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SPECTROMAXx

Stationary metal analyzer

Original operating instructions

Table of Contents
1 Description of instrument ................................................................................... 5
1.1 Description ......................................................................................................................... 5
1.2 Function ............................................................................................................................. 5
1.3 Overview ............................................................................................................................ 6
1.3.1 Instrument (front) .................................................................................................. 6
1.3.2 Unit (left side) ........................................................................................................ 7
1.3.3 Instrument (right-hand side) .................................................................................. 8
1.3.4 Instrument (back) .................................................................................................. 9
1.3.5 Spark stand......................................................................................................... 10
1.3.6 Spark stand insert ............................................................................................... 11

2 Safety .............................................................................................................. 12
2.1 Symbols used................................................................................................................... 12
2.2 User information ............................................................................................................... 14
2.3 Intended use .................................................................................................................... 15
2.3.1 Samples .............................................................................................................. 15
2.3.2 Preparing the Sample ......................................................................................... 15
2.3.3 Sample material .................................................................................................. 16
2.3.4 Sample weight .................................................................................................... 17
2.3.5 Gas cleaning cartridge ........................................................................................ 17
2.3.6 Spark stand......................................................................................................... 17
2.3.7 Sample clamp ..................................................................................................... 18
2.3.8 Gas supply .......................................................................................................... 19
2.4 Prohibited operating conditions ........................................................................................ 19
2.5 Residual risks ................................................................................................................... 20

3 Technical data ................................................................................................. 22

4 Transportation/Setting-up ................................................................................ 24
4.1 Space requirements ......................................................................................................... 25
4.2 Storage ............................................................................................................................ 25
4.3 Gas supply ....................................................................................................................... 26

5 Initial start-up ................................................................................................... 27

5.1 Preparing the instrument for use ...................................................................................... 27

6 Operation ......................................................................................................... 28
6.1 Overview of controls......................................................................................................... 28
6.2 Switching on the instrument ............................................................................................. 29
6.2.1 Argon saving module .......................................................................................... 29
6.3 Switching off the instrument ............................................................................................. 30
6.4 Measuring procedure ....................................................................................................... 31
6.4.1 Preparing the measuring procedure.................................................................... 32
• iCALising the measuring device (iCAL)............................................................... 33

SPECTROMAXx — 22.07.2021 —3
 • Changing the base (multi-base instruments only) ...............................................33
6.4.2 Start the measurement........................................................................................34

7 Maintenance ................................................................................................... 35
7.1 Maintenance Reminder ....................................................................................................35
7.2 Maintenance schedule .....................................................................................................36
7.3 Cleaning the UV optics light inlet window .........................................................................37
7.4 Cleaning the UV optics light inlet window .........................................................................39
7.5 Cleaning the spark stand..................................................................................................42
7.6 Exhaust filter system - Change filter insert .......................................................................47
7.7 Exhaust filter system - Inspecting the gas-washing bottle ................................................49
7.8 Replacing the filter mats ...................................................................................................51
7.8.1 Housing of air filter ..............................................................................................51
7.8.2 Optic air filter .......................................................................................................52
7.9 Replacing the ICALization sample....................................................................................53

8 Status messages ............................................................................................ 54

9 Troubleshooting .............................................................................................. 55
9.1 Error messages ................................................................................................................57
9.2 Diagnosis tool...................................................................................................................58

10 Spare parts and consumables ......................................................................... 59

11 De-commissioning........................................................................................... 59

12 Manufacturer address ..................................................................................... 59

—4 SPECTROMAXx — 22.07.2021
 Description of instrument

1 Description of instrument

1.1 Description
Instrument: SPECTROMAXx
Model: LMX09
Type/Part No.: 76004145

1.2 Function
Sample material is evaporated by spark discharge inside the unit. In this process,
the released atoms and ions are excited and emit light. This light is directed into
the optical systems and measured using sensors.
Calibration data are already stored in the unit's memory. The measured values are
compared with these data. The measured values are converted into
concentrations and then displayed on the screen.

SPECTROMAXx — 22.07.2021 —5
Description of instrument

1.3 Overview

1.3.1 Instrument (front)

Benchtop instrument Floor instrument

Fig. 1

No. Component No. Component

1 PC data transmission socket 4 Spark stand

2 Argon connection 5 Gas-washing bottle and filter bottle

3 PC 6 Air filter

—6 SPECTROMAXx — 22.07.2021
 Description of instrument

1.3.2 Unit (left side)

Fig. 2

No. Component No. Component

1 Optic room filter mat 4 On/Off switch spark excitation

(plasma generator)
2 Unlocking mechanism for
protective cover 5 Sample clamp

3 Start/Stop measurement

SPECTROMAXx — 22.07.2021 —7
Description of instrument

1.3.3 Instrument (right-hand side)

Fig. 3

No. Component No. Component

1 Sample clamp 4 Unlocking mechanism for

protective cover

2 Start/Stop measurement 5 Filter mat housing

3 On/Off switch spark excitation 6 Main switch

(plasma generator)
7 Access to exhaust filter system
(gas-washing bottle and filter
bottle)

—8 SPECTROMAXx — 22.07.2021
 Description of instrument

1.3.4 Instrument (back)

Fig. 4

No. Component No. Component

1 Power connection socket 3 Argon connection

2 PC data transmission connection

SPECTROMAXx — 22.07.2021 —9
Description of instrument

1.3.5 Spark stand

Fig. 5

No. Component No. Component

1 Replaceable window 6 Spark stand plate

(in the light channel to the UV
7 Holder for fiber-optics to air optics
optics)
2 Clamp (swinging) 8 Locking wheel for contact

3 Contact (movable) 9 Outlet to filter system

4 Electrode and spark stand insert 10 Heat sink

(below the spark stand plate)
11 Electrode holder

5 Spacer

— 10 SPECTROMAXx — 22.07.2021
 Description of instrument

1.3.6 Spark stand insert

Fig. 6

No. Component No. Component

1 Air optics light channel 4 Electrode

2 Spark stand insert 5 Argon outlet

3 UV optics light channel

SPECTROMAXx — 22.07.2021 — 11
Safety

2 Safety
Every user of the instrument must have read and understood these operating
instructions. This applies in particular to the safety instructions.

