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High Pressure Vessels and Reactors

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0% found this document useful (0 votes)
33 views12 pages

High Pressure Vessels and Reactors

Uploaded by

mohsen fatemi
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

1295 Full Line Catalog 216.

qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 108

High Pressure Equipment


Pressure Vessels
and Reactors
High Pressure Equipment Company designs and manufactures a broad range of pressure vessels and reactors
for both bench-scale and pilot plant applications. We have over 250 standard reactor designs which address
varied size, material, pressure and temperature requirements.
There are many applications that demand ASME approval for work involving pressure vessels. To satisfy this
need, HiP produces a variety of pressure vessels and reactors that meet the requirements of the ASME Pressure
Vessel Code.
Complementing our standard product offering is our capability to provide a custom reactor designed to meet
your specific needs. Our engineering and technical support will help you identify the specific options you need,
ranging from exotic materials to unusual sizes and connections, and then incorporate the appropriate approvals,
including ASME.

Index Page

Pressure Vessel Selection . . .10.2-10.3


O-Ring Seal Reactors
Series OC . . . . . . . . . . . . . . . . .10.4
Confined Gasket Closure
Reactors - Series GC . . . . . . . .10.5
Bolted Closure Reactors . . . . . . . .10.6
Clover Leaf Reactors . . . . . . . . . . .10.7
O-Ring Closure Reactors
Series R . . . . . . . . . . . . . .10.8-10.9
Tubular Reactors
Series TOC . . . . . . . . . .10.10-10.11
Micro Reactors
Series MS . . . . . . . . . . . . . . . .10.12

10.1
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 109

High Pressure Equipment


Reactor Selection Guide Maximum
Maximum Working
Reactor Standard Temperature Pressure Standard
Design Description Material (degrees F) (psi) Capacity

Simple closure design allows for


O-ring easy assembly/disassembly and 125 mL
Seal reliable operation. Series OC are 316SS 250 16,000 to
Series OC economical reactors ideal for low 6,750 mL
temperature gas or liquid service.

Series GC is designed for


Confined studying high temperature and 125 mL
Gasket pressure reactions. The vessels 316SS 800 16,000 to
Closure utilize thrust bolts and a thrust 6,750 mL
ring to ensure positive seating
Series GC of the gasket.
These versatile reactors are
Bolted the standard of the industry for
Closure applications involving moderate 300 mL
pressure ranges. Standard 316SS 650 5,000 to
Series BC O-rings may be used in place 2 gal.
of the metal gasket for lower
temperatures.

Quick opening cover design


Clover needs only one-eighth of a turn 4340 1,000 mL
Leaf rotation for sealing. Ideal for high
alloy 250 30,000 to
pressure operations requiring
Series CL repetitive opening/closing. steel 3,700 mL

Designed for extremely high


O-ring pressure/low temperature 4340 77 mL
Closure operation, series R reactors alloy 250 150,000 to
Series R feature a threaded closure for
easy assembly and disassembly.
steel 30 liters

Series MS are fixed bed tubular


Micro reactors designed for a variety 2 mL
Reactors of applications such as small 316SS 800 30,000 to
Series MS volume testing of components 64 mL
and miniature scale reaction tests.

This line of economical and O-ring


versatile reactors satisfy many 250 50 mL
Tubular moderate pressure applications. 304SS confined 10,000 to
Reactors Accumulators can be customized
15 liters
Series TOC through a variety of options gasket
including piston separators. 800

HiP makes every reactor to


order, allowing for economical
Custom and timely customizing. We offer
Reactors a broad range of exotic metals,
sizes and connections to meet
virtually any requirement.

10.2
Note: For ASME code stamping of HiP vessels, please consult factory R1 12/97
for available reactor designs, materials, and pressure ratings.
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 110

Pressure Vessel Volume Table (cubic inches)


