Rotary Evaporator

Model

RE301

Instruction Manual

- The Second Edition -

This document is the exclusive instruction manual to the RE301 model rotary
evaporator main unit.
Please use this document together with the instruction manual of the VR300
model vacuum controller or TA300 model vapor temperature indicator as for the
operating instructions of device.

z Thank you for purchasing "Rotary Evaporator,

RE Series" of Yamato Scientific Co., Ltd.
z To use this unit properly, read this "Instruction
Manual" thoroughly before using this unit.
Keep this instruction manual around this unit for
referring at anytime.

WARNING!:
Carefully read and thoroughly understand the
important warning items described in this
manual before using this unit.

Yamato Scientific Co. LTD.

 Contents

‹ [Link] in the Package...................................................................... 1

‹ [Link] in Using with Safety............................................................. 2
• Explanation.................................................................................................................... 2
• Table of Illustrated Symbols .......................................................................................... 3
• Fundamental Matters of "WARNING!" and "CAUTION!" ............................................... 4
‹ [Link] Using This Unit......................................................................... 6
‹ [Link] Appearance............................................................................. 9
‹ [Link] Method............................................................................. 10
• RE301 model installation............................................................................................. 10
• Installation Method ...................................................................................................... 11
• Connecting method and assembling procedures of glass unit.................................... 14
• Installation Method (Optional accessories) ................................................................. 17
‹ [Link] Panel...................................................................................... 22
‹ [Link] Function ............................................................................ 23
‹ [Link] and Function of Each Part ............................................ 24
‹ [Link] Precautions ........................................................................ 26
‹ [Link] Method........................................................................ 27
‹ [Link] storage and disposal.............................................................. 28
‹ [Link] the Event of Failure… .................................................................. 29
• Safety Device and Error Code..................................................................................... 29
• Trouble Shooting ......................................................................................................... 29
‹ [Link] Service and Warranty ............................................................. 30
‹ [Link] ..................................................................................... 31
‹ [Link] Diagram................................................................................. 32
‹ [Link] Parts Table ................................................................. 33
‹ [Link] of Dangerous Materials ............................................................ 34
‹ 18. Standard Installation Manual.......................................................... 35
 [Link] in the Package
Contents in the Package
Affirmation of content package
Check the content of package before setting up the device.
Contact our selling office or sales office if any components or parts are missing.

RE301 main unit(main unit and appurtenant)

No. Name QTY Notes check
1 RE301 main unit 1 set
2 Vacuum seal 1
3 Condenser fixing nut 1
4 Coil ring 1
5 Rotary joint retainer 1
6 Ring(large/middle/small) each 1
7 O-ring 2
8 Vacuum grease 1
9 Power cord 1
10 Bath ways 1
11 Instruction manual 1
12 Warranty card 1
13 Battery(9V alkaline dry cell) 2
Caution: Please check being attached to RE main part about 1-7.

1
 [Link] in Using with Safety
Explanation

MEANING OF ILLUSTRATED SYMBOLS

Illustrated Symbols
Various symbols are used in this safety manual in order to use the unit without
danger of injury and damage of the unit. A list of problems caused by ignoring
the warnings and improper handling is divided as shown [Link] sure that you
understand the warnings and cautions in this manual before operating the unit.

WARNING! Ifmaythecause
warning is ignored, there is the danger of a problem that
a serious accident or even fatality.

If the caution is ignored, there is the danger of a problem that may

CAUTION! cause injury/damage to property or the unit itself.

Meaning of Symbols

This symbol indicates items that urge the warning (including the caution).
A detailed warning message is shown adjacent to the symbol.

This symbol indicates items that are strictly prohibited.

A detailed message is shown adjacent to the symbol with specific actions not to
perform.

This symbol indicates items that should be always performed.

A detailed message with instructions is shown adjacent to the symbol.

2
 [Link] in Using with Safety
Table of Illustrated Symbols

Warning

Warning, Warning, Warning, Warning, Warning,

generally high voltage high temperature drive train explosive

Caution

Caution, Caution, Caution, Caution, Caution,

generally electrical shock scald no road heating not to drench

Caution, Caution, Caution,

water only deadly poison water

Prohibit

Prohibit, Prohibit, Prohibit, Prohibit,

generally inflammable to disassemble to touch

Compulsion

Compulsion, Compulsion, Compulsion, Compulsion, Compulsion,

generally connect to the install on a flat disconnect the periodical
grounding surface power plug inspection
terminal

3
 [Link] in Using with Safety
Fundamental Matters of "WARNING!" and "CAUTION!"
WARNING!
Do not use this unit in an area where there is flammable or explosive gas
Never use this unit in an area where there is flammable or explosive gas. This unit is not
explosion-proof. An arc may be generated when the power switch is turned on or off, and
fire/explosion may result. (Refer to page 34 "[Link] of Dangerous Materials
".)

Always ground this unit

Always ground this unit on the power equipment side in order to avoid electrical shock due to a power surge.

Plug the power cord securely

Plug the power cord securely into the main unit. If not, overheat or fire disaster may result in.

If a problem occurs
If smoke or strange odor should come out of this unit for some reason, turn off the circuit breaker right away,
and then disconnect the power plug. Immediately contact a service technician for inspection. If this
procedure is not followed, fire or electrical shock may result. Never perform repair work yourself, since it is
dangerous and not recommended.

