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Particle Size Sepration Through Seiving Method

The document outlines the procedure for separating and classifying powder particles by size using the sieving method. It details the principle of sieving, required apparatus, step-by-step procedure, and calculations for determining weight retention. Additionally, it discusses applications, advantages, limitations, and precautions associated with the method.

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arhamabbas14xyx
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8 views2 pages

Particle Size Sepration Through Seiving Method

The document outlines the procedure for separating and classifying powder particles by size using the sieving method. It details the principle of sieving, required apparatus, step-by-step procedure, and calculations for determining weight retention. Additionally, it discusses applications, advantages, limitations, and precautions associated with the method.

Uploaded by

arhamabbas14xyx
Copyright
© All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

PARTICLE SIZE SEPARATION BY SEIVING METHOD

Aim:
To separate and classify powder particles according to their size using the sieving method.

Principle:
Sieving is a mechanical method used to separate particles based on differences in particle
size. When a powdered sample is placed on a sieve and shaken, smaller particles pass
through the openings (apertures) of the sieve, while larger particles are retained on the
surface.

Sieves are arranged in descending order of aperture size (largest opening at the top and
smallest at the bottom). The separation depends upon mesh size.

Mesh number indicates the number of openings per linear inch of the sieve. Higher mesh
number indicates smaller particle size, while lower mesh number indicates larger particle
size.

Apparatus Required:
• Standard test sieves (10, 20, 40, 60, 80 mesh)
• Mechanical sieve shaker / Manual shaking setup
• Electronic weighing balance
• Brush
• Sieve lid
• Receiving pan
• Sample powder

Procedure:
1. Select appropriate standard sieves.
2. Arrange the sieves in descending order of mesh size (coarse to fine).
3. Place a receiving pan at the bottom of the sieve stack.
4. Accurately weigh the powder sample.
5. Transfer the sample onto the top sieve.
6. Cover the sieve stack with a lid.
7. Shake manually for 10–15 minutes or use a mechanical sieve shaker for uniform
shaking.
8. After completion, carefully remove each sieve.
9. Collect and weigh the powder retained on each sieve separately.
10. Record the observations.
Observations Table:
Sieve No. Weight Retained (g) % Weight Retained

10

20

40

60

80

Pan

Calculations:
% Weight Retained = (Weight Retained on Sieve / Total Weight of Sample) × 100

Result:
The given powder sample was successfully separated into different particle size fractions
using the sieving method.

Applications:
• Determination of powder fineness
• Evaluation of flow properties
• Tablet and capsule formulation
• Quality control testing

Advantages:
• Simple and economical method
• Easy to perform
• Suitable for coarse and moderately fine powders

Limitations:
• Not suitable for very fine powders
• Irregular particle shape affects accuracy
• Electrostatic charge may interfere with separation

Precautions:
• Ensure sieves are clean and dry before use.
• Do not overload the sieve.
• Avoid excessive shaking.
• Record weights accurately.
• Handle sieves carefully to prevent damage.

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