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Mechanical Testing of Composite Materials

The document outlines practical instructions for two experiments in a Material Science and Engineering Laboratory course. The first experiment focuses on mechanical testing of composite materials using a 3-point bend test to evaluate properties like tensile strength and Young's modulus. The second experiment involves fabricating composite materials using a hand-layup technique, emphasizing the selection of appropriate polymers and fibers, and the advantages of composite materials in various industries.
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0% found this document useful (0 votes)
21 views4 pages

Mechanical Testing of Composite Materials

The document outlines practical instructions for two experiments in a Material Science and Engineering Laboratory course. The first experiment focuses on mechanical testing of composite materials using a 3-point bend test to evaluate properties like tensile strength and Young's modulus. The second experiment involves fabricating composite materials using a hand-layup technique, emphasizing the selection of appropriate polymers and fibers, and the advantages of composite materials in various industries.
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Practical-Instruction Sheet

Course: Material Science and Engineering Laboratory


Course code: AM13203
Department of Applied Mechanics

Experiment: Mechanical testing of composite materials made by hand-layup technique in


laboratory.
Objective:
> Learming to characterize mechanically the composite material in the laboratory.
> Understanding of the standards to characterize the composites.
> Use of characterization facility.
To investigate the mechanical properties of composites.
> Learming of selection of the composite for real application.
Equipment:
Tensometer, Specimen as per standard, 3 point bend set-up, dial gauge, power supply, Vermier caliper,
graph paper, ctc.
Theorv:
Composite materials can be recommended for a suitable engineering appiication after investigating
the properties of the same in the laboratory. There are numerous properties like mechanical
properties, chemical properties, electrical properties, optical properties, heat resistant, resistant to
corrosion and water absorption etc. The polymer based composites are widely used for structural
purposes where the mechanical properties are more important to study. Students are advised to study
the characterization of composites in the areaofelectrical, chemical engineering etc.
Composite materials can be mechanically characterized to diagnose the properties such as tensile
strength, compressive strength, shear strength, elastic modulii in different directions, poison's ratio
in different directions, energy absorbed by impact loading or ballistic impact etc.
Procedure:
First look at geomnetry of the sample as per the standard guided by instructor in the laboratory.
Cut the approximate size of the sheet by sawing and file the edges to remove any unwanted
projected part.
Make surface finish good so as to satisfy the standard.
Adjust the anvil of 3 point bend test setup shown Figurel as per the [Link].
Place the sample over the anvil of 3 point bending set up.
Make sure there should be no initial bending load.
Place dial gauge just below the sample to display the deflection while subjected to bend load.
Switch 'ON' the Tensometer to apply the load gradually.
Record the load value corresponding to each increment in deflection.
Keep on loading tillthe fracture.
Record load at the initiation of crack if possible.
Stop the test when complete fracture occurs in the specimen.
Take the fractured specimen under microscope to observe the mode of fracture.
Draw load deflection curve on graph paper and measure the slope.
Repeat the same procedure (Optional) for another specimen having different fraction of
reinforcing material and draw the load- deflection curve for same on the same plot.
Make comparison between the slopes.

Page l ot 2
P

Specimen

Span (|)
P/2 P/2

Figure1. Loading diagram of3point bend test Observations:


Specimen width b = mm

Specimen thickness d = mm

Span = mm
Moment of inertia I= mm4

Calculation: A1
PI3
W=
48 EI
Where,
w =Central deflection of simply supported beam (glass slide)
P=load at centre
l= Span between supports
E-Young's modulus
I= Moment of inertia = (bdy12
P 3
E = = (slope of curve) 4bd3
w 48(bd3 /12)
Result:
Young's Modulus of the composite is
Bending strength of composite is
Fracture strength of composite is
Crack initiatior load/stress is
Write down nnicroscopic observations of the fractured surface of the composite like mode of fracture,
failure of matrix or failure of reinforcing element, fiber pullout, ett. i..

Precautions:
Take care of geometry of specimen.
Loading must be gradually as slow as possible.
The distance between the end supports must be carefully fixed [Link] may be
affected.
Take care of your self when specimen breaks.
Dial gauge reading must be corresponding to actual load.
Careless measurement of slope of curve may affect the properties of composite.
As and when specimen have complete fracture the machine should be stopped immediately.

Page 2 of 2
Practical-Instruction Sheet
Course: Material Science and Engineering Laboratory
Course code: AM13203
Department of Applied Mechanics
Experiment: Fabrication of conmposite materials by hand-lay up technique.
Objective:
> Learning of the use of polymer in making composite.
> Selection of suitable polymer and fiber (Reinforcing material) in fabricating the
composite.
Learning of fabrication of natural fiber reinforced or artificial fiber reinforced
composite.
Equipment: Suitable resin (epoxy), hardener (catalyst), natural fiber or artificial fiber
(short glass fiber), mould, pot for blending;of polymer, fiber and hardener etc.
Theory:
Now-a-days, in the industries of aerospace, marine, automobile and structural;
composites are replacing costly and difficult to machine the metals and alloys.
"Composite may be defines as a material composed of two or more than two
material which is chemically inhomogeneous, physically distinct and mechanically
separable resulting in to average properties of matrix and reinforcing material." Composite
materials broadly may be categorized as
(i) Polymer based metal reinforced composite (PMC)
(i) Ceramic based metal reinforced composite (CMC)
(ii)Metal based metal reinforced composite (MMC)
Further, there are many ways to categorize the composite materials. Students are advised to
go through some text books for detailed study.
Advantages: There are main advantages of composites as follows:
Development of composites is basically a replacement of heavy metals and alloys due
to its light weight.
Strength to weight ratio is high as compared to metals and alloys.
A cheaper material can be produced as compared to metals and alloys.
Properties can be tailored as per requirement and application.
Waste material can be used to economise the production cost of component.
Natural fiber reinforced composites may be eco-friendly. etc.
Procedure:
a. Select a suitable polymer resin whether is a thermoplast or thermoset.
b. Select any suitable hardener (catalyst) as per the use of resin.
C. Select an artificial or natural fiber. These fibers may be short, long, chopped or
WOven.