2.1 Symbols used

The following symbols are used in these abbreviated operating instructions and/or
on the instrument.
If required, additional important information is available in connection with these
symbols.

General warning sign!

Warning of hazardous voltage!

Warning! Flammable substances!

Warning! Hot surface!

Warning! Toxic substances!

Warning! Optical radiation!

Warning of hand injury!

Warning! Risk of suffocation!

— 12 SPECTROMAXx — 22.07.2021
 Safety

Notice!
This sign warns of activities or conditions that may adversely affect the function of
the instrument.

Information
Displays information that is important for the correct and safe use of the
instrument.

SPECTROMAXx — 22.07.2021 — 13
Safety

2.2 User information

 Non-compliance with the operating and safety instructions may lead to injuries
and can cause a health hazard.
 Carefully read the manual and always comply with the safety instructions.
 If the instrument is located on an incline and equipped with castors, it can roll
away during operation. Secure the instrument for operation.
 Only service personnel authorized by the manufacturer are permitted to
unpack, install, set up, and connect the instrument.
 The instrument must only be connected to the power supply with a protective
grounding conductor. The instrument must be operated only in a dry
environment (protection class IP 20, DIN 60529).
 Disconnect the power plug before opening the instrument. The instrument is
only completely disconnected from power if the power plug is removed.
 Never tamper with the safety devices! If it is suspected that a safety device
does not work properly, shut down the instrument immediately. Please
contact your Service Center.
 Compliance with the information labels on the instrument is mandatory.
 While operating and maintaining the instrument, compliance with all safety
instructions and accident prevention regulations is mandatory.
 Compliance with the relevant safety regulations for the use of auxiliary aids
and operating equipment is mandatory.
 Carry out only those maintenance tasks that are described in the chapter
“Maintenance” of the operating instructions. The operating personnel are not
permitted to perform any other maintenance work. Any further maintenance
work (e.g. technical maintenance) or repairs must only be performed by
service personnel authorized by the instrument manufacturer.
 Check the protective measures after every technical maintenance or repair
activity. The checking procedure is carried out in accordance with DGUV V3
(German Social Accident Insurance) or an equivalent national regulation.
 Compliance with the maintenance schedule specified by the manufacturer
and the recording of all maintenance activities is mandatory. This helps
maintain the operational safety of the instrument.
 Only genuine spare parts must be used when repairing the instrument. If
using components other than OME parts, the CE Declaration of Conformity
shall be null and void.

— 14 SPECTROMAXx — 22.07.2021
 Safety

2.3 Intended use

This instrument analyzes and identifies metals. Only such metals may be analyzed
for which the instrument has been calibrated by the manufacturer or by qualified
technical personnel.
Only the original accessories supplied with the instrument must be used and shall
only be used indoors (laboratory environment).
The instrument is intended for use in the industrial sector. Electromagnetic
interference may occur during the operation of the instrument. In this case, the
manufacturer must be contacted.

2.3.1 Samples
Only dry metal samples must be measured.

Warning! Risk of injury and health hazard!

Risk of injury and health hazard due to pressurized or combustible samples.
 Pressurized or flammable samples must not be measured.

2.3.2 Preparing the Sample

Warning! Harmful and toxic substances!

During the preparation of samples, e.g. during the grinding process, toxic vapors
and toxic clouds of dusts may be generated, depending on the sample material.
 When disposing of these dusts, compliance with legal regulations and fire
prevention instructions is mandatory.
 The operating company of the spectrometer shall be responsible for
compliance with the limit values of the maximum permissible pollutant
concentrations in the breathing air.
 During the preparation, compliance with the safety instructions provided by
the manufacturer of the sample preparation machine is mandatory. Personal
protective equipment must be worn.
When preparing samples that could potentially release toxic substances,
wearing protective goggles and the use of appropriate respiratory protection
equipment is mandatory.

SPECTROMAXx — 22.07.2021 — 15
Safety

2.3.3 Sample material

Warning! Toxic substances!

 The sparking process produces a black precipitate (metal condensate). The
condensate could be toxic or flammable, depending on the sample material.
Metal vapors may be generated by sparks of the sample material. Depending
on the sample material, these vapors may be toxic, e.g. if using heavy metals
or other hazardous metals during the test.
 Protective gloves and safety goggles must always be worn when
cleaning the spark stand and when cleaning the gas-washing bottle or
the filter bottle. This also applies when replacing the filter insert. If metals
with toxic components have been sparked off, wearing a breathing mask
to prevent the inhalation of condensate particles is mandatory.
 When disposing of the condensate, compliance with legal regulations
and fire prevention instructions is mandatory.
 If the samples contain toxic substances, an extraction system must be
installed at the spark stand.
 In this case, the gas escaping from the spectrometer's exhaust pipe must
be channeled to the outside of the building.
 The installation of an extraction system and the discharge of the exhaust
gas into the open air makes it easier to comply with the maximum
permissible pollutant concentrations in the breathing air below the
applicable limit values, MAK values (Maximale Arbeitsplatzkonzentration:
maximum workplace concentration) or comparable national regulations.
Compliance with these limits is the sole responsibility of the owner of the
spectrometer. If samples with toxic components must be measured,
further protective actions such as wearing breathing protection may be
necessary.

— 16 SPECTROMAXx — 22.07.2021
 Safety

2.3.4 Sample weight

The weight of the sample to be measured must not exceed 15 kg (33 lbs).

