MP236 Economic Geology
and Mineralogy
Week 4. Lecture
INTRODUCTION TO ORE MICROSCOPY
Dr. Kaul Gena
Outline
• Preparation of specimens
• Introduction to microscopy
• Qualitative mineral identification
• Quantitative mineral identification
• Implications for process mineralogy
Preparation of Samples
• Different preparation techniques for different microscopic
methods
• Polished sections/blocks for reflected light petrography
• mainly used for ore petrography
• Thin sections (30 microns thick) for transmitted light
petrography
• Polished thin sections allow both reflected and transmitted
light petrography
Sphalerite in Reflected Light
(From Craig & Vaughan, 1994)
Sphalerite in Transmitted Light
(From Craig & Vaughan, 1994)
Preparation of Polished Sections
• Sample needs to be cut to size (ore sample), or
mounted in epoxy (mill or porous samples)
• Grinding to produce a flat surface
• usually silicon carbide paper or powder
• Polishing to produce a reflective surface
• aluminium oxide or diamond paste
• powder may go down to 0.05 microns
• Samples may be chemically etched
Preparation Sequence
(From Craig & Vaughan, 1994)
600-mesh Silicon Carbide
(From Craig & Vaughan, 1994)
15-micron Aluminium Oxide
(From Craig & Vaughan, 1994)
0.05-micron Aluminium Oxide
Sphalerite
Chalcopyrite
(From Craig & Vaughan, 1994)
Without Intermediate Steps
(From Craig & Vaughan, 1994)
Pyrite Grain Prior to Etching
(From Craig & Vaughan, 1994)
After Etching With HNO3
(From Craig & Vaughan, 1994)
Reflected Light Microscope
(From Craig & Vaughan, 1994)
Qualitative Mineral Identification
• Crystal habit
• Colour
• Hardness
• Reflectivity
• Bireflectance
• Reflectance pleochroism
• Anisotropy
Colour in Ore Petrology
Pyrite
Sphalerite
Chalcopyrite
Silicates
Colour in Ore Petrology
Marcasite
Galena
Sphalerite
Section With High Relief
(From Craig & Vaughan, 1994)
Section With No Relief
(From Craig & Vaughan, 1994)
Polishing scratch
Hard mineral
Soft mineral
Relative Hardness
Cleavage
Triangular pits
Internal Reflections
Internal Reflections
(From Craig & Vaughan, 1994)
Deformation Lamellae
(From Craig & Vaughan, 1994)
Advanced Optical Properties
• Bireflectance and reflectance pleochroism
• The reflectance and colour of a mineral may vary slightly as the
microscope stage is rotated
• Anisotropy
• With the polarizers crossed, the colour of the mineral may vary as
the stage is rotated
Both of these properties may be quite subtle, and
are best demonstrated in the laboratory
Bireflectance
The stage has been rotated 90 degrees between views
(From Craig & Vaughan, 1994)
Anisotropy
Conclusions
• Reflected light microscopy relies on a characteristic
set of properties different from those used in
transmitted light microscopy for mineral identification
• Of particular importance are colour, bireflectance, and
anisotropy
• Like transmitted light microscopy, reflected light skills
take considerable time to develop