d. Weigh fiber or measure the diameter and length of fiber precisely. Take 2 to 5 % of
fiber by weight.
e. Clean mould with acetone to remove any dust or oily surface.
f. Blend the polymer resin with catalysts in a particular ratio by weight or by volume.
g. Lay down a sheet of Mylar in to the cavity of mould or coat the wax.
h. Lay down one layer of blended polymer in to cavity of mould.
i. Immediately lay down one layer of the fiber ensuring the straightening and
orientation of fiber (if long fiber is being used otherwise spread short fiber over the
surface of poured resin). If mat is being used, lay down one layer of mat.
j. Immediately lay down one more layer of blernded polymer over the surface of fiber.
Page lof 2
k. Ensure proper layering of polymer uniformly.
1, Cover the mould and press it in to cavity of mould so that air bubbles can be
escaped.
m. Leave it for curing to at least 24 hour or suggested by instructor.

Observations:
(i) After completion of curing time, take the composite sheet out of the mould very
carefully.
(ii) Observe the sheet and check there should be no bubble or unfilled space.
(üi)If there is any unfilled space, fill the space with the same blended polymer and
again leave it for 24 hour.
(iv)Observe with naked eyes or any other instrument to ensure proper alignment of
fiber in to the matrix of polymer.
(V) Trim the sheet corners to remove extra material and cut the sheet as per the
required dimension for further use.
Results:
In the laboratory, a composite has been developed using .(name the materials
and its proportions)
Discussion:
Discuss about the application of composite which has been developed in the
laboratory.
Discuss about the advantages and limitations of Hand Lay-up technique.
Discuss about the advantages and limitations of developed composite.
Precautions:
Take care of yourself while handling the mould.
Before blending the polymer with catalysts weigh or measure the volume of the
same.
Don't be late after blending the polymer with hardener because chemical reaction is
started and curing takes place.
Press the mould cavity after pouring the material immediately.
Give sufficient time to be cured the material.

Page 20f 2

Common questions

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Key considerations include ensuring that the specimen geometry conforms to standards, the loading is applied gradually to avoid premature failure, and the span between supports is fixed accurately to prevent skewed results. Deviation in geometry can lead to inaccurate Young’s modulus and fracture strength calculations. The meticulous setup ensures the reliability and accuracy of data such as the load-deflection curve, which is critical for determining the material's mechanical properties .

Precautions include ensuring the precise measurement of specimen dimensions, calibrating instruments like dial gauges for accurate deflection readings, and gradually applying load to avoid dynamic impacts. The environmental conditions such as temperature and humidity should also be consistent as they can affect the material properties. Carefully aligning specimens in test fixtures can prevent uneven stress distributions which would skew results .

Short fibers are generally used to improve toughness and impact resistance, whereas long fibers provide better tensile strength and stiffness. Woven fibers allow for directional strength and flexibility depending on the weave pattern. The choice of fiber type influences both the manufacturing process and the performance in applications; for example, long fibers are ideal for high-strength structural components, while woven fibers might be used where flexibility and multidirectional strength are needed .

Challenges of the hand-layup technique include difficulty in ensuring uniform fiber distribution, potential voids or air bubbles, and longer curing times. The manual process may lead to inconsistencies in layer thickness and alignment, impacting the material properties. Additionally, it might not be suitable for high-volume production or complex shapes without significant labor and time investments .

Proper curing is essential as it ensures the complete polymerization of the resin, which directly impacts the mechanical strength and durability of the composite. Inadequate curing can lead to weak bonds between fibers and the matrix, resulting in reduced load-bearing capacity and an increased risk of failure under stress. This stage solidifies the composite's structural integrity, making it crucial for achieving desired material properties .

The key mechanical properties that can be investigated include tensile strength, compressive strength, shear strength, elastic modulus in different directions, and Poisson's ratio in different directions. These properties are crucial because they determine the composite's ability to withstand loads and deformations, which is essential for their application in structural engineering where strength-to-weight ratios and flexibility of design are pivotal .

The hand-layup technique allows for precise control over the placement of fibers and resin, which can enhance the material properties by optimizing fiber orientation and density. Its primary advantages include lower production costs, ease of use, and the ability to use a variety of fibers and resins to tailor properties for specific applications. Additionally, it facilitates the use of natural fibers, making it an eco-friendly option .

The load-deflection curve is utilized to evaluate the mechanical strength by plotting the applied load against the corresponding deflection of the specimen. The slope of the curve reflects the stiffness or Young’s modulus of the material, and the area under the curve can indicate the energy absorption capabilities. Critical points on the curve, like the onset of non-linear behavior or fracture, provide insights into the strength and ductility of the material .

The high strength-to-weight ratio allows for the construction of lighter and stronger components, enhancing fuel efficiency and performance. This leads to significant reductions in energy consumption and emissions in aerospace and automotive industries. Additionally, their tailoring properties enable specific design optimizations, improving aerodynamics, safety, and overall vehicle performance .

Natural fibers provide environmental benefits as they are biodegradable, have lower energy requirements for production, and reduce dependency on synthetic, non-renewable materials. This makes them preferable in sustainable engineering, particularly where eco-friendly solutions are prioritized. Their use in composites can also contribute to a reduction in carbon footprint and promote waste recycling by using agricultural or industrial by-products .

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