2.3.5 Gas cleaning cartridge

The instrument contains a gas cleaning cartridge.
Only a qualified technician shall be permitted to change the gas cleaning cartridge.

Warning! Toxic substances!

The content of the gas cleaning cartridge is toxic.
 Compliance with the safety data sheet is mandatory. To request the data
sheet, go to [Link]

2.3.6 Spark stand

The opening of the spark stand plate must be completely covered by the sample
or the respective adapter.

Warning! Optical radiation!

The plasma in the spark stand generates UV radiation. UV radiation may cause
damage to the eyes or skin.
 For samples that do not completely cover the spark stand opening, use the
respective sample adapters in such a way that the opening is completely
closed.
 Take appropriate protective measures (e.g. wear safety goggles) when the
spark stand opening is not fully covered.

When maintaining the spark stand, compliance with the following information is
mandatory:

Warning! Flammable substances!

 Do not vacuum the spark stand. The condensate could ignite an unsuitable
vacuum cleaner.
 The exhaust filter of the vacuum cleaner may not be suitable for the pore size
of the condensate.

SPECTROMAXx — 22.07.2021 — 17
Safety

2.3.7 Sample clamp

The sample clamp must have contact with the sample (the function circuit of the
spark stand is closed).

Warning! High voltage!

The sample clamp provides the contact between the sample and the spark stand.
There is a risk of suffering an electric shock when handling the sample clamp.
 Never tamper with the sample clamp.

Warning! Risk of hand injury!

Springs are used to keep the sample clamp in position. However, the clamp may
fold down unexpectedly. If your hand is caught underneath the clamp, this may
cause injuries.
 Never place your hand under the sample clamp.

— 18 SPECTROMAXx — 22.07.2021
 Safety

2.3.8 Gas supply

Information! Measurement errors!

Impurities in the argon supply cause measuring errors.
 Ensure the installation of the argon supply line is free of oil and grease.
Only argon must be used when operating the instrument.

Argon quality (min.) 4.8 (99.998% Ar) with O2<3ppm, N2<10ppm,

H2O<5ppm, kV<1ppm
Argon of higher purity or gas pre-purification is
required for a nitrogen/oxygen analysis.

The spectrometer requires an argon supply line.

A suitable pressure reducer is required for the argon supply (bottles or liquid gas
tank).
 Adjustable output pressure 0 - 10 bar
 The argon inlet pressure at the instrument is 4.8 – 5.0 bar (69.6 – 72.5 psi)

2.4 Prohibited operating conditions

Do not operate the instrument if one of the following conditions exists:
 If the instrument is faulty or damaged.
 If the ambient conditions do not comply with the specification.
 If the area where the instrument is used is not a commercial/industrial
premise.

SPECTROMAXx — 22.07.2021 — 19
Safety

2.5 Residual risks

This instrument has been manufactured in accordance with the latest state-of-the-
art technology. Residual risks cannot be completely excluded, however.

General warning sign!

 The light inlet window of the air optics is located at side of the spark stand.
 Protective gloves must be worn to prevent cuts and contact with metal
condensate, which can be toxic, depending on the sparked material.
 The instrument is operated with argon. Argon is heavier than air. It can
accumulate in a closed room, especially on the floor or lower-lying areas.
 Ensure that adequate ventilation is provided. If necessary, install oxygen
sensors.

Warning of hazardous voltage!

When the instrument is switched on, there is a risk of an electric shock when the
electrode is touched or when the sample is removed during a measurement.
 Never touch the sample while a measurement is in progress.
 Avoid any contact with the electrode if the excitation is activated (plasma
generator).
 Shut down the plasma generator when working on the spark stand.

Warning! Hot surface!

 Contacting the electrode increases the risk of burn injuries. During normal
operation, the electrode will heat up to several hundred degrees.
 Never touch the electrode with your bare hands, even after shutting
down the spectrometer. Always use pliers.
 A sample can get hot if it is measured several times.
 Touch the sample only after it has sufficiently cooled.

Warning! Risk of suffocation!

 The instrument is operated with argon. Argon is heavier than air. It can
accumulate in a closed room, especially on the floor or lower-lying areas.
 Ensure that adequate ventilation is provided. If necessary, install oxygen
sensors.

— 20 SPECTROMAXx — 22.07.2021
 Safety

Information
A high-voltage pulse ignites the plasma. Subsequently, the burning voltage is
applied to the electrode.

When the instrument is switched on, there is an inherent danger of an electrical

emission during a spark test, especially if the sample is removed during the
measuring process.
 For a healthy person, this electrical transmission is of no concern. These are
electromagnetic fields of low intensity. Due to this transmission, the
electromagnetic characteristics of the instrument may be outside the limits of
EN61326-1 in some areas. As a result, interferences of radio transmissions
can occur in the immediate (close) range of the spectrometer. This means, for
example, interference during the reception of radio transmissions is possible
(crackling, image disturbances).
 Users of life-sustaining or supporting medical devices (e.g., insulin pumps,
pacemakers, defibrillators, EEG, ECG devices, etc.) should not be affected by
CE-compliant instruments. For this group of operators, however, it is strongly
recommended to contact the manufacturer of the instrument before using the
spectrometer!