Inside
Depth
(inches) Inside Diameter (inches)
1 2
/" 1" 11/2" 2" 21/2" 3" 4" 5" 6" 7" 8" 9" 10"
4" 0.7856 3.142 7.068 12.57 19.63 28.27 50.26 78.54 113.1 153.9 201.1 254.5 314.2
6" 1.178 4.712 10.60 18.85 29.45 42.41 75.40 117.8 169.6 230.9 301.6 381.7 471.2
8" 1.571 6.283 14.14 25.13 39.27 56.55 100.5 157.1 226.2 307.9 402.1 508.9 628.4
10" 1.964 7.854 17.67 31.42 49.09 70.69 125.7 196.3 282.7 384.8 502.6 636.2 785.2
12" 2.357 9.425 21.21 37.70 58.90 84.82 150.8 235.6 339.3 461.8 603.2 763.4 942.4
14" 2.749 11.00 24.74 43.98 68.72 98.96 175.9 274.9 395.8 538.8 703.7 890.6 1100
16" 3.142 12.57 28.27 50.27 78.54 113.1 201.1 314.2 452.4 615.8 804.2 1018 1257
18" 3.535 14.14 31.81 56.55 88.36 127.2 226.2 353.4 508.9 692.7 904.8 1145 1415
20" 3.928 15.71 35.34 62.83 98.17 141.4 251.3 392.7 565.5 769.7 1005 1272 1571
22" 4.231 17.28 38.88 69.12 108.0 155.5 276.5 432.0 622.0 846.7 1106 1400 1728
24" 4.714 18.85 42.41 75.40 117.8 169.6 301.6 471.2 678.6 923.6 1206 1527 1885
26" 5.106 20.42 45.94 81.68 127.6 183.8 326.7 510.5 735.1 1001 1307 1654 2042
28" 5.499 21.99 49.48 87.96 137.4 197.9 351.8 549.8 791.7 1078 1407 1781 2199

Volume Equivalents Pressure Conversions


1 in3 = 16.39 mL psi atm kg/cm2
1 mL = 0.061 in3 psi 1 0.068 0.070
1 gal = 231 in3 = 0.134 ft3
1 ft3 = 1728 in3 = 7.481 gal atm 14.696 1 1.033
1 L = 61.02 in3 = 0.264 gal kg/cm2 14.224 0.968 1

10.3
High Pressure Equipment Company R1 12/97
2955 W. 17th Street • Erie, PA 16505 U.S.A. • Phone: (814) 838-2028 • 1-800-289-7447 • Fax: (814) 838-6075 • Website: [Link]
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 111

High Pressure Equipment

OC Series O-Ring
Seal Reactors
The OC Series provide a simple closure that is reliable and easy
to assemble and disassemble. Standard material for the body and
cover is Type 316 stainless steel. The standard O-ring material is
BUNA-N. Temperature is limited by the O-ring to 250°F.
These reactors are suitable for either gas or liquid service.
Capacities range from 125 mL to 6,750 mL.
Standard connections are for 1/4" O.D. high pressure (coned
and threaded) tubing (HF4). Models OC-1 and OC-3 have one
connection in the cover. All other models have two connections
in the cover. Contact factory if other connections and/or locations
are preferred.

1
Series OC Reactors
Working
Catalog Inside Pressure
No. I.D. O.D. Depth Capacity Material psi
2
OC-1* 1" 21/2" 10" 125 mL 316 S.S. 13,800
3 OC-3* 11/2" 21/2" 10" 280 mL 316 S.S. 7,750
OC-5 11/2" 43/8" 10" 280 mL 316 S.S. 16,000
OC-7 11/2" 43/8" 21" 600 mL 316 S.S. 16,000
OC-9 2" 43/8" 10" 500 mL 316 S.S. 12,500
OC-11 2" 43/8" 21" 1,040 mL 316 S.S. 12,500
DEPTH

4
OC-13 21/2" 43/8" 10" 800 mL 316 S.S. 9,200
OC-15 21/2" 43/8" 21" 1,160 mL 316 S.S. 9,200
I.D.
OC-17 3" 67/8" 10" 1,150 mL 316 S.S. 13,000
OC-19 3" 67/8" 21" 2,430 mL 316 S.S. 13,000
OC-21 31/2" 67/8" 10" 1,575 mL 316 S.S. 10,500
OC-23 31/2" 67/8" 21" 3,300 mL 316 S.S. 10,500
OC-25 4" 67/8" 10" 2,060 mL 316 S.S. 8,500
OC-27 4" 67/8" 21" 4,325 mL 316 S.S. 8,500
OC-29 41/2" 67/8" 10" 2,600 mL 316 S.S. 6,500
1. COVER 316 S.S.
2. CAP ALLOY STEEL OC-31 41/2" 67/8" 21" 5,475 mL 316 S.S. 6,500
3. "O" RING BUNA-N
4. BODY 316 S.S.
OC-33 5" 67/8" 10" 3,200 mL 316 S.S. 5,000
OC-35 5" 67/8" 21" 6,750 mL 316 S.S. 5,000
* One (1) opening only in cover

