Compost Quality Specifications Guide
Compost Quality Specifications Guide
Odor Smells like rich humus from the forest floor; no ammonia or anaerobic odor.
Sulfide 0 PPM
Ammonium 0 or trace
pH 6.5-8.5
Compost Maturity >50% on Maturity Index at dilution rate appropriate for compost application.
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COMPOST SPECIFICATIONS
There are many chemical and biological measurements used to assess quality. A list of some common measurements and comments on these
measurements are given below.
Chemical Measurements
Measurement Comments
pH and alkalinity pH plays a large role in the availability of plant nutrients. A basic pH can reduce phosphorous, manganese, and zinc availability,
while an acidic pH can cause potassium, calcium, nitrogen, copper and molybdenum deficiency. An optimal pH value depends on
the system to which compost is to be applied.
A pH< 5 is a good indication that the compost measured is not stable and one which probably contains phytotoxic compounds.
Very little is known about the effect of alkalinity in composts, except that a compost with high alkalinity may help buffer the system
against large pH changes.
cation exchange capacity The CEC is a measure of the exchangeable cations that a compost can absorb. The higher the CEC of a compost, the more
(CEC) exchangeable cations it can hold. The CEC of compost tends to increase as maturity and humic substances increase.
The CEC depends on the pH of the compost, thus care should be taken when comparing the CEC of composts with different pH.
salinity The desired salinity of a compost will vary depending on the application. The salinity of manure composts is usually higher than
composts from yard waste.
The salinity is typically measured by preparing a water-based paste of the compost, thus this measurement is a function of the
dilution ratio of compost to water. Caution should be taken when comparing salinity values of composts where dilution ratios are
unknown or are different.
Carbon to Nitrogen ratio The C/N ratio is a measure of the ratio of the total carbon and nitrogen. This ratio is typically used to assess stability and maturity
(C/N) yet it provides no measure of the biological availability of carbon or nitrogen in a sample. For instance, a compost with a high C/N
where lignin represents a large fraction of the carbon may have the same impact on a system as a compost with a lower C/N
where cellulose represents a large fraction of the carbon.
In general it has been suggested that composts with a large C/N may cause nitrogen immobilization, while composts with a small
C/N may result in ammonia toxicity
heavy metals Measurement of heavy metal concentrations in composts produced at composting facilities may be considered if the source
material has been shown to contain heavy metals. Studies have shown composts to reduce leaching of heavy metals, but
research is still needed to evaluate the extent of irreversibility of this process.
Plant nutrients such as N, P, and K are also commonly measured for composts. The importance of these values will again depend on the desired
application.
Stability
Biological measurements such as stability and plant bioassays are often used to assess the quality of compost. Stability measurements will be mentioned
below. Plant growth and disease suppression bioassays are discussed in other sections of these proceedings.
The stability of a compost is often measured to assess potential phytotoxic affects of compost. Stability has also been used in combination with other
chemical measurements to assess the degree to which composts suppress plant pathogens. A stability measurement is defined here as a measure of the
biological activity within a compost sample which has adequate moisture and oxygen and is not inhibited by high (>50 oC) or low (<20 oC) temperatures. A
stability test essentially allows one to gain insight into the rate of decomposition and thus how a "finished" compost may be measured with respect to raw
or mature composts.
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1. Heat production
This test relies on the fact that aerobic microorganisms decomposing the compost produce heat and the heat produced is proportional to
microbial activity. This test is typically performed by placing the sample in an insulated container with a thermometer. The temperature rise in
the sample is used to assess stability. An important note about this test is that the temperature rise is not only a function the heat generated
from microbial activity, but also on the sample weight and moisture content.
2. Oxygen consumption
This test measures oxygen depletion by microbial activity. The test is usually performed in a controlled-temperature and sealed environment.
The rate of oxygen depletion from the environment and/or the change in oxygen within the environment over a given period of time are used to
assess stability.
3. Pressure change
If a biologically active compost sample is placed in a sealed container along with a solution which absorbs CO2, the pressure in the container
will drop. As oxygen is consumed by aerobic microbes, CO2 is produced; absorbing the CO2 from the gas in the container results in a pressure
drop. Stability can be assessed by measuring the pressure drop in the container over a given period of time.