SPECTROMAXx — 22.07.2021 — 21
Technical data

3 Technical data
Description Value

Instrument height Benchtop instrument: 450 mm; 17.7"

Floor instrument: 1350 mm; 53.1"

Instrument width Benchtop instrument: 660 mm; 26"

Floor instrument: 660 mm; 26"

Instrument depth Benchtop instrument: 790 mm; 31.1"

Floor instrument: 790 mm; 31.1"

Instrument weight Benchtop instrument: approx. 74 kg; ~ 163 lbs

Floor instrument: approx. 125 kg; ~ 276 lbs

Power supply 90 - 253 VAC, 50/60 Hz

Power during measurement 600 VA

Power during stand-by 180 VA

Supply voltage fuse 16 A (B)

Operating range (permissible ambient 10°C – 30°C; 50°F – 86°F

temperature)

Recommended temperature range to 18°C – 28°C; 64°F – 82°F

achieve the specified performance

Place of installation Inside of dry, dust-free rooms up to an altitude of

2000 m above sea level, vibration-free (not
subject to impact or vibration load conditions)

Air humidity range 20 – 80%, not condensing

Sound pressure level 55 dB(A)

— 22 SPECTROMAXx — 22.07.2021
 Technical data

Description Value

Argon inlet pressure on the instrument 4.8 to 5.0 bar (69.6 to 72.5 psi)

Argon quality (min.) 4.8 (99.998% Ar) with O2<3 ppm, N2<10 ppm,
H2O <5 ppm, kV<1 ppm
Argon of higher purity or gas pre-purification is
required for a nitrogen/oxygen analysis.

Argon flow rates Constant flow 9 l/h

Analytic flow 200 l/h

Storage conditions Ambient temperature

-15°C – 45°C; +5°F – +113°F

Protection class / Contamination class IP 20 (DIN 60529), contamination class II

(laboratory environment)

EMC environment Industrial environment / Laboratory environment

SPECTROMAXx — 22.07.2021 — 23
Transportation/Setting-up

4 Transportation/Setting-up
Notice! Damage to instrument!
Improper transport may cause damage to the instrument or to other property within
the surroundings.
 Only specifically trained personnel shall be permitted to transport the
instrument in its transport packaging.
 The properly trained employees have the corresponding instructions at
their disposal.
 If the usage site must be changed, please contact our Service Center.
 Consider the dimensions and the weight of the instrument.
 Ensure that the transportation route is free of obstacles and bottlenecks
are avoided.
 Ensure that the static properties of the transport route and the installation
location correspond to the weight of the unit (approx. 74 kg for the
benchtop or 125 kg for the floor instrument).
 Only service personnel authorized by the manufacturer are permitted to
unpack, install, set up, and connect the instrument.

Information: Measurement errors!

 If the instrument is subject to vibrations and shocks, measurement errors may
occur during the measuring process.
 The instrument must be installed at a vibration- and shock-free location.
 Measurement errors can result from temperature differences inside the
instrument.
 The instrument must be installed at a location, where it cannot heat up or
cool down on one side only.
 The instrument may be operated only in a dry environment (protection class
IP 20, DIN 60529).
Observe the following information regarding the instrument's installation:
 All connections are located at the rear side.
 The instrument must be accessible from all sides for maintenance. Set up the
instrument accordingly. Sufficient space should be provided for the computer
workstation (keyboard, monitor, printer) and the operating personnel.
 The clearance to other objects should be at least 20 cm on all sides. In
addition to the space required by the instrument, some space is needed for
the gas supply, unless fixed gas connections are available.
 In order to disconnect the instrument from the power supply, access to the
main switch of the instrument must be ensured at all times.

— 24 SPECTROMAXx — 22.07.2021
 Transportation/Setting-up

4.1 Space requirements

Floor instrument Benchtop instrument

Fig. 7

4.2 Storage
Storage conditions:
 The instrument must be stored in a dry place
 Room temperature -15°C – +45°C (5°F – 113°F)

SPECTROMAXx — 22.07.2021 — 25
Transportation/Setting-up

4.3 Gas supply

Information: Measurement errors!

Impurities in the argon supply cause measuring errors.
 Ensure the installation of the argon supply line is free of oil and grease.
The spectrometer requires an argon supply line.
A suitable pressure reducer is required for the argon supply (bottles or liquid gas
tank).
 Adjustable output pressure 0 - 10 bar
 The argon inlet pressure at the instrument is 4.8 – 5 bar (69.6 - 72.5 psi)
 The pressure reducer must be adjusted so that the maximum permissible inlet
pressure of the instrument is not exceeded.
A copper tube for the argon supply is provided with the delivery of the SPECTRO:
 Diameter 6 x 1 mm, length 3 m
 When using longer lines and/or smaller tube diameters, a possible
pressure drop must be taken into account.
This line is screwed to the connection on the rear panel of the instrument. The
threaded connection is included in the scope of supply.

— 26 SPECTROMAXx — 22.07.2021
 Initial start-up

5 Initial start-up

5.1 Preparing the instrument for use

Before switching on the instrument, proceed as follows:
1. Check the filling level of the gas-washing bottle. Fill with water if required, see
page 49.
2. Set the argon pressure to 4.8 - 5.0 bar (69.6 - 72.5 psi).
 If the argon pressure is not properly set, turbulences result in the spark
stand insert. Thus, correct measuring results cannot be obtained.
 The instrument is ready for use.

SPECTROMAXx — 22.07.2021 — 27
Operation

6 Operation

6.1 Overview of controls

Fig. 8

No. Control element Function

1 Switch Start/Stop measurement

2 Switch Switches the plasma generator on/off, see chapter 6.2.

— 28 SPECTROMAXx — 22.07.2021
 Operation

6.2 Switching on the instrument

Notice! Damage to instrument!

Only use power cables that are rated for the currents of the instrument.

Information
To operate the instrument in compliance with the specification, it should be
stabilized for at least 2 hours after it has been switched on.
This may take longer because this procedure is dependent on the temperature
during instrument transport and/or storage.
Before proceeding with any other activities, ensure that the operating temperature
of the optical room of 33 °C (91.5 °F) has been reached (see chapter 9.2).
To switch on the instrument, proceed as follows:
1. Connect the instrument to the power supply.
2. Turn the main switch to the “ON” position.
3. In order to switch on the plasma generator, press the following buttons:

4. Switch on the computer.

 The operating system is booted.
5. After booting the operating system, start the “Spark Analyzer Pro MAXx”
spectrometer software.
 The instrument is switched on.

