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CHEMICAL ENGINEERING DEPARTMENT
PARTICULATE TECHNOLOGY PRACTICAL MANUAL
NAME:
FATHER’S
NAME
ROLL
NUMBER
CHEMICAL ENGINEERING DEPARTMENT LAB TRAINER
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GROUP
NUMBER
BATCH
SECTION
CERTIFICATE
This is to certify that Mr/Ms…………………………………………………………… bearing
Roll#...................................... of Batch……………………………………….. has successfully completed
all the labs prescribed for the course of INSTRUMENTATION AND PROCESS CONTROL.
________________ ______________________
External Examiner Lab Engineer (Instructor)
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CHAIRPERSON
Dr. Abdul Karim Shah
DEPARTMENT OF CHEMICAL ENGINEERING
DAWOOD UNIVERSITY OF ENGINEERING AND TECHNOLOGY, KARACHI
Course Learning Outcomes (CLO)
CLO 1 Demonstrate the operation of basic equipment involved in Level 3
instrumentation and process control.
Level 4
CLO 2 Calibration and error calculation on basic control devices.
Level 2
CLO 3 Deliver oral reporting on instrumentation and process experiments.
Marks Distribution
% Marks CLO Distribution ( Full Marks)
Assessment Tools Total Total
[Link]: Overall Actual CLO 1 CLO 2 CLO 3 CLO 4
(AT) Marks CLOs
1 Abstract 3 1.5 1.5 3 2
2 Introduction 3 1.5 1.5 3 2
Manual
Experimental
20 6 6 6 1
Procedure
Results and graph 3 1.5 1.5 3 2
3 Discussion 5 2.5 2.5 5 2
4 Appearance 3 3 3 1
Exam
Final
15
5 Greetings 3 3 3 1
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6 Communication 3 3 3 1
7 Subject Knowledge 6 3 3 6 2
8 Subjective 15 15 7.5 7.5 15 1
Total 50 26.5 23.5 0 50
CLO Contribution
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Table of Content
S# DATE OBJECT PAGE# CLO ABSTRACT INTRODUCTION EXPERIMENTAL RESULT DISCUSSION TOTAL SIGN
PROCEDURE
3 3 6 3 5 20
1. 1 Student Laboratory Code of
Conduct
2. 1 To Investigate the Source of
a Error When Measuring
Pressure
3. 2 To Investigate the error of
a pressure measuring device and
also discuss calibration
4. 2 Process Control Unit
b
5. 3 Process Control Unit (Pressure)
a
6. 3 Study the temperature
b measuring devices
7. 4 Study the temperature
a measuring devices
8. 4 Feedback ward and Feed
b forward Control
9.
10.
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RUBRICS FOR ASSESSMENT OF LAB MANUAL
CRITERIA PERFORMANCE
Beginning or Developing Accomplished Exemplary
incomplete 1 marks 2 marks 3 marks
0 marks
Abstract/summary Several major aspects Abstract misses one Abstract reference Abstract contains
3 marks of the experiment are or more major aspects most of the major reference to all major
missing, student of carrying out the aspects of the aspects of carrying
displays a lack of experiment or the experiment, some out the experiments
understanding about result minors details are and the result , well
how to write an 1 marks missing written
abstract 2 marks 3 marks
0 marks
Introduction Very little Some introductory Introduction is nearly Introduction complete
3marks background information , but still complete missing and ell written;
information provided, missing some major some minors points provides all necessary
or information is points 2 marks background
incorrect 1 marks principles for
0 marks background
principles for the
experiment
3 marks
Experimental Missing several Written in paragraph Written in paragraph Written in paragraph
procedure important format, still missing format, still missing format, all
6 marks experimental details some important some minor experimental details
or not written in experimental details experimental details covered
paragraph format 2 marks 4 marks 6 marks
0 marks
Results: Figures , graph , Most Figures , graph , All Figures , graph , All Figures , graph ,
data;figure,graph, tables contain errors tables is OK still tables is OK still some tables is OK , are
table;etc or poorly constructed, some important minor important numbered contain
3 marks have missing titles, details missing details missing title/caption
captions or numbers , 1 marks 2 marks 3 marks
unit missing
0 marks
Discussion Very incomplete or Some of the result Almost all of the All important trends
5 marks incorrect have been correctly results have been and data comparison
interpretation of trend interpreted and correctly interpreted have been interpreted
and comparison of discussed partial but and discussed only correctly and
data indicating a lack incomplete minor improvement discussed good
of understanding of understanding of the are needed understanding of
result result is still evident 3 marks result is conveyed
0 marks 2 marks 5 marks
Total=20 Marks/50 Marks
RUBRICS FOR CONDUCT OF VIVA VOCE
CRITERIA unacceptable Needs acceptable Proficient
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improvement
Appearance Overall appearance is Appearance Overall neat Overall appearance is
3 marks untidy somewhat untidy; appearance choice in very neat choice in
Choice in clothing is choice in clothing is clothing is acceptable clothing is
inappropriate for appropriate (shirt un- for the types of viva appropriate for viva
viva(torn, unclean, tucked, tee-shirt, too Well groomed(shirt Very groomed (hair,
wrinkled) much jewelry etc.) tucked in, jewelry makeup, clothes
Poor grooming 1 marks blends with clothing, pressed, etc.)
