey -lly-CH sas Wy-CHyACHg-CH Ally ge oO Gn? ¢ Ly CHlg CH a bab (parm) ow , Shui Ae ci ellsctinl (CH : Mea , ro 3 ait Be aly CH Ch Re HP ee 5 ty My Mhebd 2 mbol5 Nay his ni M94 Be. Me yg the A rol} | gyal ff ete Las oe nlp 4n yay spucsoorcbey of oy ie ad fiw Beponattd ty cy wacky tha Sample pot Be 3 Coan hotron chain alkanes > i Foanchedl “autkarws bh ulation ey high brated chain Suldoad Peggle ep qt Gus — wleone > the-d@4 uc, we Lo Pycee- Ch cls f dus CAs, CH; oud gang Bh (hain 2 a nadical | iihomudick AlKams > Sry pent oa ube) poled agoatalin ! (Oe CleO- “C+ be ton” 3s" Yay ; } oe ' - iho butte fdbylan ise cation (il Bi ds] wc te: in yclo alkanes nw ok abty) gump as a nadiay ou dered Peagroiakin g og h2OQ-o chs, tls Joov : QO OT Cy — § +c43° | Alfons 2 jn alkuus pr homolysis Gx) abiylic Chowage Heed dova ‘on sewellicg spouts oe sf ain Sp clubs in Yh feel ob | F ieee 20%, 4 oul dort ra ; Cos rc er. “Hg ly 2 1 @ 4 Ay ic Calton, aHge-ch=CHe a 5 1 ahonds ; A ® ‘ clicty,icH=cHy oO HC Haag = —sthe-cll hh 7] * el og Iac=cu-Clh : ; » Auglic cakton | ibe ed geal (OD) jah be “me ag) max but) oe Réao = ar, | ag Cop Sic adduat liane _ cliente Rage cei ctenop hile Oe oe een 2 S yee coyclohemert dine bene © Sn 6 monbenecl Geli c cnseubiouabion ruated int din cenophile Cold Rebo ciel allen Spon sub lat allot Hes smalaucle mest oe onlato 6 manbewel yale canseitiowtion in nibuclits ally ruling “oodudi “are dunt rude tion: are — clienep bile tuwtrual Species > Th Followni ng ali the lanproinch’ perk do RDA “£0 0.0 Pou DOS Balin mata Miso tg OA- “aoew , porde oo» “oe te Co " . Oe fare by elk Ltd Vit 0 BA a ad “al woe fr bot eo BooUco-Ch! 2 rei —ay. i Cent ao oa an Hy Pe saa": CO-OL B hereby hiyhty gouddoned Pagraclako ‘in allyl aS At bys 4 = Lye 7 e - af 0 wedge cocn 2% pln, cHed — Hee =t" Sees ay i eo Hes cet ce = ag et 7 @ ge - CHa Cae 2S rye l cate ad eace dtl er mh pan ne ral esp an] Bo harap 3 Aahly chiro inis be drogen tion ns sp Damp tga gu aa era wees gc, a“ plein, LS x src, o yr C9) bax peak | hope Cy jaboolyss _ 2. » " eee Rk Ceay aR > rec O_enze. i G-CHs-R SP? ee ee Ba ay -Srety-R mh -9 Boxes otelah Gs bela R-Cu- a? soi R-Clly-CHly-0 TS ou, gucagl tustt on — gt hg- | Frhomalysis . 3B, RACH g 1 (ly OH - m/2=3!) m/re3l ds tthe fra puak of foviranss ae dm $= ka gdlodp? @,4 —_ ae, CHa Ley WH. ee Reciyrtl + MM © Rael, -CHo~ Wha pe? Ro |e bys P-cHs Hy =N ui? m/z =30 + of u bog of m/xeze 2 te haw peo! me Bebploaly Ari. af ano a | antyl hrengene G1) altey| coomalic Ip Jini ( bomylt op Ps fretoud 9 mun fethtn I cual i ya oe (oe pe, é. - He a e —_ (es ae | 5), 2 fi 30 a en ee “4 (Ho CAs, nts L Gy ty OG: {fFropeitiusy ~ Hoa 2 i Has Uy! | vy Ris af ®_, 1) | 0 eth Jo non altyleced onamaltc clon pactoredl Presale ( Box peat) + ne & |* FO O-O“ | on [yaa (bow quok) | oc ota? B= 5 ooy g é LO] VP oy [0] Oct melhor dporsent ! mn /pead oy) HU gol x @ gt a- fy Et A og 1G os . on [pat ‘neladdesty , hragnwalehon s= WA a je aba Galas “A C8" fa ee nt oa ue eer ae i Bee * Jha ue ea . eZ , ae ; 4 | b Ral} Spurioa ( 2 Amalulan fo | by I A . én yo) ost ZY ena seacical colion + & bow pork os) =) mp =e ihe 5B petinadion +> Arash ol