6.2.1 Argon saving module

The argon flow is deactivated by switching off the Plasma generator. This
minimizes the overall argon consumption.
For restoring the readiness for measurements, flushing with the analytic flow is
carried out.
When the argon flow is automatically activated again is determined in the "Argon
saving module" screen dialog. Immediately thereafter, the instrument is ready for
operation.
For a detailed description, refer to the online help of the instrument.

SPECTROMAXx — 22.07.2021 — 29
Operation

6.3 Switching off the instrument

Information
If the instrument was completely switched off, restarting may take some time as
the optics need to reach the right temperature and the system must be flushed with
argon.
It is recommended to leave the instrument connected to the power supply and to
leave the argon supply line open all the time.
To switch off the instrument, proceed as follows:

1. Turn off the plasma generator by pressing the switch.

2. Exit the spectrometer program "Spark Analyzer Pro MAXx".
3. Select the dialog item "Shut down" and confirm the dialog field.
 The program is shut down.
 The computer is turned off.
4. In order to switch off the instrument completely, set the main switch to the
OFF position.
 The instrument is switched off.

— 30 SPECTROMAXx — 22.07.2021
 Operation

6.4 Measuring procedure

Warning of hand injury!

Springs are used to keep the sample clamp in position. However, the clamp may
fold down unexpectedly. If your hand is caught underneath the clamp, this may
cause injuries.
 Never place your hand under the sample clamp.

Warning of hazardous voltage!

The sample clamp provides the contact between the sample and the spark stand.
There is a risk of electric shock when handling the sample clamp.
 Never tamper with the sample clamp.

Warning! Hot surface!

A sample can get hot if it is measured several times.
 Touch the sample only after it has sufficiently cooled.

Warning! Optical radiation!

The plasma in the spark stand generates UV radiation. UV radiation may cause
damage to the eyes or skin.
 For samples that do not completely cover the spark stand opening, use the
respective sample adapters in such a way that the opening is completely
closed.
 Take appropriate protective measures (e.g. wear safety goggles) when the
spark stand opening is not fully covered.

Information
A flawed initial start-up, operation or sample preparation can lead to measurement
errors.
 Therefore, ensure all necessary requirements for a correct measurement are
met.

SPECTROMAXx — 22.07.2021 — 31
Operation

6.4.1 Preparing the measuring procedure

Information
An optimum measurement requires a good argon atmosphere inside the spark
stand. Therefore, the opening of the spark stand must always be covered. This will
make it more difficult for ambient air to enter the spark stand. A flat sample is
highly recommended.
Oxygen and humid air inside the spark stand may result in poor burn spots (see
Chapter 9 „Troubleshooting“).
In order to remove any oxygen that may have penetrated from the spark stand,
use the “Flush” button on the computer to invoke the flush function.
Before starting the measurement, proceed as follows:
1. Ensure that
 the instrument is ICALized, see page 33,
 the correct and base-relevant parts have been installed, see page 33.
2. Check the spark stand and the sample for any moisture.
 It is important that no moisture is visible on the outside.
 If necessary, dry the sample.
3. If working with toxic samples, ensure to verify the safety precautions.
 The measurement is now prepared.

— 32 SPECTROMAXx — 22.07.2021
 Operation

iCALising the measuring device (iCAL)

The iCALising procedure (standardizing using iCal) requires a reference sample.
The average values of these measurement results are calculated and stored in the
instrument.
In order to proceed with iCALization, follow the steps below:
1. Place a clean electrode in the spark stand, see page 44 ff.
2. Start the iCAL function by pressing the “iCAL” button.
3. Follow the instructions on the screen and perform the necessary
measurements with the reference sample.
4. Poor measurements are highlighted in the ICAL measurement window and
can be deleted. Please repeat the respective measurements.
 The instrument is iCALized.

Changing the base (multi-base instruments only)

When changing the base, the spark stand must be cleaned in order to avoid
memory effects, see page 42.
 Change the spark stand insert, the electrode, and the electrode brush.
Preparation of the instrument for measuring another base is now complete.

SPECTROMAXx — 22.07.2021 — 33
Operation

6.4.2 Start the measurement

Information
Use the electrode brush in order clean the electrode tip after each measurement.

To measure the probe, proceed as follows:

1. Start the required measuring program using function key F10.
2. Put the sample in position.
 The sample must fully cover the opening in the spark stand plate.
 The sample clamp must have contact with the sample (the function circuit
of the spark stand is closed).
3. Use the function key F2 or the start/stop button to start the process.
 The measurement is fully automated.
 The measurement is finished automatically.
 The measurement results are displayed on the screen.
4. Perform further measurements as needed.
 Use the electrode brush in order clean the electrode tip after each
measurement.
 Rotate the sample slightly for each further measurement. The respective
burn spots must not overlap.
5. Use "Start" or press the respective function key to start the series of
measurement.
 The measurement process is finished.

— 34 SPECTROMAXx — 22.07.2021
 Maintenance

7 Maintenance
Information
In order to ensure the availability and operational safety of the equipment, we
recommend having the system checked for correct operation and performance at
least once per year by specialized technicians. To find contact addresses of
service organizations authorized by SPECTRO go to [Link]

7.1 Maintenance Reminder

The instrument is equipped with a diagnostic system that will prompt you to
proceed with a variety of maintenance tasks. The intervals between the individual
maintenance tasks are based on certain periods and/or the number of
measurements taken during normal use of the instrument. If the instrument is used
very little or intensively, the respective defaults should be adjusted accordingly.
The following maintenance intervals are monitored.
 General maintenance
 iCALing
 Cleaning the spark stand
 Servicing the argon outlet
 Servicing the air filter

SPECTROMAXx — 22.07.2021 — 35
Maintenance

7.2 Maintenance schedule

Start of work Tasks to be performed

1. Check the argon supply. The min. pressure in the bottle is 10 bar.

2. Diagnosis system - maintenance or Will be specified by the diagnosis system.

check the number of measurements.