4. CO2 production
This test measures the CO2 produced by both anaerobic and aerobic microbial activity. The test is performed in a sealed
environment and is usually done with some temperature control. The measured rate of CO2 production and/or the change in CO2
within the environment over a given period of time are used to assess stability.
One issue common to the biological measurements of stability is that sufficient time is needed for the microbes within the compost to recover from the
perturbation associated with material sampling. Most of the techniques listed above require at least two days for the microbial population within the sample
to "adjust" to the new environmental conditions before an accurate assessment of stability can be obtained. The user should be wary of stability tests done
in less than 48 hours.
Records that must be kept by a composting operation to be in compliance with the Nevada requirements and include compost temperature measurements
(temperature history), mixing frequency, and metal and fecal coliform concentrations of the final product. Other measurements often recorded include
oxygen and carbon dioxide concentration, moisture and volatile solids content. These measurements can be very helpful to you in assessing compost
quality.
Temperature
Temperature plays an important role in stability, pathogen (human and plant) destruction and weed seed inactivation. With respect to temperature the
Nevada requirements would include: (1) for an enclosed or within-vessel composting operation, temperatures must equal or exceed 55oC (131oF) for a
period of three days, (2) for a windrow operation, temperatures must equal or exceed 55oC (131oF) for a period of 15 days and the windrow must be
turned at least 5 times during this period, and (3) for an aerated static pile operation, temperatures must equal or exceed 55oC (131oF) for a period of three
days and the compost must be covered with 6-12 inches of insulating material during this period.
Temperatures and temperature histories as required by Nevada are sufficient for both pathogen and weed seed inactivation. This result will only hold
when actions have been taken (such as mixing or enclosing the pile) to ensure all portions of the compost have been exposed to high temperatures. Thus,
the user would want to verify by analysis of temperature histories at several locations in the process that the compost had been exposed to sufficiently
high temperatures.
Some compost piles can reach temperatures as high as 70oC (158oF) if not controlled properly. Temperatures this high can significantly reduce microbial
activity and the rate of decomposition. This can result in an unstable product and one which is potentially phytotoxic. The user would want to verify longer
processing and curing times for a material exposed to temperatures greater than 65oC (150oF) for long periods of time
One common rule of thumb regarding temperature and stability is that if the temperature difference between the compost and ambient air is greater than
10oC (15oF), the compost is still fairly unstable.
Decomposition in composting is performed by both aerobic and anaerobic microorganisms. Aerobic microorganisms are favored because they decompose
organic materials more rapidly than anaerobic organisms and they do not produce the nuisance odors typically associated with composting. Thus, one
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important management strategy in composting is to increase oxygen transfer within the pile. Oxygen transfer can be enhanced by increasing the porosity
(volume fraction of air) and/or by forcing air through the compost. Porosity is increased by the addition of bulking agents, control of moisture and mixing of
the pile. Overmixing, however, can reduce the particle size and subsequently the porosity of the compost.
Studies have shown that biological activity within a composting operation begins to decrease when oxygen concentration drops below 10% (CO2>11%),
and is significantly reduced when the oxygen concentration drops below 3% (CO2>18%). Processes operated with a low oxygen concentration could
produce unstable compost. If records of a composting operation show low oxygen or high CO2 concentrations for long periods of time, the user should
verify that the material was composted and cured for an extended period to ensure the product is stable.
Moisture
The balance of moisture within the process is highly coupled to both temperature and oxygen control. Moisture is required by all organisms, yet too much
moisture will reduce the amount of oxygen supplied to the process. Not enough oxygen will result in anaerobic activity and a decrease in the rate of
decomposition. This decrease could result in an unstable product. Also, a large fraction of the heat generated during the composting process is removed
by evaporative cooling. Significant amounts of water can be lost as a result of this cooling, so moisture management must be a key component to any
composting process.
The moisture content at which moisture becomes limiting to microbial activity and oxygen transport varies among materials. The lower limit of moisture
content is about 35-40% (weight of water x 100/total wet weight) and the upper is about 60-70%. The user would want to verify that if moisture content
went below 35-40% during the process, measures were promptly taken to increase the moisture content. If moisture was never adjusted, the product
could be unstable. If the moisture content of the material went above 60-70%, the user would want to verify that the material was composted longer to
compensate for the reduced oxygen transfer, and thus aerobic microbial activity.
