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Sample 1

The document presents data from an X-ray diffraction analysis of the H2SM sample, detailing the strongest three peaks along with their corresponding 2Theta, d-spacing, intensity, and other parameters. It includes a comprehensive peak data list and outlines the measurement conditions, such as X-ray tube specifications and scanning parameters. Additionally, it describes the data processing conditions applied during analysis, including smoothing and background subtraction methods.
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0% found this document useful (0 votes)
11 views4 pages

Sample 1

The document presents data from an X-ray diffraction analysis of the H2SM sample, detailing the strongest three peaks along with their corresponding 2Theta, d-spacing, intensity, and other parameters. It includes a comprehensive peak data list and outlines the measurement conditions, such as X-ray tube specifications and scanning parameters. Additionally, it describes the data processing conditions applied during analysis, including smoothing and background subtraction methods.
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

*** Basic Data Process ***

Group : Standard
Data : H2SM

# Strongest 3 peaks
no. peak 2Theta d I/I1 FWHM Intensity Integrated Int
no. (deg) (A) (deg) (Counts) (Counts)
1 2 7.7478 11.40158 100 0.28940 181 3043
2 20 22.9769 3.86754 96 0.41960 174 3569
3 3 8.6542 10.20936 69 0.33510 124 2320

# Peak Data List


peak 2Theta d I/I1 FWHM Intensity Integrated Int
no. (deg) (A) (deg) (Counts) (Counts)
1 7.1400 12.37073 7 0.16000 12 208
2 7.7478 11.40158 100 0.28940 181 3043
3 8.6542 10.20936 69 0.33510 124 2320
4 9.0200 9.79613 10 0.10000 19 176
5 11.3050 7.82072 4 0.19000 8 112
6 11.7000 7.55756 6 0.40000 11 275
7 13.0100 6.79937 6 0.22000 10 115
8 13.7158 6.45103 10 0.25830 18 247
9 14.2800 6.19739 3 0.08000 5 42
10 14.5975 6.06330 18 0.31500 33 507
11 15.2600 5.80153 8 0.17340 14 170
12 15.7300 5.62922 12 0.26000 21 336
13 17.0800 5.18721 3 0.06000 5 41
14 17.5383 5.05268 9 0.34330 16 300
15 19.0300 4.65985 5 0.22000 9 126
16 20.2000 4.39251 6 0.26000 11 163
17 20.6666 4.29438 12 0.26670 21 291
18 22.0300 4.03159 5 0.22000 9 141
19 22.5000 3.94843 5 0.16000 9 154
20 22.9769 3.86754 96 0.41960 174 3569
21 23.6407 3.76043 42 0.46650 76 1771
22 24.2250 3.67103 24 0.29000 43 640
23 25.5000 3.49030 6 0.22000 10 141
24 25.7200 3.46094 9 0.24000 16 204
25 26.4600 3.36580 9 0.21340 16 220
26 26.7400 3.33119 9 0.28000 17 233
27 27.2600 3.26882 3 0.20000 6 62
28 27.8800 3.19752 3 0.08000 5 31
29 28.1400 3.16856 3 0.12000 5 60
30 29.0883 3.06739 12 0.19670 21 239
31 29.8300 2.99278 14 0.54000 26 581
32 30.2200 2.95504 7 0.20000 12 143
33 31.1300 2.87070 3 0.06000 5 43
34 32.6150 2.74331 4 0.19000 8 84
35 34.2150 2.61859 6 0.25000 10 136
36 34.7300 2.58093 3 0.30000 6 113
37 35.5900 2.52051 4 0.22000 8 105
38 35.9383 2.49688 7 0.22330 12 135
39 37.0500 2.42447 4 0.14000 8 66
40 37.3200 2.40755 5 0.16000 9 112
41 38.0950 2.36034 3 0.07000 5 35
42 44.8700 2.01842 12 0.26000 22 291
43 45.2766 2.00123 12 0.35330 21 357
44 46.2800 1.96015 4 0.22000 7 114
45 47.2500 1.92215 4 0.38000 8 180
46 48.4600 1.87695 5 0.28000 9 171
47 51.5850 1.77034 3 0.13000 5 53
48 51.9000 1.76034 3 0.16000 6 80
49 54.6650 1.67765 5 0.15000 9 81
50 54.9866 1.66860 4 0.22670 7 128
51 62.0500 1.49453 3 0.18000 5 127
52 63.4100 1.46571 4 0.22000 7 96
53 63.9250 1.45514 3 0.19000 5 51
peak 2Theta d I/I1 FWHM Intensity Integrated Int
no. (deg) (A) (deg) (Counts) (Counts)
54 64.3150 1.44726 4 0.13000 7 59
55 65.6000 1.42198 4 0.16000 7 105
56 65.9866 1.41459 4 0.17330 7 61
57 66.9000 1.39747 4 0.28000 8 120
58 67.1250 1.39333 4 0.11000 7 45
59 67.4900 1.38668 3 0.18000 5 59
*** Basic Data Process ***

# Data Infomation
Group : Standard
Data : H2SM
Sample Nmae : H2SM
Comment : ok
Date & Time : 07-06-21 16:52:54

# Measurement Condition
X-ray tube
target : Cu
voltage : 40.0 (kV)
current : 30.0 (mA)
Slits
Auto Slit : not Used
divergence slit : 1.00000 (deg)
scatter slit : 1.00000 (deg)
receiving slit : 0.30000(mm)
Scanning
drive axis : Theta-2Theta
scan range : 7.0200 - 70.0000 (deg)
scan mode : Continuous Scan
scan speed : 2.0000 (deg/min)
sampling pitch : 0.0200 (deg)
preset time : 0.60 (sec)

# Data Process Condition


Smoothing [ AUTO ]
smoothing points : 17
[Link] [ AUTO ]
sampling points : 17
repeat times : 30
Ka1-a2 Separate [ MANUAL ]
Ka1 a2 ratio : 50 (%)
Peak Search [ AUTO ]
differential points : 15
FWHM threhold : 0.050 (deg)
intensity threhold : 30 (par mil)
FWHM ratio (n-1)/n : 2
System error Correction [ NO ]
Precise peak Correction [ NO ]
< Group: Standard
I (CPS)
Data: H2SM >

Profile

400

200
I (CPS)

Smoothing Profile

400

200
I (CPS)

B.G. Subtract Profile

400

200
I (CPS)

Ka1 Profile

400

200
I (CPS)

Peak

400

200

0
10 20 30 40 50 60 70
Theta-2Theta (deg)

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