i- oan jy 0 (reodalay dion! hy unsilotlion and doltownc! is Ca-CB Feemalysts tel radial LoHon ary selling spele om * alent : goodyeh ou. ind sll “Frogrtlation Some rant € A R @ - Ls, OR ° LA. Ll | Cnbengfe och aha poi Soo al te @& (at 0 AL 8 oH teen awyrs Aidala , : OLA, aed 2 A oeu. Nn Ee? 1 Be LN tl sop OH 6 & 8a le & ts || + A oP er —\p OH 8 ae ; LU ARAie D 1 7 n/a > shy T1= sop Ya mfp of trolulor aed ok (neleskn sgh) . on pombube oth o/eun root pool ah bbe smut trad aut toval ot da isi : 7 poot esint— - j a Tat af dn ‘dirty wa Did wh af anlinsity of 1 46 nef eopsnl to foo's ue Shout oe Paben tors of ainkinsihy ob pha neleudan ton 1 3) > fof Jirsiby ot) RA of (a/e=tod) = DY retog =100"¢- >'h of inkinsily Ga/ye tol] = Gy lod =s0'/. yo ulvaity (m/r-tor] = Yar iog =o’ D) om miroi50 = 257: 6 xtoy = word Lt mfpe 51 = 6% Bas nido = OWA mo meee ge 4 Yeo G |p ists a fof en quale Stip TM petshion: ef tae AB? Ws Seis yee/e RA a! o/- of acitie — [novod. 0's 74 RA ob iz no-od S's x0 R mor 04 “Ch = 1 zo cb babar” part tS gw abut fun Bx Cankons main ob alk tx tnalet of | Bes Songs FF boule = i: y pitedioo jot aloo 4s oo aa ote, unite 1 Oe = 8 : ; y | ad i776 , Su pt ae TN Mage ter a pd lo —? vt , \ ‘a \ &BY —>» \ : a? ) _3er > 1% See RN Cael ceubeb ional envsivany = 10Be © a = uoee 1 oBE=5 porsibh shbudbioe OD ALS TN, y , o Oped DBE=5 Tx Ty By Ba ye peoltla valbrt afirns Jo gfe roth eyie C! oundly si" altorn ' 4 Phono veil alins 30 th roid ea Hyp ge nmal trivalind cchrey gowenl in he roluale ey= ‘wy P. a= noob uso ds solnt abs Mn Wes sriocdbiule aye OS, Sey an Cs Hs N OBE= [s-%] +vo = loo8 1, 4) ~My = 5 iat ey G- 5), 43 /y. Bohubb. + (UNG | @ bOCl = p61 = CoJ+ | obe = +1, ® Gre DBE = 6- %) AGH | = (258) 10/4] = Yet wt / = a DeE= ay © Creo | 3 ppe -0-% 494 4) C$ 7 Neu OBe hy r 6 Cio Hr , yy, oBe = (10-Yy) VAC = 464] | @ Kei Bi <1 Oca [é oy | + “) Ocal ne 4y A () phere 4\ : Y, @G@ Hy 4] DBE = | e-F 4 yy te y+ af. a a x, + An ¢ 3, gui saline ee a H¢o: 4) @ Choo: ; f OBE 1y- 6 ¥ | hip $ = oe —> Aiwuent — 14/$)0 ame obser thon spook tH ood Halim = rust fey a ah Hop iL nisio ae font 1 nl iL garnodhS + lbxwd food Y= mul Fala wre ae a3 (mt) = a2 AW) : mt (ma) = 93083) ta (made WM (ois) se [Link] in He Geer) ds 2 Cen Uh tre aflainy 30 Gy oun so-0F beg oer “ak palualen ten “iy arb ss too, we Gill enhandes ‘be Hoy 10a ‘Hof Ra (oma = 92) = sp od R&C /e=33)= 237) A of RA&Cm/p=D4)= OB (00.5 oR sep Ui rune MS wy abuend Spb b ahone 43, loo =l00'7 ys 4 xloo = UrSahk ae of ohm | 1] Asieune falogea ynay dn abyad. } , $10 pb a he runt — (124 nv» of ‘cl aban | 2 ae eye! = 79a - = ayy 4 he ottoked dou! | Lb bud au H! Cont av grou PONT ¢ 1. mit ‘ued ane 36% (ike snort Hon Sangli mart) UC+ S = 50% : ume Lg a? UCER'O' = $Ox 1 Uck O= 64 vencieg ml = ja-fr+i6] = By & conbbluds 2 Beo-of H Jon a the above infoouralion Doak hand owen y= DBE = (-%A)* “i = (u-¥a)*! Boy ft) — Vy por bul Sudo Couette tH) “ey | (0) (cus? -a-ch} weg be Ha srotusdan formula Cy He @ ¥ Gy) v6(02) oot! (le) = $3 (0-564) mi® (m/z) = 88 (oor) &hp T3= / ee rt’ bs $6 Urn H rau lonlnin en OY) Beno nos O- es "7+ od RA (mhs=86) = qr l00 = (00% 0+ od RA Crnly= 89) = 0567 