10.4
R2 12/99
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 112

Confined Gasket
Closure Reactors
The Confined Gasket Closure reactors listed below are ideally
suited for use at elevated temperatures and pressures as shown
in the chart. Thrust bolts with a hardened thrust ring are supplied
to insure positive seating of the gasket. Torque required on thrust
bolts will range from 70 to 125 foot pounds, depending upon size
of reactor, pressure, temperature and media being pressurized.
Torquing of bolts should be done in a crisscross staggered pattern
to insure uniform seating. A commercial high temperature lubricant
should always be applied to the bolt threads and outside cap
threads to facilitate removal of the closure.
Standard material for the body, cover and gasket is Type 316
stainless steel. These reactors are suitable for either gas or liquid
service and capacities range from 125mL to 6,750 mL.
Standard connections supplied are for 1/4" O.D. high pressure
(coned and threaded) tubing (HF4). Models GC-1 and GC-3 have
one connection in the cover. All other models have two connections
in the cover and a thermowell that extends two-thirds of the inside depth.
Included with each reactor are eye bolts for lifting and necessary
collars and glands for the connections. Vise flats are machined
on to the bottom of the body for securing while assembling or
disassembling closure.

1
Series GC Reactors 2

3
Catalog Inside Working Pressure (psi)
No. I.D. O.D. Depth Capacity Material 100°F 650°F 800°F 4
5 8
GC-1 1" 21/2" 10" 125 mL 316 S.S. 13,800 12,500 12,000
GC-3 11/2" 21/2" 10" 280 mL 316 S.S. 7,750 7,000 6,900 6

GC-5 11/2" 43/8" 10" 280 mL 316 S.S. 16,000 14,500 14,000
GC-7 11/2" 43/8" 21" 600 mL 316 S.S. 16,000 14,500 14,000
GC-9 2" 43/8" 10" 500 mL 316 S.S. 12,500 11,400 11,000 7
DEPTH

GC-11 2" 43/8" 21" 1,040 mL 316 S.S. 12,500 11,400 11,000
GC-13 21/2" 43/8" 10" 800 mL 316 S.S. 9,200 8,400 8,200
GC-15 21/2" 43/8" 21" 1,160 mL 316 S.S. 9,200 8,400 8,200
I.D.
GC-17 3" 67/8" 10" 1,150 mL 316 S.S. 13,000 11,000 10,000
GC-19 3" 67/8" 21" 2,430 mL 316 S.S. 13,000 11,000 10,000
GC-21 31/2" 67/8" 10" 1,575 mL 316 S.S. 10,500 9,000 8,000
GC-23 31/2" 67/8" 21" 3,300 mL 316 S.S. 10,500 9,000 8,000
GC-25 4" 67/8" 10" 2,060 mL 316 S.S. 8,500 7,300 6,500 1. COVER 316 S.S.
2. SET SCREW COMM.
GC-27 4" 67/8" 21" 4,325 mL 316 S.S. 8,500 7,300 6,500 3. CAP ALLOY ST'L
4. THRUST RING TOOL ST'L
GC-29 41/2" 67/8" 10" 2,600 mL 316 S.S. 6,500 5,500 5,000 5. GASKET COPPER
41/2" 21" 6. GASKET 316 S.S.
GC-31 67/8" 5,475 mL 316 S.S. 6,500 5,500 5,000
7. BODY 316 S.S.
GC-33 5" 67/8" 10" 3,200 mL 316 S.S. 5,000 4,300 4,000 8. WEEP HOLE

GC-35 5" 67/8" 21" 6,750 mL 316 S.S. 5,000 4,300 4,000

10.5
High Pressure Equipment Company R1 12/97
2955 W. 17th Street • Erie, PA 16505 U.S.A. • Phone: (814) 838-2028 • 1-800-289-7447 • Fax: (814) 838-6075 • Website: [Link]
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 113

