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Designing Efficient Parallel-Plate Separators

This document describes a method for designing parallel plate separators to separate oil globules from water. These separators are smaller and more efficient than traditional American Petroleum Institute separators. The design method involves calculating the retention time, transversal area, and length of the separator based on factors like flow rate, viscosity, plate spacing, and rising velocity of oil globules. Nomographs are provided to help designers determine the separator dimensions given specific conditions. An example calculation demonstrates how to use the nomographs to size a separator for a given oily water flow.
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0% found this document useful (0 votes)
45 views4 pages

Designing Efficient Parallel-Plate Separators

This document describes a method for designing parallel plate separators to separate oil globules from water. These separators are smaller and more efficient than traditional American Petroleum Institute separators. The design method involves calculating the retention time, transversal area, and length of the separator based on factors like flow rate, viscosity, plate spacing, and rising velocity of oil globules. Nomographs are provided to help designers determine the separator dimensions given specific conditions. An example calculation demonstrates how to use the nomographs to size a separator for a given oily water flow.
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

Designing

parallel-plates separators
Here is a way to design parallel-plates interceptors to separate
oil globules from water. According to the author, in addition to
being smaller, these interceptors are in many ways superior
to widely used separators for this type of servicf;.
*

Jdw G. Miranda, Empresa Nacional del Petr&lo


4

0 Traditionally, oil-water separation in d u e n t s from


petroleum refineries has been achieved by means of the
American Petroleum Institute ( M I ) type separators as
the first separation step. Even though a properly designed API separator is very efficient and easy to operate, it has disadvantages that in some cases are very
difficult to overcome. Typical problems are: construction cost, space requirements, evaporation losses, fire

hazard, high steam-consumption to avoid freezing of


heavier products, etc.
An APT separator has been designed to allow oil
globules 0.015 cm dia. and larger to rise from the separator bottom (at the entrance of the unit) to the liquid
surface, just before the outlet of the separator. In other
words, the globules have to cross the entire separator

DESIGNING PARALLEL-PLATESSEPARATORS

95

Parallel-plates-separatoroperation
The difficulties mentioned above have been minimized by the parallel-plates interceptor (PPI), a different type of separator first introduced by Shell Oil Co. in
1950, and whose use has received wide acceptance during the last years.
By means of a PPI, the oil path has been reduced to a
slight distance by a set of parallel plates inclined at 45
deg. Oil coagulates at the undersurface of each plate
and slides upward to the liquid surface where it can be
skimmed off. Furthermore, solid particles collect on top
of each plate and slide down to the bottom. These
properties make a PPI much smaller t h h its equivalent
API separator, which allows automatic oil recovery
without skimmers, with only one pump (see Fig. l), and
by means of two weirs o$.different heights { I ] .
Although the PPI has been increasing in popularity,
very little has been written about criteria to get a sound
design of this separator. This article deals with a theoretical design approach that agrees fairly well with at
least one existing PPI [2]. Tbe development of this
approach will be based on one package of plates such as
the one shown in Fig. 2.

Retention time
The retention time ( t , ) is provided by two equations:
t, = d f i / V t
t, = A L / &

Piv

line

Piw

line

(1)

(2)
where V, = rising velocity of the
bubbles, cm/s; d = distance between plates, cm; A = transversal
area, cm2, (u) ( b ) in Fig. 2; L =
separator length, cm; and
=
flow through A , cm3/s (Fig. 1).
If a and b are much greater than
the distance between plates d,
then R, = d / 2 . Hence, the Reynolds number ( N R c )is given by:

NRc= Pd&p/Au
(3)
where p = fluid density (usually
the same as water); and u = fluid
viscosity (usually the same as
water). Therefore:

A = 2d&P/UNRc
(4)
Combining Eq. (1)) ( 2 ) and (4):
L =

fi/2PV,

But since u / p = u, where


kinematic viscosity, finally:
A = 2d&/uNRc
L = uNRc f i / 2 V t

(5)
u

=
(6)
(7)

