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Measuring Aluminum Thickness with Isotopes

This document describes an experiment to measure the thickness of aluminum foil using a radioactive isotope and a nuclear scaler. Students will: 1. Measure counts of radioactivity passing through aluminum samples of various known thicknesses to construct a calibration curve. 2. Measure counts passing through an aluminum sample of unknown thickness and use the calibration curve to determine its thickness. 3. Verify the unknown thickness by direct measurement with a Vernier caliper. The purpose is to demonstrate how radioactive isotopes can be used as a gauge to determine thickness or depth of materials by measuring absorption of particles through samples of varying thickness.
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0% found this document useful (0 votes)
17 views7 pages

Measuring Aluminum Thickness with Isotopes

This document describes an experiment to measure the thickness of aluminum foil using a radioactive isotope and a nuclear scaler. Students will: 1. Measure counts of radioactivity passing through aluminum samples of various known thicknesses to construct a calibration curve. 2. Measure counts passing through an aluminum sample of unknown thickness and use the calibration curve to determine its thickness. 3. Verify the unknown thickness by direct measurement with a Vernier caliper. The purpose is to demonstrate how radioactive isotopes can be used as a gauge to determine thickness or depth of materials by measuring absorption of particles through samples of varying thickness.
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Purdue University Science Express

Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 1

f current which can be counted by the scaler


Previous experiments have demonstrated that various materials will shield
against alpha particles, beta particles, and gamma rays. The identity of the material, its
thickness, and its chemical composition will affect the material’s ability to absorb or
transmit these particles and rays. Thus, we can use a radioactive isotope as a gauge for
depth or thickness. We allow particles or rays to pass through materials of the same
identity but varying known thickness; we then measure the counts of radioactive
particles which pass through the sample. Once a calibration curve is constructed, a
sample of unknown thickness can be tested and compared to the curve in order to
determine its thickness
There are many engineering situations in which thickness or depth must be
precisely controlled (rolled metals like steel or aluminum, depth of material in a
container, thinness of paper or plastic lms). Industries routinely make use of
radioactive isotopes like americium 241, krypton 85, or cesium 137 for these purposes
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Purdue University Science Express


Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 2

PURPOSE
1. To measure counts of radioactivity through samples of aluminum which have various
thickness

2. To measure counts of radioactivity through samples of aluminum of unknown


thickness

3. To determine the thickness of the unknown sample using the calibration curve

4. To determine the thickness of the unknown sample using a Vernier caliper

5. If time permits, repeat the experiment with samples of other metal

SAFETY

1. Students should observe all laboratory safety precautions, including the wearing of
appropriate clothing, footwear, and safety goggles

2. There should be no eating or drinking during the experiment

3. Wash hands thoroughly after clean-up

4. Students with compromised immune systems should consult their physicians before
participating in this experiment
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Purdue University Science Express


Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 3

PRELAB QUESTIONS

1. Make a sketch of the SpecTech ST-150 nuclear scaler with its sample storage
compartment open. Draw and label these parts

sample storage compartmen


sample storage compartment doo
samples (in their storage slots
detector compartmen
source holder (top view
beta sourc
source holder with beta source, in detector compartmen
aluminum sample in detector compartmen
control button
display scree

2. What is the purpose of measuring the background count

3. Write a hypothesis statement that relates beta particle count to thickness of a


sheet of aluminum

4. Explain how we will determine the unknown thickness of the aluminum foil
sheet. Be speci c!
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Purdue University Science Express


Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 4

MATERIALS PER GROUP

SpecTech ST-150 nuclear scale


assorted samples of metal of various thicknesse
radioactive source
forcep
vernier calipe
aluminum foi
milligram balanc
metric rule
scissor

PROCEDURE for college preparatory Chemistry or Physics students:

INSTRUMENT SETUP
1. Put on your safety apparel and equipment as speci ed by your teacher
2. Obtain the materials listed above, and take them to your lab bench. Make sure
that the scaler is near an electrical receptacle. Also make sure that the radioactive
source is at least one meter away from the detector until you are ready to place it
in the detector compartment
3. Open the door to the sample storage compartment. Ensure that there are
samples in each of the eleven slots and that there is also a clear plastic source
holder in slot number 5
4. Remove the source holder from slot number ve. Slide the empty source holder
onto the bottom shelf of the detector compartment
5. Connect the power cable to the electrical receptacle, and switch on the scaler
6. Press the “H.V.” button one time to set the detector voltage; the red light should be
lit. Press the “UP” button several times until the display reads “460”. Press the
“H.V.” button again to turn off the red light. You have just set the voltage in the
detector tube to 460 Volts
7. Press the “TIME” button one time to set the sampling time; the red light should be
lit. Press the “UP” button several times until the display reads “90.” Press the
“TIME” button again to turn off the red light. You have just set the sampling time to
90 seconds.

continued. . .