Do not use the power cord if it is bundled or tangled

Do not use the power cord if it is bundled or tangled. If it is used in this manner, it can overheat and fire
may be caused.

Do not process, bend, wring, or stretch the power cord forcibly

Do not process, bend, wring, or stretch the power cord forcibly. Fire or electrical shock may result.

Perform periodic check

Check the device frequently. Do not leave the dust and dirt on the wiring terminals and electrical
components. A fire disaster may result in.

Substances that can not be used

Never use explosive substances, flammable substances and substances that include explosive or flammable
ingredients in this unit. Explosion or fire may occur. (Refer to page 34 "[Link] of Dangerous Materials ".)

Do not disassemble or modify this unit

Do not disassemble or modify this unit. Fire or electrical shock or failure may be caused.

4
 [Link] in Using with Safety
Fundamental Matters of "WARNING!" and "CAUTION!"
CAUTION!
During a thunder storm
During a thunderstorm, turn off the power key immediately, then turn off the circuit breaker and the
main power. If this procedure is not followed, fire or electrical shock may be caused.

When electric power failure occurs…

The device stops operation when electric power failure occurs. In this case, turn off the breaker for safety.
When the power is applied again, if the power switch is turned on, the main unit will go to automatically upper
step.

5
 [Link] Using This Unit
Requirements for Installation

WARNING!
1. Always ground this unit
• Be sure to connect the ground wire to the earth conductor or earth terminal to prevent
accidents caused by an electric shock.
• Do not connect the earth wire to gas or water pipes. If not, fire disaster may be caused.
• Do not connect the earth wire to the ground for telephone wire or lightning conductor. If not,
fire disaster or electric shock may be caused.
• Consult your local electrical contractor for power connecting work.

2. Choose a proper place for installation

• Do not install this unit in a place where:
♦ Rough or dirty surface.
♦ Flammable gas or corrosive gas is generated.
♦ Ambient temperature above 35°C.
♦ Ambient temperature fluctuates violently.
♦ There is direct sunlight.
♦ There is excessive humidity and dust.
♦ There is a constant vibration.
♦ Without a ventilation system.
♦ The unstable place of a power supply.

• Make sure that no flammable substances are placed around the devices. Keep space as
shown, at least, in the figure below. We recommend the installation inside the ventilation
system such as a draft chamber.
More than 10cm

More than More than

Main Unit
10cm 10cm

More than 10cm

3. Do not use this unit in an area where there is flammable or explosive gas
• Never use this unit in an area where
there is flammable or explosive gas. This

×
unit is not explosion-proof. An arc may
be generated when the power switch is
turned ON or OFF, and fire/explosion
may result.
• To know about flammable or explosive
gas, refer to page 34 "17. List of
Dangerous Materials ".

6
 [Link] Using This Unit
Requirements for Installation

4. Install exhauster and ventilator

• Be sure to install an exhauster,
ventilator and extinguisher around
the device.
The oily smoke of silicone oil
generated by heating is flammable
and may cause fire disaster.
Silicone oil also may generate Exhauster and ventilator
harmful gas when it reaches a high
temperature.

Extinguisher

CAUTION!
5. Do not modify
• Modification of this unit is strictly
prohibited. This could cause a failure.

Modification

6. Installation on horizontal surface

• Place this unit as flat a place as possible. If the
three rubber feet and adjuster are not in
uniform contact with the floor surface, noise or
vibration may result. Additionally, the unit may
cause a problem or malfunction.

7. Choose a correct power distribution board or receptacle

• Choose a correct power distribution board or receptacle that meets the unit’s rated electric
capacity.
Electric capacity: RE301: 1.5A at AC100V to AC240V
Electric capacity for RE main unit (except water bath or oil bath) and
vacuum controller. The water bath or oil bath uses the other power source.
The electric capacity of 12.5A and 6.5A are required for the BM500/BO400
and BM510/BO410 models respectively.
NOTE)
The device adopts the free power system for AC100V to AC240V. The RE main unit includes
the switching power source, the secondary power source of which is driven with DC24V.
Do not connect the lines that share the power source, or do not place the appliances that
generate noise around the device. A malfunction may occur on the device.

7
 [Link] Using This Unit
Requirements for Installation

8. Before/after installing
• It may cause injure to a person if this unit falls down or moves by the earthquake and the
impact. etc..To prevent, take measures that the unit cannot fall down, and not install to busy
place.
• Be sure to install an exhauster, ventilator and extinguisher around the device.

9. Handling of power code

• Do not entangle the power cord. This will cause overheating and possibly a fire.
• Do not bend or twist the power cord, or apply excessive tension to it. This may cause a fire
and electrical shock.
• Do not lay the power cord under a desk or chair, and do not allow it to be pinched in order to
prevent it from being damaged and to avoid a fire or electrical shock.
• Keep the power cord away from any heating equipment such as a room heater. The cord's
insulation may melt and cause a fire or electrical shock.
• If the power cord becomes damaged (wiring exposed, breakage, etc.), immediately turn off the
power at the rear of this unit and shut off the main supply power. Then contact your nearest
dealer for replacement of the power cord. Leaving it may cause a fire or electrical shock.
• Connect the power plug to the receptacle which is supplied appropriate power and voltage.

