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Rheology Lab: Viscosity Analysis

This document summarizes an experiment measuring the viscosity of various fluids using a rotational viscometer. Water and vegetable oil were found to be Newtonian fluids based on the linear relationship between torque and rpm. Applesauce exhibited pseudoplastic behavior with decreasing viscosity under increasing shear rates. A cornstarch-water mixture showed dilatant properties with increasing viscosity under shear. Future experiments should test all fluids using all spindle sizes and rpm levels for more accurate viscosity measurements.

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Jennifer Jury
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0% found this document useful (0 votes)
21 views6 pages

Rheology Lab: Viscosity Analysis

This document summarizes an experiment measuring the viscosity of various fluids using a rotational viscometer. Water and vegetable oil were found to be Newtonian fluids based on the linear relationship between torque and rpm. Applesauce exhibited pseudoplastic behavior with decreasing viscosity under increasing shear rates. A cornstarch-water mixture showed dilatant properties with increasing viscosity under shear. Future experiments should test all fluids using all spindle sizes and rpm levels for more accurate viscosity measurements.

Uploaded by

Jennifer Jury
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOC, PDF, TXT or read online on Scribd

1

BE 333
Rheology Lab: Viscosity
December 1, 2009
Jennifer Jury
2

Abstract
Viscosity data was collected for four fluids: water, vegetable oil, applesauce, and a
cornstarch and water mixture, at room temperature. Data was obtained using a rotational
viscometer at speeds of 50-1000 rpm. The governing equations for calculating shear and
torque were τ = F/A and T = r*F. When torque is calculated and graphed against rpm
values, the resulting graphs (Figures 1-4) indicate whether the fluid is Newtonian or not.
In the mentioned Figures, it is apparent that water and vegetable oil are Newtonian while
applesauce and the cornstarch mix are not.
3

Table of Contents
Abstract 2
Introduction 4
Discussion 4
Conclusion/Recommendations 5
Reference 6
Appendix 7
4

Introduction
The purpose of this experiment was to determine the viscosities of various fluids
and determine whether the fluids were Newtonian or non-Newtonian and further classify
them to be pseudoplastic or dilatant. The fluids used in this experiment were water,
vegetable oil, applesauce, and a mixture corn starch and water. A Newtonian fluid has a
linear relationship between the applied shear stress and the rate of deformation.
Biological fluids generally act as non-Newtonian fluids. The viscometer must first be
calibrated by lifting different test weights against the force of gravity, calculating the
torque (N*m) and relating to the voltage output of the rheometer. A large diameter
cylinder will be used for fluids with low viscosity and a small diameter cylinder for fluids
with high viscosity. The voltage output for each test will be recorded in LabView. It is
recommended that we use the largest spindle for the fluid with the lowest viscosity, thus
spindle 1 was used for water and oil while spindle 3 was used for the applesauce and
cornstarch. The second was used in this lab in applesauce but did not yield acceptable
data.

Discussion
Using the dial on the viscometer, the cylinder will rotate at different speeds
causing the fluid to shear at different rates. We observed whether the rate of shear has
any effect on the viscosity of the fluid. The experiment was performed using water,
vegetable oil, applesauce, and a water/corn starch mix. As seen in the attached figures 3
and 4, the data was somewhat skewed.
Assuming rpm is proportional to shear rate and torque for the rheometer is
proportional to shear stress, a plot of torque versus rpm will be a straight line for
Newtonian fluids. The plot will be curved for a non-Newtonian fluid. Given this
information, we can see from figure 1 and 3 that water and vegetable oil are Newtonian
fluids while the applesauce and corn starch are not. Applesauce acts as a pseudoplastic or
shear-thinning fluid with viscosity decreasing as the rate of shear increases. The
cornstarch and water mixture is dilatant which means its viscosity increases as it is
stirred. These can easily be seen in the graphs of the appendix. The nature of these fluids
is important when designing various structures, for example so that their behavior can be
5

taken into account. As said before, since most biological fluids are non-Newtonian, such
as blood and fluids in the body, it is important to understand how they will behave to
understand how it functions in the body and how a blood sample may behave in different
tests.