3. Check the water level in the gas- Top up/replace, see page 49.
washing bottle.

4. Check the burn spot. Visual inspection.

Measuring procedure Tasks to be performed

Clean the electrode. Use the small wire brush to clean the
electrode after each spark test.

Monthly maintenance work

Change water in gas-washing bottle. See page 49.

Clean the UV optics light inlet window. See page 37

Clean the air optics light inlet window. See page 39.

Clean the filter mats and replace if See page 51.

necessary.

As required

iCALizing the measuring device (iCAL) See page 33.

Replacing the iCALization sample. See page 53

Clean spark stand. See page 42.

Clean/replace the filter insert of the filter See page 47.

bottle.

Replace the filter bottle. As required.

— 36 SPECTROMAXx — 22.07.2021
 Maintenance

7.3 Cleaning the UV optics light inlet window

Warning! High voltage!
When the plasma generator is switched on, there is a risk of electric shock if the
electrode is touched.
 Shut down the plasma generator when working on the spark stand.

To clean the light inlet window, proceed as follows:

1. Turn off the plasma generator.

2. Loosen the two screws (1) of the
light inlet window (2).
3. Remove the light inlet window.
 Direct contact with the
optical surfaces must be
avoided.

Fig. 9
4. Unscrew the fixing ring (3) of the
light entry window (2) using the
auxiliary tool (1).

Fig. 10

Fig. 11

SPECTROMAXx — 22.07.2021 — 37
Maintenance

5. Subsequently, remove the

Teflon ring (1), the light entry
window (2) and the O-ring (3).
6. Clean the light inlet window (2),
using optical paper or a lint-free
soft cloth.
 If the light inlet window is
too dirty, it must be
replaced.

Fig. 12
7. Refit the light inlet window.
 Cleaning of the UV optics light inlet window is now complete.

— 38 SPECTROMAXx — 22.07.2021
 Maintenance

7.4 Cleaning the UV optics light inlet window

Warning! High voltage!

When the plasma generator is switched on, there is a risk of electric shock if the
electrode is touched.
 Shut down the plasma generator when working on the spark stand.

Warning! Toxic substances!

When removing the light entry window, contact with the condensate of the
samples is likely. Depending on the sample material, the condensate may be toxic.
 Protective gloves must be worn.
To clean the light inlet window, proceed as follows:

1. Turn off the Plasma generator

(1).
2. Unscrew the 4 fasteners (2) and
remove the spark stand plate
(3).

Fig. 13
3. Remove the spacer (1) from the
spark stand.

Fig. 14

SPECTROMAXx — 22.07.2021 — 39
Maintenance

4. Unlock the cover (1) by pressing

both buttons (2) simultaneously.
5. Remove the cover (1).

Fig. 15
6. Loosen the union nut (1).

Fig. 16
7. Remove the fiber optic holder
(1) from the spark stand.
8. Loosen the window holder (2)
from the spark stand.
 The quartz window is
located between the holder
and the O-ring.
Direct contact with the optical
surfaces must be avoided!

Fig. 17
9. Clean the light inlet window (1),
using optical paper or a lint-free
soft cloth.
 If the light inlet window is
too dirty, it must be
replaced.

Fig. 18

— 40 SPECTROMAXx — 22.07.2021
 Maintenance

10. Clean the light channel (1) with

a grease-free cloth or a bottle
brush with plastic bristles.

Fig. 19
11. If necessary, use a grease-free
cloth to clean the O-ring (1).

Fig. 20
12. Reassemble components in reverse order.
 Cleaning of the air optics light inlet window is now complete.

SPECTROMAXx — 22.07.2021 — 41
Maintenance

7.5 Cleaning the spark stand

Warning! High voltage!

When the plasma generator is switched on, there is a risk of electric shock if the
electrode is touched.
 Shut down the plasma generator when working on the spark stand.

Warning! Toxic substances!

The sparking process produces a black precipitate (metal condensate). The
condensate could be toxic or flammable, depending on the sample material.
 Protective gloves and safety goggles must always be worn when cleaning the
spark stand and when cleaning the gas-washing bottle or the filter bottle. This
also applies when replacing the filter insert. If metals with toxic components
have been sparked off, wearing a breathing mask to prevent the inhalation of
condensate particles is mandatory.
 When disposing of the condensate, compliance with legal regulations is
mandatory.

Warning! Hot surface!

Contacting the electrode increases the risk of burn injuries. During normal
operation, the electrode will heat up to several hundred degrees.
 Never touch the electrode with your bare hands, even after shutting down the
spectrometer. Always use pliers.

Warning! Flammable substances!

 Do not vacuum the spark stand. The condensate could ignite an unsuitable
vacuum cleaner.
 The exhaust filter of the vacuum cleaner may not be suitable for the pore size
of the condensate.

— 42 SPECTROMAXx — 22.07.2021
 Maintenance

Notice! Instrument damaged or malfunction!

Incorrect cleaning of the spark stand increases the risk of damage to the
instrument or malfunctions during measurements.
Please observe the following rules during cleaning:
 Only use a clean, dry and soft cloth to clean the spark stand.
 To clean holes in the spark stand, also use a clean, dry and soft cloth or a
bottle brush with plastic bristles.
 Do not use solvents to clean the spark stand. Solvent residues can adversely
affect the function of the spectrometer.
 Do not use compressed air (or similar methods) to clean the spark stand. The
use of compressed air could cause the condensate to ignite and/or spread
inside the laboratory.
 Do not vacuum the spark stand. The condensate could ignite an unsuitable
vacuum cleaner. The exhaust filter of the vacuum cleaner may not be suitable
for the pore size of the condensate.