High Pressure Equipment

Bolted Closure Reactors


The Bolted Closure Reactors are designed for use up to 650°F
(343°C) at the working pressures indicated. Standard material
for the body, cover and gasket is Type 316 stainless steel.
Standard O-rings may be used in place of the metal gasket
when temperatures permit.
Standard connections include two high pressure (coned and
threaded) tubing connections for 1/4" O.D. tubing (HF4) located
in the cover. Contact factory if other connections and/or locations
are preferred.
Other items available include:
● Heating mantle. Removable quartz fabric
cylinder column type. 110 volt, single phase.
Bolted closure reactors are supplied with
mounting bolt holes on the bottom surface.
● Thermowell for use with 1/16" thermocouple

● Safety head located in side flange with rupture


disc (see Page 3.7)

2 1
1. PRESSURE CONNECTION (2) 3
2. SOCKET CAP SCREW 4
3. COVER 5
4. GASKET
5. MAIN SEAL
6. BODY 8
7. THERMOCOUPLE WELL*
8. SAFETY HEAD* 6
* SUPPLIED AS EXTRA
Bolted Closure Reactors WHEN SPECIFIED
7
DEPTH

Working Temperature Approx. Approx.


Catalog Pressure Rating Inside Inside Weight Torque (ft-lb)
No. Capacity psi °F Diameter Depth (pounds) per Bolt Material
BC-1 300 mL 5,000 650 2" 6" 21 40 316 S.S.
BC-2 1 liter 5,000 650 3" 9" 50 75 316 S.S. I.D.

BC-3 2 liter 5,000 650 3 /2"


1
12 /2"
1
68 105 316 S.S.
BC-4 1 gallon 3,000 650 5" 12" 97 105 316 S.S.
BC-5 1 gallon 5,000 650 5" 12" 152 175 316 S.S.
BC-6 2 gallon 3,000 650 6 /2"
1
14" 245 140 316 S.S.

10.6
R3 11/14
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 114

Clover Leaf Reactors


The “Clover Leaf” Closure Reactors provide maximum ease for
quick opening or closing of the cover. The cover is simply inserted
into the body and then rotated one-eighth of a turn. A safety locking
pin is provided to insure that the cover is properly positioned and locked.
Standard material of construction for these reactors is heat
treated 4340 alloy steel. Standard connections include two high
pressure (coned and threaded) 1/4" O.D. tubing connections (HF4).
Mounting holes are provided in the top and bottom of the body
for securing or lifting.

1. LOCK PIN
2 2. COVER
3. O-RING
3 4. BODY

Clover Leaf Closure Reactors


DEPTH

4
Working Temperature
I.D.
Catalog Inside Outside Inside Pressure Rating
No. Diameter Diameter Depth psi °F Capacity Material
CL-1 9" 1,000 mL
Alloy
CL-2 3" 61/2" 18" 30,000 250 2,000 mL
Steel
CL-3 22" 2,500 mL
CL-8 9" 1,850 mL Alloy
CL-9 4" 91/2" 18" 30,000 250 3,700 mL Steel

10.7
High Pressure Equipment Company R1 12/97
2955 W. 17th Street • Erie, PA 16505 U.S.A. • Phone: (814) 838-2028 • 1-800-289-7447 • Fax: (814) 838-6075 • Website: [Link]
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 115

High Pressure Equipment

Series “R” Reactors


O-Ring Closure
The Series “R” O-ring Closure Reactors are easily
assembled and disassembled with minimal torque
required for complete engagement.
Material of construction for standard models is Type
4340 alloy steel (or equivalent) properly heat treated for
use at elevated pressures. (Some models can be provided
in stainless steel construction at reduced pressures —
consult factory).
Sealing is accomplished by a highly reliable combination
of O-ring and separate metal back-up ring. The wedge
shaped back-up ring is designed to expand and contract as
pressure increases or decreases. Consequently, the O-ring is
continuously confined with no clearance for extrusion. Minimal
initial torque is required to effect a positive seal.
Temperature on these vessels must be restricted to 250°F
maximum, due to the BUNA-N (nitrile) O-ring.
(continued on page 10.9)

O-Ring Closure Reactors (one piece cover)


1
Pressure Inside Depth
2 Rating
I.D. O.D. psi Material 6" 10" 12" 16" 20" 24"
3 / 8"
1
30,000 R1-6-30 R1-10-30 R1-12-30 R1-16-30
3
4340
3 / 2"
1
40,000 R1-6-40 R1-10-40 R1-12-40 R1-16-40
4 Alloy
5 1" 41/4" 60,000 Steel R1-6-60 R1-10-60 R1-12-60 R1-16-60
or
5 / 2"
1
100,000 equivalent R1-6-100 R1-10-100 R1-12-100 R1-16-100
I.D.
6 / 4"
3
150,000 R1-6-150 R1-10-150 R1-12-150 R1-16-150