Other issues of importance are feedstocks and how they were processed prior to composting. The importance of these issues depends on how the
compost is to be used. The extent to which contaminates such as glass, metals and lumber scraps are removed from the compost plays a large role in the
quality of the product. The user would want to look closely at the compost for small pieces of plastic and other contaminants prior to accepting delivery
Summary
A good composting facility should be able to provide the user with regulatory records as well as other monitored parameters upon request. Below is a
summary of some questions the end-user would want to answer upon analysis of facility records.
1. Were temperatures sufficiently high to ensure pathogen and weed seed destruction?
The user would check for temperatures greater than 55oC (131oF) at several locations in the pile for:
o 3 days if the process is enclosed or within-vessel
o 15 days if the process is a windrow (also check that the pile was mixed at least five time during the 55oC phase)
o 3 days if the process is an aerated static pile (also check that the pile was insulated)
The user would also want to learn about when temperatures were monitored (time before or after mixing) and the depth at which temperatures
were measured. Temperatures measured before mixing would generally be higher than if measured right after mixing. Temperatures measured
at greater depths in the pile (> 2 ft) would typically be higher than if measured closer to the surface.
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4. How were contaminants removed from the raw material and final product?
The user would request information from the facility operator on actions taken to prevent contaminants including metals, plastics,
glass and waste lumber from entering the process and the methods used to remove contaminants from the process. S/he should
also look at a few batches of compost for contaminants.
(a) Sampling. Representative samples of sewage sludge that is applied to the land, placed on a surface disposal site, or fired in a sewage sludge
incinerator shall be collected and analyzed.
(b) Methods. The materials listed below are incorporated by reference in this part. These incorporations by reference were approved by the Director of the
Federal Register in accordance with 5 U.S.C. 552(a) and 1 CFR part 51. The materials are incorporated as they exist on the date of approval, and notice
of any change in these materials will be published in the Federal Register. They are available for inspection at the Office of Water Docket, room L–102,
U.S. Environmental Protection Agency, 401 M St., SW., Washington, DC, and at the National Archives and Records Administration (NARA). For
information on the availability of this material at NARA, call 202–741–6030, or go to:
[Link] Copies may be obtained from the standard producer or publisher
listed in the regulation. Methods in the materials listed below shall be used to analyze samples of sewage sludge.
(1) Enteric viruses. ASTM Designation: D 4994–89, ―Standard Practice for Recovery of Viruses From Wastewater Sludges‖, 1992 Annual Book of ASTM
Standards: Section 11—Water and Environmental Technology, ASTM, 1916 Race Street, Philadelphia, PA 19103–1187.
(2) Fecal coliform. Part 9221 E. or Part 9222 D., ―Standard Methods for the Examination of Water and Wastewater‖, 18th Edition, 1992, American Public
Health Association, 1015 15th Street, NW., Washington, DC 20005.
(3) Helminth ova. Yanko, W.A., ―Occurrence of Pathogens in Distribution and Marketing Municipal Sludges‖, EPA 600/1–87–014, 1987. National Technical
Information Service, 5285 Port Royal Road, Springfield, Virginia 22161 (PB 88–154273/AS).
(4) Inorganic pollutants. ―Test Methods for Evaluating Solid Waste, Physical/Chemical Methods‖, EPA Publication SW–846, Second Edition (1982) with
Updates I (April 1984) and II (April 1985) and Third Edition (November 1986) with Revision I (December 1987). Second Edition and Updates I and II are
available from the National Technical Information Service, 5285 Port Royal Road, Springfield, Virginia 22161 (PB–87–120–291). Third Edition and
Revision I are available from Superintendent of Documents, Government Printing Office, 941 North Capitol Street, NE., Washington, DC 20002
(Document Number 955–001–00000–1).
(5) Salmonella sp. bacteria. Part 9260 D., ―Standard Methods for the Examination of Water and Wastewater‖, 18th Edition, 1992, American Public Health
Association, 1015 15th Street, NW., Washington, DC 20005; or
Kenner, B.A. and H.P. Clark, ―Detection and enumeration of Salmonella and Pseudomonas aeruginosa‖, Journal of the Water Pollution Control
Federation, Vol. 46, no. 9, September 1974, pp. 2163–2171. Water Environment Federation, 601 Wythe Street, Alexandria, Virginia 22314.