yio0 240 56% fod. Bee (anya 8%) = orauy dee wt vo = * fodmt) . Boas, do: of “C alone = 3% ial [stpm= * % Gaboy graak to Bh rode Ascent ne | Jre obyent Shp’ | 01S) 0 J abyend- Kovod fe ruat - (12% novod ‘pleatory) = 56~ liars ) = $6- 60 =~ 967 DP 5ct an= 39 > Ber S$ = 42 540 ? Br ao-FZ * > Beto = 2é gy ope= (5-'"%)t) = 4l, possi Subir bg Hat f toc —clls 6 os” (m= 93 = 56° tl Unig de Fy — 387. mi? (made a5— OE shiprs= Gm ra an aa add H MOY enlain eid onavat pe regees Styp~ 4 of BA tmafaras)= WA, xian (00% sh od Ba tmfa=9u)= 99% , x 100= 39°/ “fod RA (Ml r2 95)= Ol¥/, xloo= Bee Step Ws= eu *0 olin = +) of mt} ae tl Vel 3 umboy power Jo he aolenade SPE hk go Ja obi wool Wo = mut —[i2x novod ‘e! aber) wt Tr 437 (axs) = 93- 36 = ay } e SERENE a : Sack o= 59 WW act sa 6% 2 3c Liv= 050 “ay —3t+ als 68 Gwyn vpee =(3-% i454 ahrVatl = 4, Hac — a Cay Nha chins in scns spo ORS 5° Joniscrlion _ Pecknt — LT —— Banenis, pho [ beipion thre] ——Rerrricyece N- | alm bombcodment clean impnut Cc) feah CEABD | dumical ion silion x) Sums(serondoryy tors, Hud ionising Jeeh CEE a A ‘ae St Boone fonisa tion \ acon) ET ebabon ‘impok = - . adwantages $= ; eat ae Aishaiqwst ip ens Pu Samp’ ahi 6) lal in Solvent Le pouvic br memation” peaks porsih fo row Ms es Jndronalion “od he > Cina st tadntoj i Pavia of dos, chromahsyrep, 3 EL Myusy varlatil, Samples and uy is bop ualakl Compan ON geo bn 2 8 baheque Pod Gone! foo He Scum Cords nd Pre. ter “1000 troleenlery wees At!" > Tk lle al Te hal Seba (48 J rood bate fon Hom 0 hal) — e => e d > LP Leahniquee > negseirus skilled operafon Lhenteal amrisabion deahniquieys— (CT) tt Sunalifey of ven aa peatard gos, / “q' . 9 gos/ v ge / Gab 0 i Gul rt caith tte § it Gas at Simpl belek Et ae a of. G03 7 Sample morlouls Boa. subjedid to urbercmed cuith © with OL ort vba ob pagent son%ed ,Dye Jor Kaw (oblivion vith mek pe im ranged 0d give, 2 toy — ye hers male Covllivions ctthe hin nude Go Gate, (at ro” ral Ybor cou Gallid a3 “Buri tora! ve mot Grdlinsive uak Boat of thas totem, tons —5 Guisions $ abst . Hae beams wee. @ * hang, par, - 5 Seinclany fovy tac ACiy —o aif tHett me aly mv] te mi @i 7 (m4) bethattly Guo smolnh, Jn ma ci? 5 (etl) 4 Hy HCH ae a hha Glan 24 ly > ey atlanta + Qi —s [er soni] + talk | pkey ae WA 4+ tts —> ‘ah 6) onal outa cw Ott, dy ' | (nny | Geu. ork 6 bet | Wyto™ | t Cals —>] 6} clts oy > | otlty i | ou \ ous oil i fe a 0 cH i + oy ots a 4 Gelb, Lh Cho 4 = {mC Heuldan dan ia tron indunshve to cE aban cis” youdich Doe anally dednual ok de bam > cy inbhon Ge lahntony ok re a: 7 Demag ot Gamyoowl bol sui fable. Erle aethans % Th Cosryeunel joo cb fli <(v00 rmakicbaay exif oh mendedtion Bruny mmayy hab seen MoH dows snoik inbinhawe wilt Le Ms 2 SE A neopiud skilled operadores. pest lor Bombardment louhatqut CAB) = el —oxe—>ke wt, Ke > Kept puolialtd iy & see Mute 18 % qslov seunp ong ned rf oor - rele tots ae famelt pte) & wer Mol lade a % Sab pe adwansed Aonised — tabnigue jn 17088 spe wy Gath) = ths amthid ia sulle don in velabile taped => Aur do De erpurtinentel Shmplid andl ide ‘ahd Technique wo ae phe ‘mfod jhe amp duns, Subjted to Chou lgg_ rnbxitzunt ) Afi 2 arg oaBh