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Purdue University Science Express


Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 5

MEASURING THE BACKGROUND COUNT


8. Press the count button one time. The red light above the “COUNT” button will be
lit. The instrument will begin to count the number of times that a particle is
absorbed by the detector tube. The instrument will keep counting for 90 seconds,
at which time the red light above the “COUNT” button will go out. The display is
now displaying the number of particles absorbed by the detector tube in 90
seconds. This is the “background” count from the environment around the
instrument. Record this data in your data table
9. Repeat step 8 until you have made three determinations of the background count

DATA COLLECTION FOR THE Al SAMPLES OF KNOWN THICKNESS


10. Place the beta source into the circular depression of the source holder, and
replace it onto the bottom shelf of the detector compartment
11. Obtain aluminum sample number 5 from the sample storage compartment, and
place it onto the second shelf from the top of the detector compartment .
12. Press the count button one time. After the instrument completes the 90 second
count, record your data. Repeat until you have made three determinations with
this piece of aluminum.
13. Repeat steps 11 and 12 using aluminum sample number 6
14. Repeat steps 11 and 12 using aluminum sample number 7
15. Repeat steps 11 and 12 using aluminum sample numbers 5 and 6, placing them
both on the same shelf
16. Repeat steps 11 and 12 using aluminum sample numbers 5 and 7, placing them
both on the same shelf
17. Return the aluminum samples to their correct slots in the sample storage
compartment
18. Record the thickness data for the aluminum samples from the “door” of the sample
storage compartment. Be sure to record the thickness both in inches and in mg/
cm2
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Purdue University Science Express


Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 6

DATA FOR THE Al FOIL OF UNKNOWN THICKNESS


19. Remove sample number 6 from the sample compartment. Trace its outline onto
the surface of the aluminum foil. Use scissors to carefully cut the foil.
20. Place the aluminum foil square onto sample number 6 and place both onto the
second shelf from the top of the detector compartment .
21. Press the count button one time. After the instrument completes the 90 second
count, record your data. Repeat until you have made three determinations with
this two-piece thickness of aluminum.
22. Measure and record the length, width, and mass of the aluminum foil piece you
made
23. If available, use calipers to measure the thickness of the aluminum foil piece you
made

CLEANU
24. Return all samples to their proper places in the sample storage compartment
25. Turn off the scaler, and then un-plug it from the receptacle
26. Return all materials as directed by your teacher.
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Purdue University Science Express


Thickness of Aluminum Foil Using Radioactive Isotope and Nuclear Scalers, page 7

Common questions

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The purpose of creating a calibration curve is to establish a relationship between the thickness of aluminum samples and the counts of radioactive particles that pass through them. This allows for the determination of the unknown thickness of an aluminum sample by comparing its particle count against this pre-determined curve .

To determine unknown thickness, count the radioactive particles passing through the sample using a calibrated curve. Additionally, measure directly with vernier calipers for a physical thickness assessment. Using both methods provides cross-verification, enhancing accuracy and reliability by combining indirect and direct measurement approaches .

Using multiple aluminum samples with known thicknesses during calibration is necessary to develop an accurate calibration curve. It ensures that the relationship between the thickness and the radioactive particle count is well defined across a range of thicknesses, leading to more precise thickness measurements of unknown samples .

The SpecTech ST-150 nuclear scaler is used to detect and count radioactive particles passing through the aluminum samples. It allows the user to set parameters such as detector voltage and sampling time, facilitating the accurate capture and recording of particle counts necessary for analyzing sample thickness .

The chemical composition of a material affects its density and atomic structure, which in turn influences its ability to absorb radioactive particles. Materials with higher atomic numbers and densities generally have a greater ability to absorb particles and rays, resulting in fewer particles passing through them. This property is essential for determining the suitability of materials for shielding against radiation .

Repeating measurements with other metals helps illustrate the broader applicability of the radioactive isotope method and demonstrates how different materials respond to radiation due to variations in composition and density. This variation can reinforce understanding and adaptability of the technique in real-world scenarios .

Radioactive isotopes, such as americium 241, emit particles that can penetrate materials. By measuring the number of these particles that pass through metal sheets of known thickness, a calibration curve can be developed. This allows for the determination of unknown metal thickness by comparing particle counts through these samples. This method is routinely used in industries where controlling the thickness of materials like rolled metals is critical for quality and performance .

Safety precautions include wearing appropriate clothing, footwear, and safety goggles, avoiding eating or drinking during experiments, washing hands thoroughly after cleanup, and individuals with compromised immune systems consulting physicians before participating. These measures minimize exposure and ensure safe handling of radioactive materials .

Challenges include ensuring safety during handling of radioactive materials, potential inaccuracies due to environmental radiation affecting counts, and the need for precise calibration curves. Moreover, material composition and uniformity must be consistent to avoid errors in measurements. These challenges necessitate careful protocol adherence and environmental controls .

Measuring the background radiation count is crucial because it accounts for ambient radiation that can interfere with the accurate measurement of radioactive particle counts through the aluminum samples. This baseline ensures that subsequent counts can be adjusted so that only radiation attributed to the experiment is considered .

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