10. Precautions for use of sample including organic solvent

• Note the followings when using the sample which includes organic solvent.
™ A Teflon seal, which is sold separately, is recommended for the seal on the rotary joint.
™ A Teflon diaphragm model vacuum pump is recommended.
™ When using VR300, the electromagnetic valve for vacuum regulator control recommends you use
of an optional Teflon electromagnetic valve.
™ When using VR300, a vacuum regulator pressure sensor recommends you use of the optional
pressure sensor made from SUS316.
Cautions
Use an optional Teflon vacuum seal for ketone and an ether system solvent.
Acetone, methyl ethyl ketone, methyl isobutyl ketone, ethyl ether, and MTBE (methyl t-butyl
ether) etc. -- the case where ketone and an ether system solvent are used -- vacuum seal (NBR)
of standard attachment It will swell.
Use the fluorocarbon polymers vacuum seal of an option.
ORE80 ORE70

VR type Teflon solenoid valve Teflon vacuum seal

ORE90 PG200 model

VR type pressure sensor for organic solvent Teflon diaphragm model vacuum pump

8
 [Link] Appearance
RE301 model installation
RE301

Front view

Knob for speed controller

MAX250 rpm

Display

Rotar

Updown key

Knob for lower limit

Rear view

Connector(power)

Connector(signal)

Rating nameplate

Storage for battery

Socket for power supply

Circuit breaker

9
 [Link] Method
RE301 model installation
[Link] installation
Unpack the main unit of RE301 and install it on the level area.
RE301 model installation
Refer to the instruction manual of vacuum controller for the installation of VR300 model vacuum controller.

Installation example: RE301AW

Connection on back surface area DC power output connector for VR300 or TA300

Main switch of rotary evaporator

(also used as a circuit breaker)
○: OFF I: ON

Plug the attached power cord securely.

Connect a vacuum hose and a cooling hose to the cooling water circulation unit.
A vacuum hose should prepare the inside diameter of 6mm, and a cooling hose should prepare a thing
with an inside diameter of 9mm.
Pipe by the length that each hose between a vacuum pump or the cooling water circulation unit is not
pulled at the time of a main part lift rise.
Refer to P.17 for a piping configuration.

10
 [Link] Method
Installation Method
1.RE301 back surface (battery attachment)
Battery: Two 9V alkaline dry cells (accessories)

① Remove the screw of a back surface and remove a battery attachment plate lid.
② Attach 9V alkaline dry cell to a back battery storage part.
③ Set polarity correctly.
④ Attach a battery attachment plate lid with the screw.

The screw

RE301

CAUTION!
● Confirm the polarity of the electrode.
● When an electrode is connected in the opposite direction, a problem occurs, and dangerous.
● Don't mix the different kind of battery .
● Remove a battery when you don't use for a long time.

11
 [Link] Method
Installation Method
2. Attachment of Bath ways
1）The base of a main part is lifted so that the
bottom can be seen.

The base of a main part

2）An attached bath guide is inserted in a

groove portion.

Groove portion

Bath ways

3）Please return a main part and use it as a

standard of bath installation.

12
 [Link] Method
Installation Method
3. Connecting method and assembling procedures of glass unit
1) Glass set on condenser
Connect the glass set to the rotor unit on the RE main unit.

A set
Glass set A:
Photo: RE301AW The standard glass set, where the
condenser is tilted to be set, suitable for
distillation, concentration, and collection
of samples.

B set
Glass set B:
Photo: RE301BW The condenser is set vertically, suitable
for distillation, concentration, and
collection of samples regardless of their
boiling point. The condenser unit and
connecting pipe is integrated to realize
the space-saving design. The
connecting pipe is also equipped with a
unique drip-proof mechanism.

C set
Glass set C:
Photo: RE301CW The condenser is set vertically, suitable
for distillation, concentration, and
collection of samples which has a low
boiling point, such as dry ice or ice.
The condenser unit and connecting pipe
is integrated to realize the space-saving
design. The connecting pipe is also
equipped with a unique drip-proof
mechanism.

13
 [Link] Method
Connecting method and assembling procedures of glass unit
2) Connecting method and assembling procedures of glass unit①
②Ring(middle) ④P22 Viton O-ring
⑨Condenser mounting nut
①Ring(large) ③Ring(small)
⑩Coil ring

⑪Vacuum seal A

⑬Condenser ⑥Rotary joint

⑫Main unit
⑧P20 Red silicone O-ring ⑤Rotary joint retainer
⑦Sample flask extractor

[1]How to fix the rotary joint

It is inserted into ①Ring(large)→ ④P22 Viton O-ring→ ②Ring(medium)→ ④P22 Viton O-ring→ ③
Ring(small), and it clings in the order of ⑤Rotary joint retainer in the main unit rotar part. (Figure A part)

Figure B part has a glass set attached.

1. ⑤Rotary joint retainer is relaxed.

2. ⑥Rotary joint is inserted. (Though it is possible to insert the ⑥Rotary joint any position ,it is
recommended checking ⑧P20 Red silicone O-ring at the tip of ⑤Rotary joint retainer.)

3. ⑤Rotary joint retainer is tightened after ⑥Rotary joint is inserted.

