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CHM134 Lab Techniques & Reactions

This document contains summaries of two chemistry experiments conducted by Muhammad Adib Bin Azahari. Experiment 1 involved basic laboratory techniques like calibrating a volumetric flask, pipette, and burette. The actual volumes measured slightly differed from the stated volumes. Experiment 3 examined the limiting reagent of the reaction between sodium carbonate and calcium nitrate to produce calcium carbonate. Calculations showed calcium nitrate to be the limiting reagent. The percent yield of calcium carbonate formed was 93.66%. The document includes results, calculations, and signatures from the lecturer evaluating the experiments.

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Adib azahari
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13 views6 pages

CHM134 Lab Techniques & Reactions

This document contains summaries of two chemistry experiments conducted by Muhammad Adib Bin Azahari. Experiment 1 involved basic laboratory techniques like calibrating a volumetric flask, pipette, and burette. The actual volumes measured slightly differed from the stated volumes. Experiment 3 examined the limiting reagent of the reaction between sodium carbonate and calcium nitrate to produce calcium carbonate. Calculations showed calcium nitrate to be the limiting reagent. The percent yield of calcium carbonate formed was 93.66%. The document includes results, calculations, and signatures from the lecturer evaluating the experiments.

Uploaded by

Adib azahari
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd

CHM134

EXPERIMENTS: EXPERIMENT 1 BASIC LABORATORY TECHNIQUES


EXPERIMENT 3 LIMITING REAGENT OF REACTION
LAB INSTRUCTORS DR MOHD ZULI JAAFAR
NAME:
CLASS: M3AT1102A
STUDENTS NAME: MUHAMMAD ADIB BIN AZAHARI
MARKS:
COMMENT:
DATASHEET EXPERIMENT 1

BASIC LABORATORY TECHNIQUES

Name : MUHAMMAD ADIB BIN AZAHARI Date:

Student ID : 2022156973 Group: M3AT1102A

RESULT

a. Calibration of Volumetric Flask

Mass of empty volumetric flask (g) 209254 g


Mass of volumetric flask + distilled water (g) 45.8486 g
Mass of distilled water (g) 24.9232 g
Temperature of distilled water (oC) 25oC
Density of water (from Table 1) (g/mL) 1.0039 g

b. Calibration of pipette

(i) (ii)
Mass of empty beaker (g) 37.8655 g 36.4375 g
Mass of beaker + distilled water (g) 57.6901 g 57.8018 g
Mass of distilled water (g) 19.8246 g 21.3643 g
Mass of distilled water (g) 26oC 25oC
Density of water (from Table 1) (g/mL) 1.0042 g 1.0039 g

c. Calibration of Burette
Mass of empty beaker (g) : 37.6835 g

Temperature of distilled water (oC) : 24oC

Density of water (from Table 1) (g/mL) : 1.0037 g

After the addition of distilled water.

Reading of burette Mass of beaker + Mass of distilled Mass of distilled


(mL) distilled water (g) water (g) water for each 5 mL
burette reading (g
5 42.0055 g 4.3220 g 4.3220 g
10 47.0460 g 9.2625 g 4.9405 g
15 52.0141 g 14.3306 g 5.0681 g
20 56.9015 19.2180 g 4.8874 g
CALCULATION

a. Determine the actual volume of the volumetric flask based on calculation.


mass
Volume=
density

24.9232 g
Volume=
1.0039 g
Volume = 24.8264 mL

b. Determine the actual volume of the pipette based on the calculation for the experiment (i) and
experiment (ii).
mass
Volume=
density

19.8246 g 21.3643 g
i. Volume= ii. Volume=
1.0042 g 1.0039 g

Volume = 19.7417 mL Volume= 21.2813 mL

c. Determine the actual volume of distilled water (in mL) for each 5 mL burette reading based on
calculation.

Reading of burette (mL) Reading of burette (mL)


0-5 4.3060
5-10 4.9223
10-15 5.0494
15-20 4.8693

Lecturer’s signature,
____________________

DATASHEET EXPERIMENT 3

LIMITING REAGENT OF REACTION

RESULT

Data:

Mass of Na2CO3 (g) 0.5019


Mass of Ca(NO3)2 (g) 1.0246
Mass of filter paper (g) 1.0990
Mass of CaCO3 precipitate + filter paper (g) 1.5424
Mass of CaCO3 precipitate (g) 0.4434

CALCULATIONS

1. Write a balanced chemical equation including phases for the reaction.

Na 2 CO 3(solid )+ Ca¿ ¿

2. Determine the limiting reagent for the reaction.


1) Mole of Na2CO3
0.5019 g
106 g /mol
=0.00473490566 mol

2) Mole of Ca(NO3)2

1.0246
220 g /mol
=0.00465727272 mol

3) Divide moles of Na2CO3 and Ca(NO3)2 with their stoichiometric coefficients

i. Na2CO3

0.00473490566 mol
=0.00465727272 mol
1
ii. Ca(NO3)2

0.00465727272mol
=0.00465727272mol
1
3. Calculate the expected mass of CaCO 3 produced from the masses of Na2CO3 and Ca(NO3)2.

1 mol CaC O3
0.00473490566 mol=0.00473490566 mol Na2 CO 3
1 mol Na2 CO3
= 0.00473490566 mol CaC O3

Mass of CaC O3

= mol × molar massCaC O3

¿ 0.00473490566 mol ×100.0 g/mol


¿ 0.4734 gTheoritical Yield

4. Determine the percentage yield CaCO 3

Actual yield
Percent Yield= × 100
Theoretical yield

0.4434 g
×100 %
0.4734 g
Percent Yield = 93.66%

Lecturer’s signature,
____________________

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