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Creams Lab Notes

A cream is a semi-solid emulsion used for topical drug delivery, containing active pharmaceutical ingredients in a cream base. There are two main types of creams: oil-in-water (o/w) and water-in-oil (w/o), each with distinct properties, uses, advantages, and disadvantages. The document also outlines preparation methods for creams and differentiates between emulsions and creams.

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0% found this document useful (0 votes)
3 views5 pages

Creams Lab Notes

A cream is a semi-solid emulsion used for topical drug delivery, containing active pharmaceutical ingredients in a cream base. There are two main types of creams: oil-in-water (o/w) and water-in-oil (w/o), each with distinct properties, uses, advantages, and disadvantages. The document also outlines preparation methods for creams and differentiates between emulsions and creams.

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hannah
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 Definition of a cream

o A cream is viscous, semi-solid emulsion (either o/w or w/o


depending on the emulsifying agent used)
o Pharmaceutical / medicated cream is a semi-solid dosage form
that contain one or more active pharmaceutical ingredients
dispersed or dissolved in a cream base
 Function: Used topically for therapeutic or cosmetic purposes
 Topical drug delivery
o Definition: The application of a drug formulation directly to
the skin or mucous membranes to exert a local or systemic
effect
o Why use this route?
 Localised effect
 Local anaesthetics – numbing of the skin
 Anti-inflammatories – treat inflammation on the
skin
 Oral route is unavailable
 Patients with nausea / vomiting, difficulties
swallowing (paediatrics + geriatrics)
 Oral drug delivery is unsuitable
 Extremely lipophilic drug – very poor oral
absorption and better absorption through the skin
 Bypass hepatic metabolism
o Routes of absoprtion
 Transcellular – Through the cells of the stratum
corneum
 Intercellular – Between the cells of the stratum
corneum
 Appendageal – Via hair follicles, sweat glands, or
sebaceous glands (minor route)
o Factors affecting drug absorption

Factor Simple Explanation


The drug must separate from the cream or ointment base before it can
Release from base
enter the skin.
Concentration A higher drug concentration on the skin surface drives the drug into
gradient the skin faster.
Drugs that are somewhat lipophilic (fat-loving) can pass through the
Lipophilicity
oily skin layers better.
Smaller drug molecules move through the skin more easily than
Molecular size
larger ones.
Diffusion through The drug must pass through the layers of skin, especially the outer
layers barrier (stratum corneum).
o
 Types of creams
o o/w creams
- composition: usually contain an equal amount of oil and
water or a lower amount / conc. of oil
 small droplets of oil dispersed in an aqueous
continous phase
- emulsifying agents:
 synthetic waxes (macrogols, cetomacrogols) – water
soluble bases
 self-emulsifying waxes (emulsifying wax)
 fatty alcohols (cetostearyl alcohol)
 surfactants:
 Non-ionic – polysorbates (Tweens – tween 20,
tween 80)
 Anionic (-ve charge hydrophilic head group) –
sodium lauryl sulfate (SLS), sodium sulfate
 Natural emulsifiers: acacia, gelatin
- Properties / characteristics: white, lightweight (low
viscosity), non-greasy, smooth, spreads easily, rapidly
absorbed, easily water washable
- Uses:
 Topical drug delivery of APIs for acute conditions (e.g.
anti-inflammatories, antifungals, local anaesthetics
etc.)
 Sooth irritated / inflamed skin – acute eczema
flare-ups, allergic dermatitis, and insect bites
 Cosmetic applications (e.g. moisturising creams,
sunscreens etc.)
- Advantages: usually quicker drug release rate (water
facilitates the diffusion), rapid drug absorption, and better
patient acceptability
- Disadvantages: Susceptible to microbial growth – affects
stability (higher water content and often requires a
preservative), short residence time on the skin (can be
easily removed)
o w/o creams
- composition: usually contain a higher amount of oil than
water
 small droplets of water dispersed in an oily continous
phase
- emulsifying agents:
 Natural emulsifiers: wool fat (lanolin), bees wax, wool
alcohols (absorption bases)
fatty alcohols (cetyl alcohol, stearyl alcohol)
surfactants:
 Non-ionic – sorbitan esters (Spans – span 60,
span 80), glyceryl monostearate
- Properties / characteristics: creamy white, heavy feel
on skin (high viscosity), greasy, occlusive (forms a barrier),
difficult to spread (feels sticky), not easily water washable
- Advantages: usually slower drug release rate (suitable for
chronic conditions), long-term stability compared to o/w
creams (less susceptible to microial growth), fewer
preservatives required, emollient (long-term moisturising
and hydrating effect) and provides a protective barrier,
longer residence time on the skin
- Disadvantages: poor patient acceptibility due to sticky,
heavier feel on the skin
- Uses:
 Topical drug delivery of APIs for chronic conditions
(e.g. chronic dry skin conditions – psoriasis, eczema)
 Emollient therapy and barrier protection (e.g. hand
creams, nappy creams etc.)
 Cosmetic application – night creams etc.
o Preparation methods of creams
- Fusion Method
 Used for: Emulsifying waxes, oils, and emulsifiers
(aren’t sensitive to heat - thermolabile)
 Steps:
 Heat the oil phase (oils, waxes, emulsifiers) in a
separate container.
 Heat the aqueous phase (water, water-soluble
ingredients) in another container.
 Slowly combine the two phases while stirring
continuously.
 Allow the mixture to cool, stirring occasionally
until it thickens into a cream.

- Levigation (wet grinding)


 Used for: Incorporating solid ingredients into the
cream base.
 Steps:
 Triturate the solid drug or active ingredient with
a small amount of the cream base or a
levigating agent.
 Once smooth, gradually add more base, continuing to
mix thoroughly.
 Ensure the mixture is free of grit and uniformly
blended.

-Geometric Dilution
 Used for: Mixing small amounts of active ingredients
with a larger base.
 Steps:
 Take a small amount of the active ingredient
and mix it with an equal portion of the base.
 Add an equal amount of base to the mixture
and blend.
 Continue adding base in equal portions, mixing
well each time until the entire base is
incorporated.
o Doubling up technique
- involves gradually mixing equal amounts of two substances
in successive steps, doubling the quantity with each step,
until a uniform mixture is achieved
- Used when:
 When mixing a small amount of an active ingredient
or colourant into a larger quantity of base
 Ensure even distribution and prevents clumping or
uneven dispersion
- If you have 1 g of drug and 15 g of cream base:
Step 1: Mix 1 g drug + 1 g base
Step 2: Add 2 g base (total 4 g), mix
Step 3: Add 4 g base (total 8 g), mix
Step 4: Add remaining 7 g base, mix
Differences between Emulsions and Creams

Properties Cream Emulsion

A liquid or semi-solid
A semi-solid dosage form
Definition system of two immiscible
containing an emulsion base
liquids (oil and water)

Semi-solid (thicker, Usually liquid (but can be


Appearance
spreadable) semi-solid, e.g. in creams)

Broader use – in oral,


Function and Used topically for therapeutic
topical, or parenteral
Application or cosmetic purposes
formulations

Typically contains an O/W or Composed of two


Composition W/O emulsion along with immiscible liquids, one
other excipients dispersed in the other

Hydrocortisone cream (O/W), Milk (natural emulsion),


Example
cold cream (W/O) emulsified oral syrups

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