0 marks minimal wrinkles) 3 marks
2 marks
Greeting Unacceptable Used typical Acceptable behavior,
Professional behavior
3marks behavior and behavior and well mannered, and language
language language –did professionalism (handshake, hello,
Unfriendly and notmodify behavior to somewhat lacking thank you etc.)
courteous fit the viva courteous to all Friendly and
0 marks Attempt to be involved in viva courteous to all
courteous to all in 2 marks involved in viva
viva sittings 3 marks
1 marks
Communication Speaking is Speaking is Speaking is cleared Speak clearly and
3 marks uncleared- very uncleared-lapses in with minimal mistakes distinctly with no
difficult to understand sentence structure in sentence structure lapse in sentence
messeage of what is and grammar and grammar structure and
being said(mumbling) 1 marks 2 marks grammar usage;
volume is speaks concisely with
inappropriate for viva correct pronunciation
(spoke too loudly) 3 marks
0 marks
Subject knowledge Student does not have Student is Students is at ease with Student demonstrate
6 marks grasp of information ; uncomfortable with information and gives full knowledge(more
structure cannot information and can expected answer to all than required) and
answer question answer only question but fail to answer all question
about subject rudimentary question elaborate with explanation and
0 marks 2 marks 4 marks elaboration
6 marks
Total=15 Marks/50 Marks
GUIDELINE FOR ABSTRACT WRITING
An abstract is an important part of any academic/ professional paper /manual/folder. This briefs overview
serves as a summary of what your paper/manual contains, so it should succinctly and accurately represent
what your paper/manual is about and what the reader can expect to find.
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Fortunately, by following a few simple guidelines, you can create an abstract that generates interest in
your work and help readers quickly learn if the paper/manual will be of interest to them.
The purpose of your abstract is to provide a brief yet thorough overview of your paper/manual. your
abstract should function much like your title page ,it should allow the person reading it too quickly
determine what your paper/manual is all about.
Your abstract is the first thing that most people will read, and it is usually what informs their decision to
read the rest of your paper. A good abstract lets the reader know that your paper is worth reading.
According to the official guidelines, a good abstract should be:
1. Brief but packed with information. Each sentence must be written with maximum impact in
mind. To keep your abstract short, focus on including just four or five of the essential points,
concepts, or findings.
2. Objective and accurate. The abstract's purpose is to report rather than provide commentary. It
should also accurately reflect what your paper is about. Only include information that is also
included in the body of your paper.
GUIDELINE FOR INTRODUCTION
Introduction is an important part of any paper/article/manual etc. it can reflects the overview of basics of
your article, major aspects, its history and your future goal.
When you Introduction of your article you should remember in your mind each paragraph must have only
one topic major aspects to be discussed with proper grammar and punctuation
GUIDELINE FOR EXPERIMENTAL PROCEDURE
Experimental procedure should cover all the steps which would be done during performance of
experiments.
Each step must write in a single line. Each line may contain number of sentences
GUIDELINE FOR RESULTS
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Each experimental data can be used for further calculation and plotting of graph.
Do calculation neat and clean with proper accurate formula with its reference.
Graph should be plot on graph paper, rough sketch not acceptable
Units must be written, all calculation must be unit consistent
Any schematic diagram if required to be sketch, it should be clean and draw with pencil, don’t used
marker, ballpoint for schematic diagram and graph
DISCUSSION
It should cover overall experiments and its outcomes, limitation and errors, comparison of data
GUIDELINE FOR PERFORMANCE
1. Student should use proper PPEs (PERSONAL PROTECTIVE EQUIPMENTS) i.e. lab
coat, gloves, goggles etc.
2. Sandal, slippers not allowed during lab performance
3. Mobile phones strictly prohibited during lab performance
4. Do not used rubber shoes
5. Loss clothing not allowed during lab performance
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SAFETY RULES AND REGULATIONS
The rules and regulations that follow are universal for the laboratories. In addition to becoming
familiar with these, take note of safety warnings given with specific experiments. These are
noted in this manual.
1. Housekeeping: All designated experimentation areas should be left in a neat orderly
state at the conclusion of an experiment. The following items should be checked:
1. All excess water should be removed from the floor.
1. All loose paper should be picked up and deposited in trashcans.
2. All working surfaces (tables, chairs, etc.) should be cleaned if needed.
3. All miscellaneous items should be returned to their proper initial locations (kits to
stockroom, tools to tool shop, chemicals and glassware to proper stockroom).
4. All hoses should be coiled and placed in designated locations.
5. All glassware should be washed prior to returning to the stockroom.
1. All scales should have weights removed and scale arms locked.
2. All manholes (sewers) should have their lids closed.
3. All drums or containers used should be checked.
4. Check all valves and electrical units. Turn off what is required.
1. Horseplay: Repeated incidents are unprofessional, and will result in a grade penalty.
1. Equipment Difficulties: The student is encouraged to correct any minor equipment
difficulties by taking the appropriate action. However, any major equipment difficulties
should be reported to the lab attendant, instructor, or teaching assistant and the student
should not attempt any further corrective action.
