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Sulfur Guard Bed Process Specification

This document provides specifications for a sulfur guard reactor including: - Operating data such as inlet/outlet temperatures, pressures, and gas flow rates. - Reactor vessel details like dimensions, materials, insulation, and connections. - Catalyst bed layout including the number and type of catalyst layers and support design. - Requirements for nozzles, pipes, and analysis points.

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100% found this document useful (1 vote)
140 views5 pages

Sulfur Guard Bed Process Specification

This document provides specifications for a sulfur guard reactor including: - Operating data such as inlet/outlet temperatures, pressures, and gas flow rates. - Reactor vessel details like dimensions, materials, insulation, and connections. - Catalyst bed layout including the number and type of catalyst layers and support design. - Requirements for nozzles, pipes, and analysis points.

Uploaded by

idilfitri
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
  • Process Specification Overview
  • General Reactor Datasheet
  • Reactor Diagram
  • Reactor Internal Details
  • Technical Nozzle Design

Document ID

S-03848 P52002-R 1
Job No. Doc. No Rev.
Page Item No.
Sulfur guard
1 of 5
09-R-0002

Process Specification
for
09-R-0002
Sulfur guard

Revision Description Date Made By Chd. By Appd. By


0 First Issue 29-Jul-2013 GOPA ANKS JYH
1 Revised as Indicated 23-Aug-2013 GOPA ANKS JYH
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Document ID
S-03848 P52002-R 1
Job No. Doc. No Rev.
Page Item No.
Sulfur guard
2 of 5
09-R-0002

Datasheet for General Reactor


General Equipment Information
Design case SOR
Location Outdoor
Reference Documents
Catalyst specification, document ID S-03848 P44003
Specification for reactor filling materials, document ID S-03848 P44004

Operating Data
Inlet
Temperature 410 F Pressure 1154 psig
Gas flow 401246 lb/h Gas density 1,34 lb/ft
Gas mole weight 11,04 lb/lbmol
Outlet
Temperature 401 F Pressure 1147 psig
Gas flow 401246 lb/h Gas density 1,34 lb/ft
Gas mole weight 11,04 lb/lbmol

Reactor Vessel
Mechanical Design Conditions
Fluid description Synthesis gas
Design temperature (min.) 14 F Design pressure (min.) psig
Design temperature (max.) 490 F Design pressure (max.) 1440 psig
1 Design H2 partial pressure 1020 psia
Vessel
Inner diameter 169 154 in Tangent to tangent distance 159 in
Construction code ASME Sec. VIII Stress relieving According to code
Construction material 1) SS304L Corrosion allowance 0 in
Insulation purpose Hot Insulation thickness in
Top head type Spherical Bottom head type Spherical

Catalyst Bed
Reactor Inlet Arrangement
Type Gas distributor Topsoe standard 4-1328/U
Layers (from Top)
Description Size Volume Unit Height Unit Rem.
Ceramic balls 1" 37,5 ft 4 in
HTG-1 5 mm rings 213,6 ft 20,75 in
HTZ-51 4 mm ext. 2069,7 ft 193,5 in
Ceramic balls 1" 157,2 ft 6 in
Catalyst Bed Support
Type Ellipsoidal dish Topsoe standard 3-1998/U
Ellipsoidal dish diameter 84,75 in Perforated dish diameter 67,75 in
Design Load for Catalyst Bed Support
Catalyst/inert weight 208592 lb Total design weight (as load) 12 psi
Design pressure drop 9 psi Total design load 21 psi

Nozzles and Connections


Ref. No. Size Description Nozzle Device
A 1 18" 20"
Inlet
B 1 18" 20"
Outlet
H 1 12" Handhole Catalyst unloading pipe
M 1 24" Manhole
O1-O2 2 2" Analysis point
Catalyst unloading pipe details (nozzle H)
The catalyst unloading pipe is to be filled with 1" ceramic balls and the pipe must extend 4 inch above the wire mesh.
The inclination of the pipe is to be minimum 30 to horizontal downwards.
A catalyst retaining lid is to be installed, reference is made to Topsoe standard 4-1320/U.

Remarks
1 Alternatively 1.25 Cr 0.5 Mo cladded with SS304L may be used.
L2 DC1 C2 gopa 1604218
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Document ID
S-03848 P52002-R 1
Job No. Doc. No Rev.
Page Item No.
Sulfur guard
3 of 5
09-R-0002

169

All sketch measurements are indicated in inches.


Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Document ID
S-03848 P52002-R 1
Job No. Doc. No Rev.
Page Item No.
Sulfur guard
4 of 5
09-R-0002

All sketch measurements are indicated in inches.


Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Document ID
S-03848 P52002-R 1
Job No. Doc. No Rev.
Page Item No.
Sulfur guard
5 of 5
09-R-0002

All sketch measurements are indicated in inches.


Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS

Document ID
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
Document ID
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
Document ID
5
Information contained herein is confidential; it may not be used for any purpose other than for which it has be
Document ID
5
Information contained herein is confidential; it may not be used for any purpose other than for which it has be
Document ID
5
Information contained herein is confidential; it may not be used for any purpose other than for which it has be

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