(6) Specific oxygen uptake rate. Part 2710 B., ―Standard Methods for the Examination of Water and Wastewater‖, 18th Edition, 1992, American Public
Health Association, 1015 15th Street, NW., Washington, DC 20005.
(7) Total, fixed, and volatile solids. Part 2540 G., ―Standard Methods for the Examination of Water and Wastewater‖, 18th Edition, 1992, American Public
Health Association, 1015 15th Street, NW., Washington, DC 20005.
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40 CFR 503.32 Requirements--To meet the NAC requirements choose one of the following alternatives
§ 503.32 Pathogens.
(a) Sewage sludge—Class A. (1) The requirement in §503.32(a)(2) and the requirements in either §503.32(a)(3), (a)(4), (a)(5), (a)(6), (a)(7), or (a)(8) shall
be met for a sewage sludge to be classified Class A with respect to pathogens.
(2) The Class A pathogen requirements in §503.32 (a)(3) through (a)(8) shall be met either prior to meeting or at the same time the vector attraction
reduction requirements in §503.33, except the vector attraction reduction requirements in §503.33 (b)(6) through (b)(8), are met.
(ii) The temperature of the sewage sludge that is used or disposed shall be maintained at a specific value for a period of time.
(A) When the percent solids of the sewage sludge is seven percent or higher, the temperature of the sewage sludge shall be 50 degrees Celsius or higher;
the time period shall be 20 minutes or longer; and the temperature and time period shall be determined using equation (2), except when small particles of
sewage sludge are heated by either warmed gases or an immiscible liquid.
Where,
D=time in days.
(B) When the percent solids of the sewage sludge is seven percent or higher and small particles of sewage sludge are heated by either warmed gases or
an immiscible liquid, the temperature of the sewage sludge shall be 50 degrees Celsius or higher; the time period shall be 15 seconds or longer; and the
temperature and time period shall be determined using equation (2).
(C) When the percent solids of the sewage sludge is less than seven percent and the time period is at least 15 seconds, but less than 30 minutes, the
temperature and time period shall be determined using equation (2).
(D) When the percent solids of the sewage sludge is less than seven percent; the temperature of the sewage sludge is 50 degrees Celsius or higher; and
the time period is 30 minutes or longer, the temperature and time period shall be determined using equation (3).
Where,
D=time in days.
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(ii)(A) The pH of the sewage sludge that is used or disposed shall be raised to above 12 and shall remain above 12 for 72 hours.
(B) The temperature of the sewage sludge shall be above 52 degrees Celsius for 12 hours or longer during the period that the pH of the sewage sludge is
above 12.
(C) At the end of the 72 hour period during which the pH of the sewage sludge is above 12, the sewage sludge shall be air dried to achieve a percent
solids in the sewage sludge greater than 50 percent.
(ii)(A) The sewage sludge shall be analyzed prior to pathogen treatment to determine whether the sewage sludge contains enteric viruses.
(B) When the density of enteric viruses in the sewage sludge prior to pathogen treatment is less than one Plaque-forming Unit per four grams of total
solids (dry weight basis), the sewage sludge is Class A with respect to enteric viruses until the next monitoring episode for the sewage sludge.
(C) When the density of enteric viruses in the sewage sludge prior to pathogen treatment is equal to or greater than one Plaque-forming Unit per four
grams of total solids (dry weight basis), the sewage sludge is Class A with respect to enteric viruses when the density of enteric viruses in the sewage
sludge after pathogen treatment is less than one Plaque-forming Unit per four grams of total solids (dry weight basis) and when the values or ranges of
values for the operating parameters for the pathogen treatment process that produces the sewage sludge that meets the enteric virus density requirement
are documented.
(D) After the enteric virus reduction in paragraph (a)(5)(ii)(C) of this section is demonstrated for the pathogen treatment process, the sewage sludge
continues to be Class A with respect to enteric viruses when the values for the pathogen treatment process operating parameters are consistent with the
values or ranges of values documented in paragraph (a)(5)(ii)(C) of this section.
(iii)(A) The sewage sludge shall be analyzed prior to pathogen treatment to determine whether the sewage sludge contains viable helminth ova.