The sparking process soils the spark stand with a black precipitate (metal
condensate). This metal condensate may create a conductive connection between
the electrode and the metal structure of the spark stand wall.

To clean the spark stand, proceed as follows:

1. Turn off the Plasma generator

(1).
2. Unscrew the 4 fasteners (2) and
remove the spark stand plate
(3).

Fig. 21

SPECTROMAXx — 22.07.2021 — 43
Maintenance

3. Use a dry, grease-free cloth to

clean both sides of the spark
stand plate (1).
4. Remove and clean the O-ring
(2) of the spark stand plate.

Fig. 22
5. To remove the electrode (1),
unscrew the spacer (2). Behind
the plug there is a through hole
in order to reach the fixing screw
of the electrode.

Fig. 23
6. Loosen the fixing screw of the
electrode (1), using the Allen
key (AF 2.5) until the electrode
can be removed.
 When loosening the
electrode, hold firmly on to
it. After loosening the
screw, a spring presses the
screw upward. Loosen the
screw only until the
electrode can be removed
easily.
7. Remove and clean the
Fig. 24
electrode.
 If the electrode is worn, it
must be replaced.

— 44 SPECTROMAXx — 22.07.2021
 Maintenance

8. Remove the spark stand insert

(1). Use a dry, grease-free cloth
to clean the insert.

Fig. 25
9. Use a dry, grease-free cloth to
clean the surface of the spark
stand body.
10. Use a dry, grease-free cloth or a
bottle brush with plastic bristles
to clean the light channel (1).

Fig. 26
11. Install the spark stand insert (1).
 Use two fitted pins (3) in
order to center the spark
stand insert.
 Ensure that the spark stand
insert is flush with the top
edge (2) of the spark stand.

Fig. 27

SPECTROMAXx — 22.07.2021 — 45
Maintenance

12. Install the spark stand plate (1).

13. Insert the electrode (2) into the
spark stand opening.

Fig. 28
14. Use the setting gage (1) in order
to align the electrode.
 Press the setting gage with
the 3.4 mm shoulder into
the spark stand opening
and at the same time use
the Allen key (AF 2.5) to
tighten the electrode screw.

Fig. 29
15. Screw the setting gage (1) back
into the spark stand.

 The spark stand is now cleaned.

Fig. 30

— 46 SPECTROMAXx — 22.07.2021
 Maintenance

7.6 Exhaust filter system - Change filter insert

Warning! Toxic or flammable substances!

The sparking process produces a black precipitate (metal condensate). The
condensate could be toxic or flammable, depending on the sample material.
 Protective gloves and safety goggles must always be worn when cleaning the
spark stand and when cleaning the gas-washing bottle or the filter bottle. This
also applies when replacing the filter insert. If metals with toxic components
have been sparked off, wearing a breathing mask to prevent the inhalation of
condensate particles is mandatory.
 When disposing of the condensate and the used filters, compliance with legal
regulations is mandatory.
To replace the filter cartridge, proceed as follows:

1. Floor instrument:
Open the door on the right side of
the instrument.
Benchtop instrument:
Turn the opening of the filter
cartridge container to the front.
2. Hold the filter cartridge (1) with
both hands and unscrew it.
3. Remove the filter insert (2).

Fig. 31

SPECTROMAXx — 22.07.2021 — 47
Maintenance

4. Insert the new filter and screw

the filter container back into the
holder.
 Ensure that the O-ring (1) is
clean and sits inside the
groove. If necessary, use a
clean cloth to clean the O-
ring.
 The filter container should
only be tightened by hand.
 The filter bottle screws in
easily. If not, the filter insert
is not positioned correctly.

 Now, the filter cartridge is replaced.

— 48 SPECTROMAXx — 22.07.2021
 Maintenance

7.7 Exhaust filter system - Inspecting the gas-washing bottle

Warning! Toxic or flammable substances!

The sparking process produces a black precipitate (metal condensate). The
condensate could be toxic or flammable, depending on the sample material.
 Protective gloves and safety goggles must always be worn when cleaning the
spark stand and when cleaning the gas-washing bottle or the filter bottle. This
also applies when replacing the filter insert.
 When disposing of the condensate and the used filters, compliance with legal
regulations is mandatory.
In order to inspect the gas-washing bottle, proceed as follows:

1. Floor instrument:
Open the right door of the instrument.
Benchtop instrument:
Turn the opening of the filter cartridge container to the front.

2. Check the water level inside the

filter cartridge.
 The gas-washing bottle must
be filled half with water (see
marking on the gas-washing
bottle).
 The water must be clean.

Fig. 32
3. In order to refill water, use both hands to hold the filter cartridge and unscrew
it.
4. Refill water or change it as required.

SPECTROMAXx — 22.07.2021 — 49
Maintenance

5. Make sure that the O-ring (1)

sits in the groove and is clean. If
necessary, use a clean cloth to
clean the O-ring.
6. Screw the gas-washing bottle
back manually.

 The water is checked/changed.

Fig. 33

— 50 SPECTROMAXx — 22.07.2021
 Maintenance

7.8 Replacing the filter mats

7.8.1 Housing of air filter

The air filter’s housing is located on the right-hand side of the instrument. To
replace the filter mat, proceed as follows:

1. Remove both fixing screws of the

applicable filter retainer bracket
(1).
2. Remove the relevant cover (2).

Fig. 34
3. Remove the filter mat (1).

Fig. 35
4. Install the new filter mat.
5. Reinstall the relevant cover.
 The housing of the air filter is replaced.