3 / 8"
5
20,000 R1.5-6-20 R1.5-10-20 R1.5-12-20 R1.5-16-20
DEPTH

4 / 8"
1
30,000 R1.5-6-30 R1.5-10-30 R1.5-12-30 R1.5-16-30
4340
43/4" 40,000 Alloy R1.5-6-40 R1.5-10-40 R1.5-12-40 R1.5-16-40
11/2" Steel
6 / 2"
1
60,000 or R1.5-6-60 R1.5-10-60 R1.5-12-60 R1.5-16-60
equivalent
8" 100,000 R1.5-6-100 R1.5-10-100 R1.5-12-100 R1.5-16-100
10 /2"
1
150,000 R1.5-6-150 R1.5-10-150 R1.5-12-150 R1.5-16-150

4 / 4"
1
20,000 R2-6-20 R2-10-20 R2-12-20 R2-16-20 R2-20-20 R2-24-20
4340
6 5" 30,000 R2-6-30 R2-10-30 R2-12-30 R2-16-30 R2-20-30 R2-24-30
1. COVER Alloy
2. BODY 2" 6 / 2"
1
40,000 Steel R2-6-40 R2-10-40 R2-12-40 R2-16-40 R2-20-40 R2-24-40
3. VENT HOLE or
4. BACK UP RING
5. "O" RING
8 / 2"
1
60,000 equivalent R2-6-60 R2-10-60 R2-12-60 R2-16-60 R2-20-60 R2-24-60
6. PRESSURE CONNECTION
12" 100,000 R2-6-100 R2-10-100 R2-12-100 R2-16-100 R2-20-100 R2-24-100

10.8
R3 8/04
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 116

Included with each vessel is a Tony Bar for removal of the cover
nut and necessary eye bolt holes for lifting of the body and
components. Outer surfaces are blackened to prevent rusting.
Vent holes are provided to prevent pressure build up behind
the closure in the event of a worn or damaged seal.
Connections include a top and bottom high pressure coned
and threaded 1/4" O.D. (HF4) tubing connection. Other sizes or
locations for connections can easily be provided when preferred.
Consult factory.
Closures are designed in one-piece (cover) for vessels up
to 2" I.D. and two-piece (cover and main nut) for vessels larger
than 2" I.D.

O-Ring Closure Reactors (two piece cover)


Pressure 1. PRESSURE
Inside Depth CONNECTION
Rating 2. MAIN UNIT NUT
I.D. O.D. psi Material 6" 10" 12" 16" 20" 24" 3. BODY
4. VENT HOLE
6" 20,000 R3-6-20 R3-10-20 R3-12-20 R3-16-20 R3-20-20 R3-24-20 5. COVER
7" 30,000 R3-6-30 R3-10-30 R3-12-30 R3-16-30 R3-20-30 R3-24-30 6. BACK UP RING
7. "O" RING
3" 81/2" 40,000 R3-6-40 R3-10-40 R3-12-40 R3-16-40 R3-20-40 R3-24-40
1
111/2" 60,000 R3-6-60 R3-10-60 R3-12-60 R3-16-60 R3-20-60 R3-24-60
2
15" 100,000 R3-6-100 R3-10-100 R3-12-100 R3-16-100 R3-20-100 R3-24-100
8" 20,000 R4-6-20 R4-10-20 R4-12-20 R4-16-20 R4-20-20 R4-24-20 3

9 /4"
1
30,000 R4-6-30 R4-10-30 R4-12-30 R4-16-30 R4-20-30 R4-24-30
4
4" 11" 40,000 R4-6-40 R4-10-40 R4-12-40 R4-16-40 R4-20-40 R4-24-40
5
13" 50,000 R4-6-50 R4-10-50 R4-12-50 R4-16-50 R4-20-50 R4-24-50
15" 60,000 R4-6-60 R4-10-60 R4-12-60 R4-16-60 R4-60-60 R4-24-60
91/4" 20,000 4340 R5-6-20 R5-10-20 R5-12-20 R5-16-20 R5-20-20 R5-24-20
DEPTH

111/4" 30,000 Alloy R5-6-30 R5-10-30 R5-12-30 R5-16-30 R5-20-30 R5-24-30


5" Steel
131/4" 40,000 or R5-6-40 R5-10-40 R5-12-40 R5-16-40 R5-20-40 R5-24-40
151/4" 50,000 equivalent R5-6-50 R5-10-50 R5-12-50 R5-16-50 R5-20-50 R5-24-50 I.D.