(B) When the density of viable helminth ova in the sewage sludge prior to pathogen treatment is less than one per four grams of total solids (dry weight
basis), the sewage sludge is Class A with respect to viable helminth ova until the next monitoring episode for the sewage sludge.
(C) When the density of viable helminth ova in the sewage sludge prior to pathogen treatment is equal to or greater than one per four grams of total solids
(dry weight basis), the sewage sludge is Class A with respect to viable helminth ova when the density of viable helminth ova in the sewage sludge after
pathogen treatment is less than one per four grams of total solids (dry weight basis) and when the values or ranges of values for the operating parameters
for the pathogen treatment process that produces the sewage sludge that meets the viable helminth ova density requirement are documented.
(D) After the viable helminth ova reduction in paragraph (a)(5)(iii)(C) of this section is demonstrated for the pathogen treatment process, the sewage
sludge continues to be Class A with respect to viable helminth ova when the values for the pathogen treatment process operating parameters are
consistent with the values or ranges of values documented in paragraph (a)(5)(iii)(C) of this section.
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(ii) The density of enteric viruses in the sewage sludge shall be less than one Plaque-forming Unit per four grams of total solids (dry weight basis) at the
time the sewage sludge is used or disposed; at the time the sewage sludge is prepared for sale or give away in a bag or other container for application to
the land; or at the time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f),
unless otherwise specified by the permitting authority.
(iii) The density of viable helminth ova in the sewage sludge shall be less than one per four grams of total solids (dry weight basis) at the time the sewage
sludge is used or disposed; at the time the sewage sludge is prepared for sale or give away in a bag or other container for application to the land; or at the
time the sewage sludge or material derived from sewage sludge is prepared to meet the requirements in §503.10 (b), (c), (e), or (f), unless otherwise
specified by the permitting authority.
(ii) Sewage sludge that is used or disposed shall be treated in one of the Processes to Further Reduce Pathogens described in appendix B of this part.
(ii) Sewage sludge that is used or disposed shall be treated in a process that is equivalent to a Process to Further Reduce Pathogens, as determined by
the permitting authority.
(b) Sewage sludge—Class B. (1)(i) The requirements in either §503.32(b)(2), (b)(3), or (b)(4) shall be met for a sewage sludge to be classified Class B
with respect to pathogens.
(ii) The site restrictions in §503.32(b)(5) shall be met when sewage sludge that meets the Class B pathogen requirements in §503.32(b)(2), (b)(3), or (b)(4)
is applied to the land.
(ii) The geometric mean of the density of fecal coliform in the samples collected in paragraph (b)(2)(i) of this section shall be less than either 2,000,000
Most Probable Number per gram of total solids (dry weight basis) or 2,000,000 Colony Forming Units per gram of total solids (dry weight basis).
(5) Site restrictions. (i) Food crops with harvested parts that touch the sewage sludge/soil mixture and are totally above the land surface shall not be
harvested for 14 months after application of sewage sludge.
(ii) Food crops with harvested parts below the surface of the land shall not be harvested for 20 months after application of sewage sludge when the
sewage sludge remains on the land surface for four months or longer prior to incorporation into the soil.
(iii) Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after application of sewage sludge when the
sewage sludge remains on the land surface for less than four months prior to incorporation into the soil.
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(iv) Food crops, feed crops, and fiber crops shall not be harvested for 30 days after application of sewage sludge
(v) Animals shall not be grazed on the land for 30 days after application of sewage sludge.
(vi) Turf grown on land where sewage sludge is applied shall not be harvested for one year after application of the sewage sludge when the harvested turf
is placed on either land with a high potential for public exposure or a lawn, unless otherwise specified by the permitting authority
(vii) Public access to land with a high potential for public exposure shall be restricted for one year after application of sewage sludge
(viii) Public access to land with a low potential for public exposure shall be restricted for 30 days after application of sewage sludge
(c) Domestic septage. (1) The site restrictions in §503.32(b)(5) shall be met when domestic septage is applied to agricultural land, forest, or a reclamation
site; or
(2) The pH of domestic septage applied to agricultural land, forest, or a reclamation site shall be raised to 12 or higher by alkali addition and, without the
addition of more alkali, shall remain at 12 or higher for 30 minutes and the site restrictions in §503.32 (b)(5)(i) through (b)(5)(iv) shall be met.
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