Jeo... ena => Pe Sample cans collisions unt dest alam ubich ors atalaaking by relic anmay i" or he Commonly uyed_dat cting orm lita) xey (ae ED 7 el ct “abu bunhonclnvad: with the Zamgle F ry P dust enoifeulaer Len 2 : ho a FAB swithou! ix moe su abe han igh srodzudlan ovight 7500 —> stall pbs) etc i an nude ately low abo the Tid by Bt Tatas Oiradbanlage 5 = > Some tims eral Jap gud anes TE dntensi ty than fhe Veggrentedion ion Jion pal — ae _ Ceeondl clos HON oy und) oe ne ote si be. analy sect | ae A Jin a Compl oleh Samy le => Sime ina biuenenl wae an ae pend ‘bao ¢ a the positive C.S™) sve Co) dy (yo ea on a Sample Sardout fo gurouth jors tal cov Mamta) ints ce OD Spebromdlin ag ah Stoke _poctialial Apel oredhoned ao oy secondong Los D sinrilon Lankiqnae , @ beam at high oped -poabaS allem SF aval goin of Set sums $= => Pe intnedtn of primoasiton dream sith sho dep fy sdrently ergy Ae eige teary ehnali yo de pm eam ia Cowpoued ob ty jh Pha eaten Gomecrr psernite 4 we tons pepo, Aroan od VE" ons exahion of “Hver “Los altho nest cons one aro gomeced from Las Sample by syatzadion od fle gowrmany ream nel Ble Sunyle cdo Ol) dee [ate ah of Te cos onised Dae coe then atcelenaled! docwsed ancl analysed ey rm ano’ speck nin Advantages 5 = uw used thot hos bw apgbieabons fn i “geasience” LOA LOE. ‘(mati assished Laver pisorplion Jorisalion), - Bn Loren dlsoaphon melhod ux Sample cases Subjeded ae igh pon’ taser padts Gerhonons) 9 > chan enn Bh Sample as “port-volli Pun Huck Indirectly —danised! sey Laven disooylion method’ = inliee “pleama_dlsonplion Pubaiqet aki Ba Sample tay tng on bo andl leh nag in He Saph a auanati muthowl f FAB are) hor cise mh tebe’ qs davisebon Hedria 2 vou mash hlphel an Jo daehin of “ara kogmunion(Cadione_ ov) ob roniacchon’ one Used Un be Foadicnss SF vot us by cally ed tales eee ~~ | | Gos ¢ hromadoprplay 1 A 93 dlovindlgvephy dros Jonl TR Te Specbudeoyy et [Doc au oucllert ] methowls ub * ot , “ Yowen f Same eluant + eed ee ida arather cos Hodive abnaninels, eran, MHS gpecbornatn oT oe akon avs! ual oud " sbinclel with Pay, Jot > 1 could yt word susorbe leas _pounsible > Te anknfacng of bo inghiamunts 3 sie Common. aru! populan ncith Chemis ‘ ae han > A aol jy nemond by i PL qunakin anu! shay inc 1 ; a, ch ete in gai opty Bap ony ont, gjeted fe” dhubon Hifien Z > dlabion Js ceed in foepoadion ato mon by thangs od Severtal races eee ( Food ma) anol (euecloy ba eredicine. aval ty gti . Lems:= ll Hil iben Halegial sen ih oft re a ens DR tsdel Combinalion ac mow y 1. ' TA chy is dildad some trotk taal om & persng_? mats Wa dite Covtho cf Hel) a om . Ay vt a A C= OL ac. 8 Roe 3 ay Ly cf Y SAY (mn-A8) Od A, qi AAw er, ACG OY = KE Cr Se ig 7 EL ul 2 H _ : oe a eed ih stl wile aver hi ah ot er . a . v or ou G Lo a ek Cll 4. anorectic tellin apyooxtmadbe tondition srweduad ¥A backs / ealed ortho eddectt q 1 vocoatins dhe by spas Con ey a Wot c a ou a ace & bao, on ee oc 2 ar rm ane q OH et en" —# |< 7 Wu, — toew won Ly ~ v : a aa Cc ne ‘ ae y os Te 7% aT ~\ oa Io van oO joew (Co) nadie! | sxthy o-eMled sunoral_agratlh mee He —

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