Recommendations
For future experiments in this class, we advise that the rheometer run at all 8 levels of
rotational speed to get a more accurate graph. Also, use all spindles in all fluids to see
the variances in force, torque, and shear.
6

References
BE333 Biosystems Engineering Laboratory. Lab 12: Rheology 2009.
Jones, [Link] into Science.
[Link]://[Link]/viscosity_overview.htm#Newtonian

Common questions

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Understanding whether a fluid is pseudoplastic or dilatant is crucial because it affects how the fluid will behave under stress, which is important for applications and design. Pseudoplastic (shear-thinning) fluids like applesauce decrease in viscosity under shear, useful in applications requiring easy spreading or mixing. In contrast, dilatant (shear-thickening) fluids like the cornstarch mixture increase in viscosity when stirred, which is significant in designing materials that harden under stress, such as protective gear . Understanding these properties also allows engineers to take these behaviors into account when designing equipment and processes that involve these fluids .

Calibrating the rheometer is significant because it ensures accurate readings of torque and voltage output, which are essential for calculating shear stress and determining fluid properties . Calibrating involves lifting different test weights against gravity to relate torque to the voltage output, providing a baseline for measurements . Spindle selection is based on the viscosity of the fluid: large diameter cylinders are used for low viscosity fluids, while small diameter cylinders are for high viscosity ones. Spindle 1 was used for water and oil, and spindle 3 for applesauce and cornstarch due to their higher viscosities .

The classification of most biological fluids as non-Newtonian has significant implications for biomedical engineering. It means that these fluids, such as blood, do not have a constant viscosity and their behavior can change under different flow and shear conditions. This affects the design of medical devices and processes, such as blood pumps and diagnostics, where understanding fluid dynamics is vital for ensuring functionality and accuracy . Additionally, this knowledge aids in the understanding of physiological processes and disease states, where fluid dynamics plays a role .

Understanding fluid viscosity plays a crucial role in designing structures and systems because it affects how fluids flow and behave under different conditions, impacting system efficiency, safety, and performance. For instance, in systems involving fluid transport or processing, misjudging viscosity properties can lead to inefficient designs or system failures. It also aids in selecting appropriate materials and methods to handle specific flow characteristics required for specific applications, such as in food manufacturing or with complex biological fluids .

The experiment uses a rotational viscometer to rotate a cylinder at different speeds, causing the fluid to shear at various rates . By plotting torque versus rpm, which is proportional to shear stress and shear rate respectively, a linear graph indicates a Newtonian fluid while a curved graph indicates a non-Newtonian fluid . The use of different spindles and the calibration of the viscometer by lifting test weights to calculate torque aids in this determination .

The experimental results were described as somewhat skewed, likely due to limitations or errors in the experimental setup or data collection methods, such as instrument calibration errors or inconsistent spindle usage . This skewness could impact the reliability and accuracy of the conclusion regarding whether a fluid is Newtonian or non-Newtonian, potentially affecting the classification and understanding of fluid properties . Ensuring precise calibration and experimental conditions is vital for drawing accurate conclusions.

To improve the accuracy of experimental results in rheology labs, it is recommended to run the rheometer at all 8 levels of rotational speeds to obtain a more accurate graph and use all available spindles in all fluids to observe variances in force, torque, and shear .

Newtonian fluids have a linear relationship between the applied shear stress and the rate of deformation, meaning their viscosity remains constant regardless of the shear rate. In the experiment, water and vegetable oil were identified as Newtonian fluids . Non-Newtonian fluids do not have a constant viscosity; they can be further classified based on how their viscosity changes with shear rate. Applesauce and the cornstarch and water mixture were identified as non-Newtonian fluids . Applesauce acts as a pseudoplastic or shear-thinning fluid, where viscosity decreases with an increasing shear rate, whereas the cornstarch and water mixture is dilatant with viscosity increasing as it is stirred .

For future rheology studies, it is recommended to ensure comprehensive data collection by running the rheometer at all levels of rotational speeds and utilizing all available spindles across different fluid types . This approach helps capture a wide range of data regarding the variance in force, torque, and shear, leading to more accurate and insightful graphs and a better understanding of fluid behaviors .

Pseudoplastic fluids, or shear-thinning fluids, decrease in viscosity as the shear rate increases, which can be advantageous in processes requiring easier flow and mixing, such as in paints or biological fluids like blood . Dilatant fluids, or shear-thickening fluids, increase in viscosity with an increased shear rate, making them useful in applications where increased resistance is desired, such as impact-resistant materials like body armor . These differing behaviors must be understood for effective product formulation and handling processes across industries.

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