Drying Rate Curve Calcium Carbonate
AIM
To dry calcium carbonate slurry and plot the rate of drying Curve. Calculate
EMC of calcium carbonate for the given drying conditions.
OBSERVATIONS AND CALCULATIONS
1. Weight of empty stainless steel plate, WË 51.7g
2. Weight of stainless stecl plate + sample slurry, w; 44
3. Weight of the sample slurry, w; = w) - W, 31.3ig
4. 45 g of sample slurry contains 15 g of calcium carbonate
W3g of sample slurry contains ? g of calcium carbonate
15 x W3
= WAg of calcium carbonate 43
45
5. Weight of total water content (TWC), ws = (W3- W4) =248 g
6. Diameter of stainless steel plate, d=Ocm
7. Radius of stainless steel plate, r = (d/2) = 5 Cm
8. Area of stainless steel plate, A = n=135 cm
9. Moisture content removed from the sample = w) - last weight of steel plate
taken with sample+ water (if any)
10. EMC=Total water content (ws g) FMC (Column 3initial -Column 3fina)
24 88 8 - 22.31 2.5| 9
57
Pharmaceut:alEnyinceringby Dr. ) Thimsetty
LiboratoyHandkook of
TABLE 8-1A
Carbonate
Drying Rate of Caleium
Weight of
water
Weight of steel Weight of Free remained
plate + wt. of calcium moisture
SI
Drying carbonate + Content
(present)/gram
time calcium
No. w. of water ofdrypowder
carbonate+ wt. of (g)
(minute) (g/g)
water (g) (8)
(5) (6)
(4)
(1) (2) (3) (4) W (5)/W4
(3) Wi
37.3| 24.88
1 4. 48
q0 4) 33- 24 2048| I,27
2 I5 "83
8543 2 . 26
3 30 |.02
25.22
4 45 7.88 O63
60 7748 20.3)
75 72.53 (S 36 2.43
O,2
6
15,05 2562
7 90
72.2| l4. 49
105 25|
9 120 72| l4.43
TABLE 8-1B
Carbonate
Drying Rate of Calcium
Rate of drying per
Drying in the Rate of drying hour per gram per
S. Drying time, time interval, perhour surface area exposed
No. (minute) (g/g min) (g'g hr) (glghrcm')
(8) (9)
(1) (2) (7)
bin:)-b(n) (7) x 60 (8)/A
(2),-(2):
1
O,0 22 "32
2
30
0,o26
3
4 45
60
|.S6
|S6
6
7 90
105 O.o006
120
cal un cabonate
REPORT "
and dyng
ve
ate calum cabonate at 6o c
"EMc
58
Dyig ate ve
Date:o7o3 2o 24
24
23
stalei
22
21
20
19
18
17
16
15
14
13
12
11
10
4 G.005
5 6 7 8 10 11 12 13 14 15 16 17 18
1 2 3 4