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Compleximetric Titration Techniques

The document describes three experiments involving titration: 1) Determination of water hardness using EDTA and EBT indicator. 2) Determination of dissolved oxygen using sodium thiosulfate and starch indicator. 3) Determination of acid dissociation constant (pKa) of a weak acid using sodium hydroxide and a pH meter. The document provides details on the titrants, standards, indicators and results reported for each experiment.

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Kim Reine Mariano
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6 views1 page

Compleximetric Titration Techniques

The document describes three experiments involving titration: 1) Determination of water hardness using EDTA and EBT indicator. 2) Determination of dissolved oxygen using sodium thiosulfate and starch indicator. 3) Determination of acid dissociation constant (pKa) of a weak acid using sodium hydroxide and a pH meter. The document provides details on the titrants, standards, indicators and results reported for each experiment.

Uploaded by

Kim Reine Mariano
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd

Experiment

Titrant

Standa
rd for
titrant

SR
Titrant:Stand
ard

Indicator

Practicals

NaOH

KHP

1:1

Phenolphthalein
Colorless pink

Complexime
tric
determinati
on of Water
Hardness

EDTA
0.47g EDTA in
250mL dist.
water + pinch
MgCl2

CaCO3

1:1

EBT
Wine red blue

Determinati
on of
Dissolved
Oxygen
(D.O)p. 31

Na2SO3
>Boil 250mL
Dist. H2O
> +6-7 g
Na2S2O3
> + pinch
Na2CO3

Determinati
on of pKa of
a weak acid
pp. 28

NaOH
Boil 250 mL
Dist.
H2O + ~1 g
NaoH

KIO3

Starch
(colorless-yellowblue)

Result
reported
as

Sample

Notes of Experiment

% acid

Acids
(Vinegar,
Soda, HCl)

Ppm
CaCO3

Water sample
(group
unknown)

MgCl2 added to
EDTA for sharper
endpoint

Delayed addition of
starch indicator
indirect titration
Ppm D.O

Water from
botanical

KIO 3+ KI ( acid ) I 2
+S 4 O62
I 2 + S2 O32 I

pH meter
(no indicator/no
color change)

Graph of
pH vs. mL
NaOH
added

Acid
(lactic, formic,
acetic)

Use of pH meter

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