14
 [Link] Method
Connecting method and assembling procedures of glass unit

[2] How to fix a Condenser

① It is passed through the condenser in order of ⑬It prepares for the condenser,in rotor installation
part⑨Condenser fixing nut→⑩Coil ring.
② Apply a thin layer of silicone grease onto the mating surface with ⑥rotary joint on the ⑪Vacuum
seal and fit it into the fitting area of condensation tube with the orientation shown in the figure.
Insert the seal into the rotary joint together with the condensation tube and tighten it with the
condenser fixing nut.

Cautions
ⅰ. Use an optional Teflon vacuum seal for ketone and an ether system solvent.
Acetone, methyl ethyl ketone, methyl isobutyl ketone, ethyl ether, and MTBE (methyl t-butyl ether) etc.
-- the case where ketone and an ether system solvent are used -- vacuum seal (NBR) of standard
attachment It will swell.
Use the fluorocarbon polymers vacuum seal of an option.
ⅱ. Be careful of the glass damage.
ⅲ. Carry out assembling in the order of [1] [2].
When ［2］ is fixed first, it sometimes becomes a problem cause such as vacuum omission.

15
 [Link] Method
Connecting method and assembling procedures of glass unit
2)Connecting method and assembling procedures of glass unit②
Setup of the sample-receiving flask (round-bottom flask) and distillation flask (recovery flask).
Apply a thin layer of silicone grease onto the facing surface as necessary and fix them with the attached
clamp.
Sample-receiving flask Distillation flask

Flask clamp (2) Flask clamp (1)

＊ ＊

＊In using 2L flask of an optional (a distillation flask and a receptacle flask), please use the metal clamp of
an optional respectively. Moreover, by the load of a repeated load, since there is a possibility of
damaging, please use the resin clamp as an consumption article. (P. 34 references)

Setup of sample induction cock

Insert the sample induction cock with Teflon tube into the connecting pipe. Apply a thin layer of
silicone grease onto the facing surface as necessary.

Sample induction cock (Teflon tube attached)

Nozzle・Cap for nozzles・Packing for nozzles

Stop・Cap for nozzles・Packing for stopping

16
 [Link] Method
Installation Method (Optional accessories)
3) Piping method
Piping between condenser and peripheral device
The rotary evaporator requires the vacuum equipment such as vacuum pump or aspirator, cooling water
circulation system to cool the condenser, and tap water. Use the vacuum hose with the inner diameter
of 6mm for vacuum route and heat insulation hose with the inner diameter of 9mm for cooling route.
Securely fix the connection between respective hoses and resin nipple using a clamp.

Piping between RE301 and glass set condenser

Piping method to glass set A condenser

Cooling water
circulation unit Vacuum pump

IN
IN
OUT

OUT

Exhaust

Piping method to glass set B condenser

Vacuum pump
Cooling water
circulation unit
IN
IN

OUT
OUT

Exhaust

Piping method to glass set B condenser

Connect the attached

drain hose.
Vacuum pump
To drain
IN

Put dry ice or ice.

OUT

Exhaust

17
 [Link] Method
Installation Method (Optional accessories)
4) Optional accessories and their connection method
Optional accessories for rotary evaporator include VR300 model vacuum controller, TA300 model vapor
temperature indicator, RT101/200 model solvent collection device, CF720, CF750, and a CF750S type
cooling water circulation unit, relay hose connection fitting used on the vacuum hose or cooling water
circulation hose, and glass trap to prevent back-flow.

Applicable model
No. Name Model
RE301
① VR300 model vacuum controller VR300 ○
② TA300 model vapor temperature indicator TA300 ○
③ RT101 model solvent collection device RT101 ○
④ RT200 model solvent collection device RT200 ○
CF720 and CF750 type cooling water
⑤ CF720/750 ○
circulation unit
⑥ Hose connection fitting ORE30 ○
⑦ Glass trap ORE40 ○

4) Optional accessories and their connection method①

① VR300 model vacuum controller
Refer to the VR300 model instruction manual for the connection method.

② TA300 model vapor temperature indicator

DC24V power harness is connected to RE main unit, and connect evaporation temperature
sensor to the condenser..
TA300

RE301

Condenser A Condenser B Condenser C

18
 [Link] Method
Installation Method (Optional accessories)
4) Optional accessories and their connection method②
③ RT101 model solvent collection device
Refer to the RT101 model instruction manual for the connection method.

④ RT200 model solvent collection device

The device consists of glass condenser and 500 milliliter collection flask. The device requires a
cooling water circulation unit.
Connect the vacuum hose between the exhaust nozzle of vacuum pump and IN nipple on the
RT200, as shown in the figure. The end connection of exhaust piping and cooling water piping
on the RT200 model are placed on the back surface of main unit.
Connected to the nozzle
on the back surface of RT200
Exhaust IN
To ventilation system
(such as a draft chamber) Exhaust OUT
Vacuum
真空ポンプpump

IN Cooling IN

Cooling OUT

OUT

Cooling water
circulation unit

IN

OUT

19
 [Link] Method
Installation Method (Optional accessories)
4) Optional accessories and their connection method③
⑤CF720 and CF750 type cooling water circulation unit

The internal piping of the unit has with two discharge ports and allows cooling in two systems(two
external units).
・Carefully check the connecting piping before use.
※About the circulation pump switch
The circulation pump switch can be operated alone free of relations with the temperature controller.
Turn the breaker on, check that proper circulation is made in each pipe and that the unit is not operating
with no-load, and then turn the switch “On”.
When circulation is not necessary, not only close the both cocks but also turn the switch “Off” to prolong
the pump life.
※Operation and indicated data is for when only one side is used (one system is connected).
Note that the flow and the lift might decrease when both sides are used (two systems are connected)
compared with when only one side is used.