Eq. (6) and (7) are design equations; the terms Q A , p and u are
known for each case, and V, is a
function of the minimum globe
diameter to be separated. Then,
by Stokes Law:

vt

=(g/W(p,

- P O P 2 (8)

PRIMARY TREATMENT METHODS


wbere g = acceleration due to
gravity; u = absolute viscosity of
water; pw = density of the water; ,
p. = density of the oil; and D =
96

Pivot line

diameter of the oil particle. (All of


the above equations must be used
with consistent units.)
Since there are two equations-(6) and (7)--and four unknown variables-A,
L, d and
"-two
variables must be arbitrarily fixed, and unless space restrictions are critical, it is convenient to assign values to d and Nm.
Because PPI dimensions are
much smaller than the equivalent
API separator, it is possible to design with laminar flow-i.e.,
a
Reynolds number equal to or less
than 2,000. In addition, the
smaller the distance between
plates (d), the smaller the transversal area required for a given
flowrate and a given Reynolds
number; therefore, the greater the
efficiency 131. On the other hand,
a small distance could mean clogging and diminished flow area by
floating debris and materials not
retained by inlet trash racks. This
would increase maintenance costs.
Taking the above into consideration, it seems convenient to design in the following ranges:

<

--.i
a02

- 300

aw
0.M

-~~

9.05

/
/
/
/
\
\ 1

0.1 5

\
\

<

a'o

a20

-100

- 70

500 NRa 2,000 and


1in<d<4in

Eq. (6) and (7) may be represented graphically to cover these


ranges, as shown by the nomographs in Fig. 3 and 4.

Sample calculation
It is desired to treat an oily flow with the following
characteristics: total flow = 27.8 l/s; kinematic viscosity = 0.011 centistokes*; rising velocity = 0.018 cm/s;
distance between plates = 7.5 cm; Reynolds number =
2,000. The separator is to have two channels, each one
with two packages of plates, i.e., & = 27.8/4 = 6.95
l/s. What should be the total area and the length of the
separator?
From Fig. 3, A = 4,740 cm2 (total area = 4A =
18,960 cm2), and from Fig. 4, L = 865 cm.
For a given type of oil (an assigned po value) at a
fixed temperature, V, depends only on globule diameter.
Therefore, if the globule-diameter distribution of the
oily flow is available, it may be superimposed on the
rising velocity in Fig. 4. The nomograph will then
provide the separator length to achieve a desired percentage of oil removal.
*I #toke = (g)/[(s)(cm)(p)J; I centirtoke = 0.01 stoke

References
C., Sump daign for oil/wata Icpllrton, Chan Sy, NOV.
2. Kirb A. W.W., The Separation of Petroleum Oils from A q u w E
m
Tk
Enginrm, Apr. 1964.
3. R a m k Z., 11,and Momo L., O., Eatudio Experimental de S e p a r d ~
AcdtaA a por Gravedad en Equipo Piloto, Revhta del INtlNto hd
u n o del$l*r6leo, July 1973.

8h

The author
Julio C. [Link].u s u f I cnginca ofY
ent of the C o d a
s g o f r N a c i o d del
Pea6le0, Cmiik 242, Condn, chile,
when he haa been in char@ of d d @
pmjcct iupvvirion and stutin up of
rdinay's pollution-oontrol fJitiea. H
hu worked for the u m e mmpny
previoutly holding ptmitiorv in
&D b r a t o r y and u iubtitua cbl
for RLD quality [Link]
ho ds a chemical e n g i d q
U n i v d d a d Tbcnica del

'4

ym

INDUSTRIAL WASTEWATER AND


SOLID WASTE ENGINEERING

Edited by

Vincent Cavaseno
and the Staff of Chemical Engineering

McCraw-Hill Publications Co., New York, N.Y.