SPECTROMAXx — 22.07.2021 — 51
Maintenance

7.8.2 Optic air filter

The filter mat of the optic air filter is located on the left-hand side panel of the
instrument.
In order to clean or replace the air filter mat, proceed as follows:

1. Loosen the two cross-head screw

(1).
2. Remove the cover (2).

Fig. 36
3. Remove the filter mat (1).

Fig. 37
4. Install the new filter mat.
5. Tighten the screws.
6. Install the cover.
 The optic air filter is cleaned / replaced.

— 52 SPECTROMAXx — 22.07.2021
 Maintenance

7.9 Replacing the ICALization sample

When the ICALizing sample is almost used up, a replacement must be provided.
The composition of the ICALizing sample is different from that of the original
samples. The intensities of the new samples must be matched to those of the old
samples.
Please contact your Service Center.

Information
Do not discard the old ICALization sample before the intensities have been
matched. Matching is not possible without using the old samples.

SPECTROMAXx — 22.07.2021 — 53
Status messages

8 Status messages
The status information is displayed in the footer of the software. These indications
provide important information about the status of the instrument.
The following information is available:

Status information Description

Ready The instrument is ready for measurement if

all specifications according chapter 6.4.1
"Preparing the measuring procedure" on
page 32 have been met.

Optic room’s temperature Is shown in red as soon as the temperature

of the instrument is outside the optic’s room
temperature range.

Sample Clamp up The sample clamp is not folded down or a

conductive contact with the sample has not
been established.

Safety check required The functional circuit between the sample

and the spark stand is tested. Briefly lift
sample clamp in order to interrupt the
contact to the sample.

— 54 SPECTROMAXx — 22.07.2021
 Troubleshooting

9 Troubleshooting
Malfunction Cause Remedy

The instrument cannot be The power plug is not Check if the power plug was
switched on. plugged in properly. properly plugged in.

Power is not available. Check the power supply.

Main switch on OFF Turn the main switch to the “ON”

position. position.

The burn spot is The argon outlet (exhaust) Clean the spark stand including
incorrect. is clogged with the argon outlet.
condensate.

Insufficient argon supply. Check argon supply and

pressure.

Poor argon quality. Connect new argon;

specifications, see page 22

Incorrect electrode gap. Clean the electrode and re-adjust

the gap using the spacer.

Plasma generator faulty. Please contact your Service

Center.

The samples have not Prepare sample properly, (grind,

been prepared properly. turn or mill).
The sample surface is not
flat enough.

SPECTROMAXx — 22.07.2021 — 55
Troubleshooting

Malfunction Cause Remedy

Low intensities in UV Light inlet window soiled. Clean light inlet window if
optics. required, see page 39.

Light entrance lens is Please contact your Service

soiled. Center.

Shutter blocked. Check shutter function, call the

Service Center if required

Low transmission. Use argon to rinse the optics

(function “Rinse” or the
corresponding function key)

Low intensities in the air Light inlet window soiled. Clean light inlet window if
optics. required, see page 39.

Limit values are not Insufficient intensity. 1. Check argon.

maintained during 2. Check sample.
iCALising.
3. Clean spark stand, adjust
electrode.
4. Clean light inlet window.
5. ICALize the instrument again
and, if necessary, contact the
Service Center.

Intensities too high. 1. Check the shutter function.

2. Check the plasma generator
parameters, contact the
Service Center if necessary.

— 56 SPECTROMAXx — 22.07.2021
 Troubleshooting

9.1 Error messages

Error Cause Remedy

When starting the “Spark Communication Exit the “Spark Analyzer Pro
Analyzer Pro MAXx” MAXx” software.
software, the instrument Disconnected the
switches into DEMO mode. spectrometer from the power
for a short time. After a
waiting period of approx. 60
sec., restart the “Spark
Analyzer Pro MAXx”
software.

The connection between the Connect the spectrometer

PC and the spectrometer is and the PC with the network
interrupted. cable.

Instrument without power. Check the power supply.

Safety check is required. Function circuit between Acknowledge the message.

sample and spark stand has Move the clamp up for
not been activated within the approx. 1 second.
last 5 minutes.

An error has occurred whilst Plasma generator is not Switch on the Plasma
attempting to access the switched on. generator.
spectrometer (Plasma Confirm by pressing “OK”.
generator is switched off,
measurement could not be Insufficient argon supply. Check the argon supply:
started). Pre-pressure (4.8 – 5.0 bar
Check the condition of the (69.6 – 72.5 psi)) and
spectrometer. available quantity.

An error has occurred during The function circuit between The function circuit "Clamp –
spectrometer access (clamp sample and spark stand is Sample – Spark stand" is
up, measurement could not not closed. not closed. Ensure electric
be started). Check the contact is provided.
condition of the
spectrometer.

SPECTROMAXx — 22.07.2021 — 57
Troubleshooting

9.2 Diagnosis tool

An LED symbol in the status bar permanently indicates the general status of the
instrument.
To open the diagnostic system, click the green or red LED symbol in the lower
right-hand corner of the status bar.

Fig. 38

When the instrument is ready for operation, the green LED symbol is lit. If an error
occurs, the LED symbol changes to red. For a detailed description, refer to the
online help of the instrument.

— 58 SPECTROMAXx — 22.07.2021
 Spare parts and consumables

10 Spare parts and consumables

You can find the spare parts and consumables for this instrument under "Support -
Parts Catalogue" (Service – Parts Catalogue) on our website at [Link].

11 De-commissioning
Only organizations or persons authorized by the instrument manufacturer shall be
permitted to de-commission the instrument. Please contact your Service Center.

12 Manufacturer address
SPECTRO Analytical Instruments GmbH
Boschstr. 10
D-47533 Kleve
Germany
Tel.: +49.2821.8 92-0
Fax: +49.2821.8 92-22 00
[Link]

SPECTROMAXx — 22.07.2021 — 59