①Discharge 1

②Return1

RE main unit1

Liquid
pouring
mouth

CF750

③Return2
+
④Discharge 2

RE main unit2

20
 [Link] Method
Installation Method (Optional accessories)
4) Optional accessories and their connection method④
⑥ ORE30:Piping hose connection to hose connection fitting
The nipple-fitting is used to reduce the load of vacuum hose and cooling water circulation hose,
which are connected to the condenser unit on the RE main unit, at the operation of lift by
supporting them.
Refer to the instruction manual of hose connection fitting for the connection method.

⑦ ORE40:Connection example of glass trap

真空ポンプ
Vacuum pump
Steam temperature
sensor IN
Cooling temperature
sensor LEAK
LEAK
Rotor lift I/O

Bath I/O
IN
IN OUT
Vacuum pump
drive output OUT
OUT
Exhaust
排気
DC24V power input

Exhaust

Hole cap

Glass trap Condensation

machine

21
 [Link] Panel
Control Panel

Rotary Evaporator RE801

② Liquid crystal rotation indicator ① Rotation control knob

RE301

・Refer to the instruction manual of VR model vacuum controller for of VR model vacuum controller.
・The VR300 model vacuum controller for the RE301 model is an optional accessory. The VR300 model
does not have memory function (MEMORY key).

No. Name Function

① Rotation control knob The control knob equipped with the rotary motor ON/OFF switch.
Clockwise rotation：Acceleration
Counterclockwise rotation：Slowdown
---The condition of “OFF”---
The rotation of the motor stops when the knob is turned
counterclockwise until with a clink.
Factory setting, it is shipped in the state of "OFF."
Maximum rotation speed: 250 rpm
② Liquid crystal rotation The indicator digital displays the rotation speed.
indicator It indicates the abnormality state when overload in motor occurs.

22
 [Link] Function
Basic Operation
Flow of Basic Operation
The operation procedure of rotary evaporator is described below.
① Set the desired bath temperature and heat the bath until the bath temperature becomes stable.
② Turn on the switch of Cooling water circulation unit and circulate the cooling water.
③ Make sure that the rotation control knob is fully turned to the left (rotation OFF). Turn on the
power switch (1 position) on the back surface of RE main unit.
④ Put the moderate amounts of sample into the distillation flask and connect it to the rotary joint.
⑤ Turn on the switch of Vacuum pump and decompression.
⑥ Set the desired rotation speed with the rotation control knob on the main unit. For VR300, set the
desired rotation speed with the rotation control knob and then start the operation by the key
operation on the VR model vacuum controller.
（Cautions: Although number of rotations is displayed from 14rpm, when using it, please use it at
20rpm or more.）
⑦ Lower the sample flask using the lift ▽ (down) key to heat it.

⑥Start the operation.

As for the VR300, use the key on the VR
model vacuum controller.
⑦Lift down the flask. Turn on the vacuum pump.

③ Put the sample into the flask.

① Heat the bath.

23
 [Link] and Function of Each Part
Other Functions
Rotation control knob drive unit
It adjusts the rotation speed.

Lift (Main unit)

The glass unit is raised or descended by the
Updown key

Rotor
It starts, stops and adjusts the rotation of
rotary joint (sample flask) by the operation of
rotation control knob.

Updown key
It’s the rise, descending switch of the lift.
Main unit slides in the rise direction while ∧
is being pushed and it slides in the
Glass set and bath are sold separately. descending direction while ∨ is being
pushed

Lift lower limit position control knob

It adjusts the lower limit position of lift when it
is lowered. Move the lift to the uppermost
position. Loosen the knob, push up to the
proper position and then tighten it again to
change the lowermost position of lift.

Adjuster
It is used to adjust the level of rotary
evaporator.

24
 [Link] and Function of Each Part
Other Functions

The lift up switch for the blackout

・ A lift is raised when a lift switch for the
blackout is pushed at the time of the
blackout.
・ The lift stops when a hand is left from
the lift switch.
・ It doesn't work even if a lift switch is
pushed if it is the position of the upper
limit.

How to check a battery (9V alkaline dry cell)

・ The lift is lowered with the lift down key in front of the device in the bottom position.
Next, it keeps pushing a lift switch for the blackout in the rear. Confirm whether lift is
raised to the upper limit within ten seconds.
・ When rise time is more than ten seconds, it becomes the standard of the battery
exchange time. An a little early exchange is suggested. Check a battery once a
month.
・ If battery use longtime, can not move lifter switch for power cut.
・ Change the battery once a year regardless of use frequency.

WARNING!
● Be sure to disconnect the power cord during inspection or maintenance of device.
● Do not disassemble the device.
● Check a battery once a month.
● Change the battery once a year regardless of use frequency.

25
 [Link] Precautions

WARNING!
[Link] that cannot be used
Never use explosive substances, flammable substances and substances that include explosive
or flammable ingredients in this unit. Explosion or fire may occur. (Refer to page 34 "17. List of
Dangerous Materials".)