91/2" 10,000 R6-6-10 R6-10-10 R6-12-10 R6-16-10 R6-20-10 R6-24-10


111/2" 20,000 R6-6-20 R6-10-20 R6-12-20 R6-16-20 R6-20-20 R6-24-20
6"
131/4" 30,000 R6-6-30 R6-10-30 R6-12-30 R6-16-30 R6-20-30 R6-24-30
15" 40,000 R6-6-40 R6-10-40 R6-12-40 R6-16-40 R6-20-40 R6-24-40
10 /4"
3
10,000 R7-6-10 R7-10-10 R7-12-10 R7-16-10 R7-20-10
7" 13" 20,000 R7-6-20 R7-10-20 R7-12-20 R7-16-20 R7-20-20
6
151/4" 30,000 R7-6-30 R7-10-30 R7-12-30 R7-16-30 R7-20-30
7
121/2" 10,000 R8-6-10 R8-10-10 R8-12-10 R8-16-10 R8-20-10
8"
141/4" 20,000 R8-6-20 R8-10-20 R8-12-20 R8-16-20 R8-20-20
9" 13" 10,000 R9-6-10 R9-10-10 R9-12-10 R9-16-10 R9-20-10 SEALING DETAIL
10" 143/4" 10,000 R10-6-10 R10-10-10 R10-12-10 R10-16-10 R10-20-10

10.9
High Pressure Equipment Company R2 12/99
2955 W. 17th Street • Erie, PA 16505 U.S.A. • Phone: (814) 838-2028 • 1-800-289-7447 • Fax: (814) 838-6075 • Website: [Link]
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:18 AM Page 117

High Pressure Equipment

Tubular Series
Reactors
The Tubular Series Reactors are double ended pressure
vessels made from commercial quality cold drawn Type
304 stainless steel seamless tubing. Outside (non-wetted)
caps are alloy steel. These are both economical and
versatile vessels proven in demand for many applications.
Finishes are commercial cold drawn finishes, with honed
internal finishes.
Standard sizes are shown in the chart on page 10.11,
but special lengths and modifications are easily supplied on
request. One pressure connection for 1/4" O.D. high pressure
coned and threaded tubing at each end is standard. Additional
end connections are possible on the larger size models. Also,
side connections and end cover thermowells can be supplied
when required. Consult factory for special requirements.
O-Ring Closures are standard when temperatures do not
exceed 250°F. This is an easily assembled closure requiring
minimal torque for positive sealing. The standard O-ring material
used is BUNA-N (nitrile) with various other O-ring materials
available on request.
Confined Gasket Closures are available for temperatures
up to 800°F. A 15% reduction in the listed working pressure is
required at this elevated temperature level. These closures utilize
a metal gasket (304 stainless steel) which can be torqued down
for positive sealing. Torque requirements on the thrust bolts will
range from 60 to 110 foot pounds depending on size, pressure,
temperature and media being pressurized. These confined gasket
closures are available for all models except the TOC1 and TOC3
series. When ordering, simply specify catalog number and add
suffix “(W/Gasket)”.
Piston Separators can be supplied with the O-ring closure vessels
for use as compression cylinders. These are ideal for separating a
liquid from a gas and other similar applications. The tubing body is
supplied with a honed inside diameter surface to accommodate the
piston. When ordering, simply specify catalog number and add suffix
“(W/Piston)”.

10.10
R1 12/97
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:19 AM Page 118

Tubular Series Reactors


Tubing Size Pressure Catalog Number (O-Ring Closure)
Rating
I.D. O.D. psi Material 20"IL 40"IL 60"IL 72"IL
1" 1 / 2"
1
5,000 TOC1-20 TOC1-40 TOC1-60 TOC1-72
/4"
3
11/2" 10,000 TOC3-20 TOC3-40 TOC3-60 TOC3-72
1 /4"
1
2" 6,000 TOC5-20 TOC5-40 TOC5-60 TOC5-72
1" 2" 10,000 TOC7-20 TOC7-40 TOC7-60 TOC7-72
13/4" 2 / 2"
1
4,000 TOC9-20 TOC9-40 TOC9-60 TOC9-72
1 /2"
1
2 / 2"
1
7,000 TOC11-20 TOC11-40 TOC11-60 TOC11-72
Body
2 /4"
1
3"
DEPTH

