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Laboratory Guide: Covalent Compounds

This document outlines a laboratory exercise focused on covalent compounds, where students will observe properties, conduct experiments, and categorize substances as ionic, polar covalent, or non-polar covalent. The exercise includes tests for melting point, solubility in water and hexane, and conductivity. Safety precautions are emphasized, and students are expected to analyze their findings in a conclusion and discussion section.

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0% found this document useful (0 votes)
10 views3 pages

Laboratory Guide: Covalent Compounds

This document outlines a laboratory exercise focused on covalent compounds, where students will observe properties, conduct experiments, and categorize substances as ionic, polar covalent, or non-polar covalent. The exercise includes tests for melting point, solubility in water and hexane, and conductivity. Safety precautions are emphasized, and students are expected to analyze their findings in a conclusion and discussion section.

Uploaded by

Venus Caringal
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOC, PDF, TXT or read online on Scribd

Chemistry

1
Covalent Compounds

Week 006 – Covalent Compounds


Laboratory Exercise 04

Objective/s:
At the end of this activity, you should be able to:
Observe and describe the properties of some covalent compounds.
Perform experiment illustrating the properties of covalent compounds.

Examine certain physical properties of three compounds to try to determine if they are


covalent compounds and if they are covalent polar or non-polar compound.

Introduction
Covalent bonds form between non-metal atoms. Each bond consists of a shared
pair of electrons, and is very strong. Simple molecular substances and giant
covalent structures have different properties. Atoms will form bonds with other
atoms in an attempt to obtain a stable valence electron shell. To obtain a stable
valence shell, atoms can either gain or lose electrons or share electrons. Atoms can
share electron pairs when their orbitals overlap to form single, double, or triple covalent bonds.
Covalent bonds are formed when nonmetals bond to nonmetals. Covalently bonded atoms form
molecules. These molecules can exist as solids, liquids, or gases. These molecules can be polar or
nonpolar depending on their shape and the distribution of charge within the molecule.

Materials:
Table Salt
Sugar
Wax
Hot Plate
Aluminum foil
Deionized water
Conductivity tester
Three 100 mL beakers
Stirring rods
Crucible tongs
Spatula

Assessments
Safety:
SAFETY GOGGLES MUST BE WORN AT ALL TIMES. Carefully follow all instructions, both written
and oral. Report any accident (spill, breakage, etc.) or injury (cut, burn, etc.) to the instructor
immediately, no matter how trivial it may appear.

Procedure
Part 1: Test of Melting Point
Generally, ionic solids have very high melting point temperatures. Covalent molecules have a lower
melting point. Polar covalent molecules have a higher melting point than non-polar covalent
molecules.
1. Mold an aluminum foil boat that will serve as a tray for the table salt, sugar, wax.
2. At different corners of the boat place a very small amount of each substance.
a. Table Salt
b. Sugar
c. Wax (from teacher)
3. Set the hot plate on high.
4. Observe and record the order of melting of the solids in your data table (1, 2, 3)
5. After observations are complete, CAREFULLY remove the aluminum foil boat with crucible
tongs and allow it to cool completely. Dispose of the boat in the garbage.

Part 2: Test of Solubility


Generally, ionic solids are only soluble in very polar solvents (such as water). Polar covalent
molecules will dissolve in polar solvents and non-polar covalent molecules will only dissolve in non-
polar solvents (“like dissolves like”).
1. Test the solubility of each of the three solids by placing a “scoop” of each solid in a 100mL
labeled beaker and filling it half way with de-ionized water. (Avoid cross contamination in
beakers!)
2. Stir the mixture and observe and record if the solid dissolved in the water. (DO NOT DUMP IT
OUT!)

Part 3: Test of Conductivity


When an ionic compound dissolves, the ions are often pulled apart by the polar water and become
free to move about in the solvent. The movement of these charged ion particles allows for the
conduction of an electric current. Undissolved solids or polar covalent solids do not form these ions in
water and thus do not allow for conduction.
1. Insert the metal electrodes of your conductivity tested into each of the three mixtures you
created in the 100 mL beakers. Using a paper towel, clean the leads to avoid cross contamination
between tests.
Chemistry
3
Covalent Compounds

2. Observe and record if conductivity was detected in each solution. A positive result is indicated
by a steady green light.

Data Table

Name of Compound Order of Melting Soluble in water? Soluble in hexane? Conducts in water?

Sugar No

Salt No

Wax Yes

Conclusion:
Based upon your observations, place each substance into one of the following categories: ionic
compound, polar covalent compound, or non-polar covalent compound. Based on the data given
for the solubility in hexane, is hexane a polar or non-polar covalent solvent? Explain.

Discussion:
Discuss the reasons why you placed each substance in its category. Provide evidence from the
melting point, solubility, and conductivity tests you did in the lab.

Assessments

Common questions

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Sugar, which is soluble in water but does not conduct electricity, can be categorized as a polar covalent compound since it dissolves in polar solvents but does not dissociate into ions. Salt is soluble in water and conducts electricity, indicating it is an ionic compound. Wax, not dissolving in water and not conducting electricity, is likely a non-polar covalent compound .

The procedure minimizes cross-contamination by instructing the use of separate, labeled beakers for each compound, filling them with deionized water, and cleaning the stirring rods between each use. These steps prevent residue from transferring between samples .

The experiment uses a consistent heat source (hot plate on high) and separate corners of the aluminum foil boat to ensure each substance is subjected to the same experimental conditions, preventing cross-contamination. This method allows for a reliable comparison of their melting points, ensuring accurate observations .

Melting point characteristics help differentiate compounds based on bond strength and type. Ionic compounds generally have very high melting points due to the strong electrostatic forces between ions. Polar covalent molecules have higher melting points than non-polar covalent molecules due to intermolecular forces like hydrogen bonds. Non-polar covalent compounds have lower melting points as these forces are weaker .

Ionic compounds conduct electricity when dissolved in water because the ions dissociate and freely move in the solution, enabling electrical conduction. In contrast, covalent compounds do not dissociate into ions in water; hence, they lack charged particles to carry an electric current, which explains why they generally do not conduct electricity .

The aluminum foil boat method allows all tested substances to be heated simultaneously under identical conditions, providing a straightforward way to compare their melting points on the same heat source. It minimizes the introduction of variables that could arise from using different containers or environments .

A substance that does not dissolve in water likely consists of covalent molecules that do not dissociate into ions. Since free-moving ions are required to conduct electricity, these substances cannot conduct electricity if they remain undissolved and retain their molecular integrity in the water .

The 'like dissolves like' principle suggests that polar solvents dissolve polar solutes, while non-polar solvents dissolve non-polar solutes. In the context of the experiment, if a substance is soluble in hexane, a known non-polar solvent, it indicates that the solute is also non-polar. Conversely, if a solute is not soluble in hexane, it suggests the solute may be polar or ionic .

It is important to use crucible tongs when handling the aluminum foil boat because the procedure involves heating the boat on a hot plate, which makes it too hot to touch directly. Using tongs ensures the safety of the experimenter by preventing burns .

Deionized water is used in solubility tests to avoid interference from ions present in regular tap water, which could affect the solubility results. The absence of ions ensures that any changes observed in the solubility tests are due solely to the properties of the solute, not contaminants .

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