[Link] a problem occurs

If smoke or strange odor should come out of this unit for some reason, turn off the power key
right away, and then turn off the circuit breaker and the main power. Immediately contact a
service technician for inspection. If this procedure is not followed, fire or electrical shock may
result. Never perform repair work yourself, since it is dangerous and not recommended.

[Link] not disassemble or modify this unit

Do not disassemble or modify this unit. Fire or electrical shock or failure may be caused.

4. Don't put things on Rotary Evaporator

If a thing is placed on a rotary evaporator, there is danger of fall. Moreover, if a solvent etc is
placed, there is a possibility of becoming a cause of failure.

CAUTION!
[Link] a thunder storm
During a thunderstorm, turn off the power switch immediately, then turn off the main power. If
this procedure is not followed, fire or electrical shock may be caused.

[Link] after power failure

Turn off the power switch when a power failure occurs to avoid unmanned operation.
After a power failure return, since it is dangerous that it will be in operational status by
uninhabited, please once turn off the power switch at the time of a power failure.

3. About the battery

Confirm the polarity of the electrode.
When an electrode is connected in the opposite direction, a problem occurs, and dangerous.
Don't mix the different kind of battery .
Remove a battery when you don't use for a long time.

26
 [Link] Method
Daily Inspection and Maintenance
For the safety use of this unit, please perform the daily inspection and maintenance without fail.
Using the city water to this unit might attach dirt. Do inspect and maintain this point while performing
daily inspection and maintenance.

WARNING!

• Be sure to disconnect the power cord during inspection or maintenance of device.

• Do not disassemble the device.
• Check a battery once in the moon.
• Change the battery once a year regardless of use frequency.

CAUTION!

• Wipe the dirt with soft cloth wrung out with mild detergent. Do not use benzene, thinner or
cleanser, or do not scrub it with a scrubbing brush. Deformation, deterioration or discoloration
may result in.

For any questions, contact the dealer who you purchased this unit from, or the nearest sales
division in our company.

27
 [Link] storage and disposal
When not using this unit for long term / When disposing

CAUTION!
When not using this unit for long term…
• Turn off the power and disconnect the power cord.
• Remove the battery stored by the equipment back.

WARNING!
When disposing…
• Keep out of reach of children.
• Remove and discard a power cord.
• Usually, discard by bulky garbage treatment.

Environmental protection should be considered

We request you to disassemble this unit as possible and recycle the reusable parts considering to the
environmental protection. The feature components of this unit and materials used are listed below.

Component Name Material

Exterior Parts
Outer covering Aluminum printed coating, ABS resin
Electrical Parts
Switches, Relay Composite of resin, copper and other
Circuit boards Composite of glass fiber and other
Power cord Composite of resin coating, copper, nickel and other
Wiring material Composite of flame-resistant vinyl, copper and nickel
Sticker Resin material
Battery 9V alkaline dry cell

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 [Link] the Event of Failure…
Safety Device and Error Code
Turn off the power and disconnect the plug immediately if the liquid leaks into the device. There is a
danger of electric shock if the power is turned on after the device is dried. In this case, please call the
service department of our company.
Error Code:
Check the error code and stop the operation immediately.

[Link] main unit

Error Display Cause/Solution
When abnormalities boil up on RE main unit rotor, "E04" is displayed on a screen
and rotation stops. It boil up, when motor disconnection, a motor lock, and the
inside temperature of a motor detect the abnormalities in overheating.
E04 From a glass set, please check whether the motor is locked and carry out
resumption of after-release operation of the unusual conditions.
Please carry out a service call, when you cannot cancel from a power supply
re-injection.
When abnormalities are in a storage cell, "E15" is displayed on a screen, and
E15 equipment [Link] it becomes board exchange when it cannot cancel from a
power supply re-injection, please carry out a service call.
When motor rotation speed frequency is less than 3rpm, "・・・" is displayed on a
_ _ _(Underbar)
[Link] rotation speed frequency goes up, it will return automatically.

When motor rotation speed frequency is 255rpm more, "- - -" is displayed on a
- - -（Upbar）
screen. If rotation speed frequency falls, it will return automatically.

Refer to the instruction manual of VR model for the display of abnormality on the vacuum controller.

Trouble Shooting

Phenomenon Check point

• Is the power receptacle contained?
It does not move up and down, even if
it pushes a lift up-and-down switch. • Is the breaker set to ON?
• Is already a lift in the highest score?
• If the rotor stops due to the overload on the rotor motor, turn
It does not rotate. off the power for about 30 minutes to cool inside the motor.
Remove the cause of overheat and reduce the overload.
• Check if the power source is turned to on.
Device does not start after turning on
the power switch. • Check if the power cable is securely plugged.
• Check if a power failure occurs.
• If the rotor stops due to the overload on the rotor motor, turn
Overload on rotor motor? off the power for about 30 minutes to cool inside the motor.
Remove the cause of overheat and reduce the overload.

In the case if the error other than listed above occurred, turn off the power switch and primary
power source immediately. Contact the shop of your purchase or nearest Yamato Scientific
Service Office.

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 [Link] Service and Warranty
When requesting a repair

When requesting a repair

If any trouble occurs, immediately stop operation, turn the ELB off, pull out the power plug and
contact your dealer or our sales office.