Common questions

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The calculation of rising velocity is pivotal in the design of a parallel-plates separator as it determines how quickly oil globules can rise through the separator to reach the surface for removal. This velocity is a function of factors such as globule diameter, density difference between oil and water, and fluid viscosity . Accurate calculation ensures that separator dimensions accommodate the specific rise characteristics of the treated effluent, directly influencing the length and configuration needed to achieve efficient separation and meet oil removal targets . Proper rising velocity estimation helps optimize separator design to ensure effective operation under given conditions .

The retention time in a parallel-plates separator impacts its design by determining the necessary dimensions and configuration for effective separation of oil globules. It is influenced by factors such as the rising velocity of the bubbles, the distance between plates, and the transversal area . Retention time is calculated using specific equations that consider these variables, and proper design ensures that oil globules cross the separator efficiently to reach the liquid surface .

Stokes' Law is applied to determine the rising velocity of oil globules in a parallel-plates separator, which is a critical factor in designing the separator's dimensions . The rising velocity, Vt, is influenced by the diameter of the oil particle, the difference in density between the oil and water, the acceleration due to gravity, and the absolute viscosity of the water . These factors are combined in an equation derived from Stokes' Law, ensuring that separators are designed to facilitate the rise of oil globules efficiently to the surface where they can be removed .

The nomograph provided in the design of a parallel-plates interceptor assists in determining the necessary separator dimensions for achieving specific oil removal targets by graphically representing the relationships between key variables such as the rising velocity of oil globules, plate distance, and Reynolds number . By inputting known values like the flow characteristics and desired percentage of oil removal, the nomograph helps in identifying optimal separator dimensions that will meet these targets efficiently. This approach supports engineers in visualizing the impact of different design choices and streamlining the design process .

Parallel-plates interceptors (PPI) are advantageous over traditional API separators due to their smaller size and reduced oil path from the undersurface of inclined plates to the liquid surface, leading to more efficient oil recovery. They also minimize common problems associated with API separators such as construction cost, space requirements, evaporation losses, and maintenance of operating conditions within safe limits . Furthermore, PPIs provide automatic oil recovery with the use of skimmers and reduce the need for multiple pumps .

The use of parallel plates inclined at a specific angle aids in the separation process by allowing oil to coagulate on the undersurface of each plate and then slide upward towards the liquid surface where it can be skimmed off . This configuration enhances the separation efficiency by reducing the physical distance that oil particles must travel to separate from the water, thus optimizing the process for quick and effective separation of oil and water . Moreover, this inclination aids in the collection of solid particles which slide down to the bottom, contributing to separation effectiveness .

The Reynolds number plays a crucial role in the design efficiency of a parallel-plates interceptor by indicating the flow regime. A Reynolds number equal to or less than 2,000 indicates laminar flow, which is desirable for higher separation efficiency and minimizes issues such as turbulence that can cause remixing of separated oil and water . By choosing appropriate design values within the range of 500 to 2,000 for the Reynolds number, the separator can operate effectively without excessive pressure drops and maintenance issues .

When determining the distance between plates in a parallel-plates separator, it is crucial to ensure that the distance is small enough to promote efficient separation and reduce required transversal area for a given flowrate and Reynolds number . However, it must not be so small that it leads to clogging from debris and materials, which would increase maintenance costs. Designing within the recommended range ensures an optimal balance between efficiency and operational challenges .

PPIs have gained popularity recently due to their ability to mitigate many of the drawbacks of traditional API separators, such as high construction costs, space requirements, and safety hazards. Their smaller size and improved separation efficiency make them an attractive option for modern refineries. Despite limited published design criteria, practical demonstrations of their effectiveness, such as in reducing operational complexities and lowering evaporation losses, have driven their adoption . Practical experiences and successful applications have propelled trust and interest in PPIs even with scant theoretical documentation .

Choosing a very small distance between plates in a PPI can lead to clogging and reduced flow area due to floating debris not retained by inlet trash racks . This increases maintenance costs and can disrupt the separation process. To mitigate these drawbacks, designers must balance efficiency with practical considerations by ensuring the plate distance avoids clogging while still optimizing the separator's performance. Following recommended design ranges and considering operational and maintenance aspects during the design phase help to address these issues .

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