1. Tools: Tools should not be taken out of any stock or maintenance rooms without
checking them out with the designated responsible person. Any tools checked out should
be returned immediately at the completion of their required task.
1. Chemicals: In several of the experiments, chemicals are required to perform the
experiment. Student should check with their instructor as to where to get these chemicals
and what safety precautions, if any, are to be taken in conjunction with the use of these
chemicals. In the case of gases being used, be sure you understand the nature of the hazards
associated with the gas and do not deviate from the procedures as outlined, either oral or
written, by the instructor. Do not use mouth suction to fill pipettes. Waste chemicals are
placed in receivers and are not discharged in the drain.
1. Electrical: In many stances electrical extension cords are required for the operation of
auxiliary equipment. Special precautions should be taken when using these cords. When an
electrical extension cord is checked out, be sure to examine its condition. If you find frayed
or broken wires, insulation broken, prongs bent, no ground, etc. do not use but return to the
stockroom, pointing out the faults to the technician. When using extension cords, be sure
they do not lie on the floor, in particular, when the floor is wet, but are safely supported in
such a fashion that they are not a bodily hazard. When making electrical connections, be
sure the area you are standing in is dry.
1. Accidents: Even with the greatest safety precautions accidents do happen. If any
accident happens, be sure to immediately inform instructor. In the case of serious accidents,
do not attempt first aid, if you are not familiar with the proper technique but do attempt to
make the person comfortable until aid arrives.
1. Unauthorized Areas: Do not touch unauthorized equipment or experiments.
1. Food or Drink: Food and drink are forbidden in laboratories.
1. Smoking: Smoking is not permitted.
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1. Ventilation: Be sure that hoods are functioning, and that your work areas are properly
ventilated.
1. Attendance: Everyone is required to attend each lab class. If you cannot attend, be sure
to notify the instructor prior to the class, as well as your lab partners. Consistent failure to
observe this rule is considered unprofessional behavior, and will be penalized.
1. Obligation: Each student has a professional obligation to contribute a full and honest
effort in the group execution of experiments and reports.
LIST OF EQUIPMENTS IN PARTICULATE TECHNOLOGY LABORATORY
S# EQUIPMENT REF COMPANY/ PURCHASE MANUAL MADE
UNIT VENDOR YEAR PRESENT OR
NOT
01 Process Control Unit UCP 2004 Yes Spain
02 Process Control Unit UCP-P 2003 Yes Spain
(pressure )
03 Bourdon Gauge Yes Spain
--------
04 Temperature TEMP 2007 Yes GERMANY
Measurement
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LAB NO. 2
TO INVESTIGATE THE SOURCE OF ERROR
ABSTRACT
EQUIPMENT/ACCESSORIES
INTRODUCTION
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EXPERIMENTAL PROCEDURE
OBSERVATIONS & CALCULATIONS
RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
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LAB NO. 3
TO INVESTIGATE THE ERROR OF PRESSURE MEASURING
DEVICE AND ALSO DISCUSS CALLIBRATION
ABSTRACT
EQUIPMENT/ACCESSORIES
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INTRODUCTION
EXPERIMENTAL PROCEDURE
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OBSERVATIONS & CALCULATIONS
RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
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LAB NO. 4
PROCESS CONTROL UNIT
ABSTRACT
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EQUIPMENT/ACCESSORIES
Components of UCP:
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
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13.
14.
INTRODUCTION
EXPERIMENTAL PROCEDURE
OBSERVATIONS & CALCULATIONS
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RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
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LAB NO. 5
PROCESS CONTROL UNIT (PRESSURE)
ABSTRACT
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EQUIPMENT/ACCESSORIES
Description of the Components:
1. Control Valves:
1. I/P Converter:
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2. Pneumatic Valve:
3. Pressure Sensor:
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4. Differential Pressure Sensor:
5. Flowmeter:
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INTRODUCTION
EXPERIMENTAL PROCEDURE
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OBSERVATIONS & CALCULATIONS
RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
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LAB NO. 6
STUDY THE TEMPRATURE MEASURING DEVICES
ABSTRACT
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EQUIPMENT/ACCESSORIES
INTRODUCTION
EXPERIMENTAL PROCEDURE
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OBSERVATIONS & CALCULATIONS
RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
LAB NO. 7
STUDY THE TEMPRATURE MEASURING DEVICES
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ABSTRACT
EQUIPMENT/ACCESSORIES
INTRODUCTION
EXPERIMENTAL PROCEDURE
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OBSERVATIONS & CALCULATIONS
RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
LAB NO. 8
FEED BACK CONTROL AND FEED FORWARD CONTROL
ABSTRACT
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EQUIPMENT/ACCESSORIES
INTRODUCTION
EXPERIMENTAL PROCEDURE
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OBSERVATIONS & CALCULATIONS
RESULTS (Should be written by student as per the instruction provided during lab)
DISCUSSION (Should be written by student as per the instruction provided during lab)
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