Information necessary for requesting a repair

● Model name of the product
See the warranty card or the nameplate on the unit.
● Serial number See the section “Names and Function of Parts”
● Date(y/m/d) of purchase
● Description of trouble (as in detail as possible)

Be sure to indicate the warranty card to our service representative.

Warranty card (attached separately)

● Your dealer or one of our sales offices will hand you a warranty card. Please fill necessary data
such as “dealer name, date of purchase, etc” and store at a safe place.

● Warranty period is one full year from the date of purchase. Repair service for free is available
according to the conditions written on the warranty card.

● For repaires after the warranty period consult your dealer or one of our sales office. Paid repair
service is available on your request when the product’s functionality can be maintained by repair.

Minimum holding period of repair parts

The minimum holding period of repair parts for this product is seven years after end of production.

Repair parts here refer to parts necessary for maintaining performance of the product.

30
 [Link]
[Link] main unit
Model RE301
Rotary motor DC brushless motor with feedback control
Configuratio

Rotation speed 20～250r/min

n

Lift motor Rod actuator

Use surrounding temperature
range 5～35℃
Lift stroke 130mm
Lift function Electrical operation and Auto
Display Rotation unit: liquid crystal display
Setting system Rotation unit: dial
Outer covering ABS resin, aluminum coating finish
Setting range of
―
vacuum degree
Measurement range of
―
vacuum degree
Resolution of
―
vacuum degree
Performance /function

Setting range of
―
hysteresis
Indicated resolution of
―
evaporating temperature
Indicated resolution of
cooling water ―
temperature
Operational function ―
Timer setting range ―
Memory function ―
Data operation ―
Circuit breaker・Rotor overload protection・Lower limit of lift by manual
Main unit
Safety Lift rise switch at Blackout
function Vacuum
―
controller
Interlocking function ―
glass set A W828×D400×H586
equipped (716: at lift-up)
External
Standard

dimension glass set

W643×D400×H723
B/C
equipped (853: at lift-up)
Rating Main unit: AC100V～240V 1.5A
Weight Approx. 14.1kg (Glass and bath not included)
Accessories of main unit ・Vacuum seal (1) ・Ring(large/middle/small) (each 1)
・Rotary joint retainer (1) ・Condenser fixing nut (1)
・O-ring (1) ・Coil ring (1)
Accessories ・Bath ways (1)
・Instruction manual (1)
・Warranty card (1)
・Battery(9V) (2)

31
 [Link] Diagram
・RE301 main unit

Symbol Part name

MCB Circuit protector
POWER Switching power unit
CN1 Connector (DC24V)
CN2 Connector (signal)
SW1 Limit switch (upper)
SW2 Limit switch (Lower)
SW3 Switch (for upper jack)
SW4 Switch (for lower jack)
M1 Gear motor (for jack)
DC brushless motor
M2
(for rotor)
VR Main volume
PLANAR PLANAR board
PIO Display board
CN1 Relay connector
CN2 Relay connector

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 [Link] Parts Table

1.RE301 main unit

Part Name Code No. Specification Manufacturer
Ring (large) RE50040190 Yamato Scientific
Ring (middle) LT00015384 Yamato Scientific
Ring (small) RE50040070 Yamato Scientific
O-ring 4210020010 Viton P22, Yamato Scientific
Rotary joint retainer RE50040080 Yamato Scientific
Condenser mounting nut RE50040700 Yamato Scientific
Coil ring 2551720503 SUS304WPA, Yamato Scientific
TAKACHI
Battery holder LT00033690 BH-9V-2
Electricity Industry
Refer to the instruction manual of VR model for the components of VR model.
2. Option parts
Part Name Code No. Specification Manufacturer
Teflon vacuum seal＊ ORE7042000 ORE70-42000 Yamato Scientific
Flask clamp (for
LT00034372 The product made from SUS Yamato Scientific
distillation flasks)
Flask clamp (for
RE51A0237A The product made from SUS Yamato Scientific
sample-receiving flasks)

3. Main unit related consumable part

Part Name Code No. Specification Manufacturer
Vacuum seal RE50040090 RE500-40091 Yamato Scientific
Flask clamp(1) F0410001 KC29 Black Yamato Scientific
Flask clamp(2) F0410005 KC35 Black Yamato Scientific
Nozzle Caution3 LT00016191 ORG10_4000_X Ikeda Glass
Packing for nozzle
LT00016192 ORG10_4001_X Ikeda Glass
Caution3
Cap for nozzle Caution3 LT00016193 ORG10_4002_X Ikeda Glass
Stop Cap for nozzles LT00016194 ORG10_4003_X Ikeda Glass
Packing for stopping LT00016195 ORG10_4004_X Ikeda Glass
Hose clamp LT00016196 Ikeda Glass
Battery(9V alkaline dry
LT00033689 6LR61XJ/2B 9V Two pieces Panasonic
cell)
* It is an article of consumption.
Consumable supplies related to main body

Caution:
1. Use the optional Teflon vacuum seal for ketone and an ether system solvent.
Acetone, methyl ethyl ketone, methyl isobutyl ketone, ethyl ether, and MTBE (methyl t-butyl ether) etc.
-- the case where ketone and an ether system solvent are used -- vacuum seal (NBR) of standard
attachment It will swell.
Use the fluorocarbon polymers vacuum seal of an option.
2. See the catalog of Yamato science when you replace a glass set.
3. Exchange Nozzle, Packing for nozzle and Cap for nozzle in a set.