DEPTH

DEPTH
3,000 TOC13-20 TOC13-40 TOC13-60 TOC13-72
304 S.S.
2" 3" 5,000 TOC15-20 TOC15-40 TOC15-60 TOC15-72
Covers
23/4" 3 / 2"
1
3,000 316 S.S. TOC17-20 TOC17-40 TOC17-60 TOC17-72
2 /2"
1
3 / 2"
1
4,500 TOC19-20 TOC19-40 TOC19-60 TOC19-72 O.D. O.D. O.D.

3 /4"
1
4" 2,500 TOC21-20 TOC21-40 TOC21-60 TOC21-72 I.D. I.D. I.D.
3" 4" 4,000 TOC23-20 TOC23-40 TOC23-60 TOC23-72
31/2" 41/2" 3,000 TOC25-20 TOC25-40 TOC25-60 TOC25-72
3" 4 / 2"
1
5,000 TOC27-20 TOC27-40 TOC27-60 TOC27-72
4" 5" 3,000 TOC29-20 TOC29-40 TOC29-60 TOC29-72
3 /2"
1
5" 5,000 TOC31-20 TOC31-40 TOC31-60 TOC31-72
O-RING PISTON GASKET
1 1 2
1
2 2

3 3 3
7 1. PRESSURE CONNECTION
2. COVER
9 9
3. CAP
9 4. "O" RING
4 4 5. BODY (BOTH ENDS ALIKE)
6. PISTON
8 7. THRUST RING
5 8. GASKET
9. WEEP HOLE
5 6
5

O-RING PISTON GASKET

How To Order Tubular Series Reactors


With O-Ring Closure: With Piston Separators: With Gasket Closure:
Specify catalog number, see ordering Specify catalog number, see ordering table Specify catalog number, see
table above. above and add “(W/Piston)” as suffix. ordering table above and add
Note: Use of Buna-N O-ring limits Because of temperature limitations “W/Gasket)” as suffix.
maximum working temperature pistons are not normally ordered in * Gasket closure is not available
to 250°F. For higher temperatures combination with the gasket closure. on 11/2" O.D. tubing size vessels.
to 800°F, order gasket closure. Example:
TOC15-20 (W/Gasket).

10.11
High Pressure Equipment Company R4 2/02
2955 W. 17th Street • Erie, PA 16505 U.S.A. • Phone: (814) 838-2028 • 1-800-289-7447 • Fax: (814) 838-6075 • Website: [Link]
1295 Full Line Catalog 216.qxp_1069 Full Line Catalog 9/04 3/31/16 11:19 AM Page 119

High Pressure Equipment

Series “MS”
Micro Reactors
The Micro Reactors shown are designed for numerous
applications including small volume testing of components
and miniature scale reaction tests.
Standard material of construction is Type 316 stainless steel.
Operation at temperatures up to 800°F is made possible by
the metal to metal seal construction. Working pressures should
be reduced by approximately 15% at the maximum 800°F
temperature level.
Connections are for 1/4" O.D. high pressure coned and threaded
tubing (HF4). One connection is provided at each end. Other sizes
or types of connections can be provided. Thermocouples can
easily be installed with the use of thermocouple adapters
(refer to section 8.0).

B
I.D. (C)
O.D. (D)

Working (C) (D) (A) (B)


Catalog Pressure Inside Outside Inside Overall
No. Capacity psi Diameter Diameter Depth Length
MS-1 2 mL 4" 7"
MS-2 3 mL 6" 9"
MS-3 4 mL 60,000 3
/
16 " 9
/
16 " 8" 11"
MS-4 5 mL 10" 13"
MS-5 6 mL 12" 15"
MS-11 5 mL 4" 6 1/2"
MS-12 7 1/2 mL 6" 81/2"
MS-13 10 mL 20,000 5
/
16 " 9
/
16 " 8" 101/2"
MS-14 12 1/2 mL 10" 121/2"
MS-15 15 mL 12" 141/2"
MS-16 24 mL 6" 9"
MS-17 41 mL 10" 13"
MS-18 65 mL 20,000 9
/
16 " 1"
16" 19"
MS-19 81 mL 20" 23"

10.12
R1 12/97

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