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 [Link] of Dangerous Materials

Never use explosive substances, flammable substances and substances that include explosive
or flammable ingredients in this unit.

EXPLOSIVE
Ethylene glycol dinitrate (nitro glycol), Glycerin trinitrate (nitroglycerine), Cellulose
nitrate (nitrocellulose), and other explosive nitrate esters

EXPLOSIVE: Trinitrobenzene, Trinitrotoluene, Trinitrophenol (picric acid), and other explosive

nitro compounds
Acetyl hidroperoxide (peracetic acid), Methyl ethyl ketone peroxide, Benzyl
peroxide, and other organic peroxides

FLAMMABLE
Lithium (metal), Potassium (metal), Sodium (metal), Yellow phosphorus,
Phosphorus sulfide, Red phosphorus, Celluloid compounds, Calcium carbide,
IGNITING:
Lime phosphate, Magnesium (powder), Aluminum (powder), Powder of metals
other than magnesium and aluminum, Sodium hydrosulfite
Potassium chlorate, Sodium chlorate, Ammonium chlorate, and other chlorate
Potassium perchlorate, Sodium perchlorate, Ammonium perchlorate, and other
perchlorate
Potassium peroxide, Sodium peroxide, Barium peroxide, and other inorganic
OXIDIZING: peroxide
Potassium nitrate, Sodium nitrate, Ammonium nitrate, and other nitrate
Sodium chlorite and other chlorites
Calcium hypochlorite and other hypochlorites
Ethyl ether, Gasoline, Acetaldehyde, Propylene chloride, Carbon disulfide, and
other flammable substances having a flash point of lower than -30℃
Normal hexane, ethylene oxide, acetone, benzene, methyl ethyl ketone, and
other flammable substances having a flash point of -30℃ or higher but lower
INFLAMMABLE than 0℃
LIQUID:
Methanol, Ethanol, Xylene, Pentyl acetate (amyl acetate), and other flammable
substances having a flash point of 0℃ or higher but lower than 30℃
Kerosene, Light oil (gas oil), Oil of turpentine, Isopentyl alcohol (isoamyl alcohol),
Acetic acid, and other flammable substances having a flash point of 30℃ or
higher but lower than 65℃
FLAMMABLE Hydrogen, Acetylene, Ethylene, Methane, Propane, Butane, and other flammable
GAS: substances which assume a gaseous state at 15℃ and 1 atm

(Source: Appendix Table 1 of Article 6 of the Industrial Safety and Health Order in Japan)

34
 18. Standard Installation Manual

* Install the unit according the procedure described below (check options and special specifications
separately).

Person in charge of installation Person in charge of

Model Serial number Date Judgment
(company name) installation

№ Item Method Reference operation manual Judgment

Specifications
Check the quantities of accessories with
1 Accessories the quantities shown in the Accessory [Link] P.31
column.
・Visually check the surrounding area.
Caution: Be careful about surrounding [Link] Using This Unit
2 Installation environment. "2. Choose a proper place P.6
for installation"
・Keep space.

・ It is checked whether load is applied to

Installation
3 a cooling hose by the upper and lower [Link] Method P.13
situation
sides of a lift.
Operation
・Using a tester, measure the voltage of [Link] Using This Unit
P.6
the voltage used by the customer "1. Always ground this unit"
(distribution board, outlet, etc.).
[Link] Using This Unit
・Measure the voltage during operation
1 Power voltage "7. Choose a correct
(the voltage must be within the P.7
standard). power distribution board or
Caution: When a unit is to be connected receptacle"
to the plug or breaker, use one that
[Link] P.31
conforms to the standard.

Start of [Link] Function P.23

2 ・Start operation.
operation
.[Link] Precautions P. 26
Description
Explain the operation of each unit to the
Description of
1 customer according to this Operation All
operation
Manual.
Explain error codes and the procedure for
[Link] the Event of
2 Error code resetting them to the customer according P.29
to this Operation Manual. Failure…
Explain the operation of each unit to the
Maintenance
3 customer according to this Operation [Link] Method P.27
inspection
Manual.
・Enter the date of installation and the
name of the person in charge of
Completion of installation on the face plate on the
installation unit. [Link] Service and
4 P. 30
Information to ・ Enter necessary information on the Warranty
be entered guarantee, and pass it to the customer.
・Explain the after-sale service route to
the customer.

35
 Limited liability
Be sure to use the unit strictly following the handling and operating
instructions in this operating instruction.
Yamato Scientific Co.,Ltd. Assumes no responsibility for an accident or a
malfunction caused by use of this product in any way not specified in this
operating instruction.
Never attempt to perform matters prohibited in this operation instruction.
Otherwise, an unexpected accident may result.

Notice
● Descriptions in this operating instruction are subject to change without
notice.
● We will replace a manual with a missing page or paging disorder.

Instruction Manual for

Rotary Evaporator
Model RE301
Mar. 1, 2010

Yamato Scientific Co., Ltd.

2-1-6 Nihonbashi Honcho, Chuo-ku,
Tokyo, 103-8432, Japan
[Link]

36